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494results about How to "Low solid content" patented technology

Preparation method of polymer weak gel deep profile control agent

The invention relates to a preparation method of a polymer weak gel deep profile control agent. The preparation method comprises the following steps of preparing sodium carboxymethyl cellulose and distilled water into sodium carboxymethyl cellulose water solution of which the mass percentage is 1%-2%; adding acrylamide of which the mass is 2-8 times as great as that of the sodium carboxymethyl cellulose into the sodium carboxymethyl cellulose water solution, and then adding a cross-linking agent which accounts for 0.01%-2% of the total weight of the sodium carboxymethyl cellulose and the acrylamide; enabling nitrogen to enter into a closed system and isolating the air, and adding an initiating agent which accounts for 1%-2% of the total mass of the sodium carboxymethyl cellulose and the acrylamide; and discharging after carrying out constant-temperature reaction for 4-12 hours under the temperature of 30-60 DEG C. According to the preparation method disclosed by the invention, the acrylamide is grafted to the sodium carboxymethyl cellulose, polymer weal gel with a mesh structure is formed under the action of the initiating agent and the cross-linking agent, and a polymer weak gel system integrates the advantages of the sodium carboxymethyl cellulose and the acrylamide.
Owner:WUHAN INSTITUTE OF TECHNOLOGY

Low solid phase and micro-foam drilling fluid or completion fluid capable of being used circularly

The invention discloses a low solid phase and micro-foam drilling fluid or completion fluid capable of being used circularly, comprising the following components in portions by weight: 3-4 portions ofmicro-foam and low-solid phase composite treating agent SD-LGA capable of being used circularly, 0.5-1 portion of low-density and low-solid phase tackifier SD-LGV, 0.5-1 portion of low-density regulator SD-LFD, 0.5-1 portion of low-density foam stabilizer SD-LFS, 0.5-1 portion of low-density flowing type regulator SD-LFR and 100 portions of clear water. The preparation method comprises the following steps: sequentially adding the components into the clear water in a conventional preparation method according to the weight content of each component at normal temperature and normal pressure, andthen, uniformly mixing and stirring the components for use. The drilling fluid or completion fluid has the advantages of low solid phase, low density, high foam stability, high structural strength, high fluid phase viscosity, high flexibility, high lubricity, very low toxicity, easy biodegradation, circular use, little influence on environment, little harm to a storage layer, high permeability recovery value, good effect on protection of an oil-gas layer and the like, and is widely applied to a drilling engineering technology of petroleum and geology.
Owner:DONGYING TAIER GASOLINE TECH

Composite salt low-activity anti-sloughing drilling fluid and construction method thereof

InactiveCN103146363AAvoid differential pressure lossThe system has strong chemical inhibition and anti-collapse effectDrilling compositionSealing/packingFriction reductionMass ratio
The invention discloses a composite salt low-activity anti-sloughing drilling fluid and a construction method thereof. The composite salt low-activity anti-sloughing drilling fluid consists of the following raw materials in percentage by mass: 0.2-0.3% of drilling fluid viscosifier, 2-3% of carboxymethyl starch, 1.5-2% of aqueous dispersion cation emulsified asphalt, 0.2-0.3% of anti-salt anti-calcium filtrate reducer, 1% of sulfonated phenolic resin, 2% of acid-soluble temporary seal reservoir protective agent, 1% of superfine calcium, 0.1% of caustic soda and the balance of clean water. In construction, the composite salt accounting for 5-15% of the dosage of the composite slat low-activity anti-sloughing drilling fluid is added, and the composite salt is formed by mixing sodium formate and sodium chloride at a mass ratio of 2:1. By utilizing the composite salt, the function of chemically suppressing mudstone and preventing sloughing in the drilling fluid as well as the density of the drilling fluid are improved. With strong chemical suppression and low solid phase, the composite salt low-activity anti-sloughing drilling fluid completely meets the strict high-quality requirements of a long open-hole section for friction reduction and resistance reduction of the drilling fluid.
Owner:中国石油集团川庆钻探工程有限公司长庆钻井总公司

Process for preparing drilling fluid for preventing polycrystalline diamond compact (PDC) bit balling

