Image forming toner, and developer and process cartridge using the toner
A toner and colorant technology, applied in the field of toner, can solve the problems of non-chargeable, poor heat-resistant storage of toner, and low productivity
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
preparation example Construction
[0100] For the preparation of the binder of the toner of the present invention, for example, the following method can be used. The polyol (PO) and polycarboxylic acid (PC) are heated at 150-280°C in the presence of known catalysts (such as tetrabutoxy titanate and dibutyl tin oxide). Then, the generated water is removed If necessary, the pressure can be reduced to prepare a polyester resin with hydroxyl groups. Then, the polyester resin polyisocyanate (PIC) is reacted at a temperature of 40-140°C to prepare a prepolymer (A) with isocyanate groups. Further, The prepolymer (A) is reacted with the amine (B) at a temperature of 0-140°C to prepare a urea-modified polyester.
[0101] When (PIC), (A) and (B) are reacted, a solvent can be used if necessary. Suitable solvents include solvents that do not react with (PIC), and specific examples thereof include aromatic solvents such as toluene and xylene; ketones such as acetone, methyl ethyl ketone and methyl isobutyl ketone; esters such...
Embodiment 1
[0187] (Preparation of granular resin emulsion)
[0188] Install a stirrer and a thermometer in the reaction vessel, add 683 parts of water, 11 parts of methacrylic acid ethylene oxide adduct sodium sulfate (ELEMINOL RS-30, Sanyo Chemical Company), 83 parts of styrene, 83 parts Methacrylic acid, 110 parts of butyl acrylate, and 1 part of ammonium persulfate, and stirring at 3,800 rpm for 30 minutes. Therefore, a white emulsion was prepared. The emulsion was heated at 75°C and reacted for 4 hours. Subsequently, 30 parts of 1% ammonium persulfate aqueous solution were added to the emulsion, and the mixture was allowed to stand at 75°C for 8 hours. Therefore, granular resin dispersion (1), (vinyl resin aqueous dispersion) (ie