The invention relates to a process for preparing drilling fluid, in particular to a process for preparing the drilling fluid for preventing polycrystalline diamond compact (PDC) bit balling. The process comprises a construction process and a dosage formula of treating agents and is characterized in that: according to the dosage formula, the treating agents are prepared by mixing clear water polymer original slurry, poly anionic cellulose (PAC), calcium carbonate (QS-4), carboxymethyl starch (CMS), sulfonated phenolic resin(SMP-2), water dispersible cation emulsified asphalt powder (SFT-1), sodium chloride(NaCL) and sodium formate (WT-1) in a mass ratio of 1,000:2-3:30-40:20-30:2-3:1.5-2:50-100:20; and the construction process comprises the following steps of: according to a circulation circle, uniformly mixing a coating agent PAC, a filtrate reducer CMS, a salt and high-temperature resistant filtrate reducer SMP-2 and an anti-sloughing lubricant SFT-1 for 12h at first; adding QA-4, NaCL, WT-1 into the mixture and uniformly mixing the mixture; and regulating the mixture to have a density Rho of 1.06 to 1.10g/cm<3>, a funnel viscosity T of 38 to 45s and an API water loss FL of 4 to 6ml. The process has the advantages of effectively preventing the balling of a sticking bit and a PDC bit at a lower curved section, reducing a frictional resistance and a torque, eliminating a sticking phenomenon, improving a mechanical drilling rate and ensuring downhole safety.
Owner:中国石油集团川庆钻探工程有限公司长庆钻井总公司

Recovery method of terephthalic acid/isophthalic acid refinement mother liquor

The invention discloses a recycling method of mother liquor, particularly a method for recycling refined mother liquor of phthalic acid / m-phthalic acid. The method comprises the steps: the mother liquor in a mother liquor tank is pumped into a mother liquor cooling tank, and the cooling tank is vacuumized, the air after flash evaporation is pumped into a cooler, after condensation, the gas returns back to the mother liquor cooling tank; the mother liquor after cooling in the mother liquor cooling tank is pumped into a filter for filtering; after filtering of the mother liquor, the filtering liquor is put into a filtering liquor collecting tank and then pumped into an incinerator for tail gas drenching; after a filter cake is formed on the inner surface of the filter element of the filter, the filtering liquor at the upper part of the tube plate of the filter is discharged; the filtering liquor at the inner lower side of the filter element and lower part of the tube plate of the filter is discharged to a buffer tank; the filter cake blow-dried by oxydic tail gas is pressed into a pulping tank; and deionized water is added into the filter to wash the undischarged filter cake to the pulping tank. By adopting filtering technology with high accuracy, the method recovers the useful components in the centrifuger mother liquor, reduces the values of solidity and chemical oxygen demand (COD) of filtering liquor, and improves the environment.
Owner:CHINA PETROLEUM & CHEM CORP

Special coloring agent of diammonium phosphate compound fertilizer and preparation method thereof

The invention discloses a special coloring agent of a diammonium phosphate compound fertilizer, comprising the following constituents: 40-50 parts of humic acid salt, 0.1-3 parts of carbon soot, 2-4 parts of acid black, 1-2 parts of acid brilliant scarlet, 0.2-1 part of sodium hexametaphosphate, and 40-56.7 parts of water by weight parts; the preparation process is that: the material is prepared by weight parts, water is added in a vertical round reaction tank, and then the humic acid salt, the carbon soot, the acid black and the acid brilliant scarlet are added and are stirred uniformly, andthen sodium hexametaphosphate is added, the mixture is stirred continuously and uniformly, so as to obtain the special coloring agent of the diammonium phosphate compound fertilizer; the invention solves the problems that the diammonium phosphate particles produced under an acid slurry condition are easy to decolorize and the chromaticity is unstable; the special coloring agent of the diammonium phosphate compound fertilizer is green and environmental-protection, has no pollution and is beneficial to the growth of crops; the product is in a liquid state and transported closely, and has convenient usage; the raw material is cheap and easy to obtain, the cost is low and the economic benefit is good.
Owner:中化重庆涪陵化工有限公司
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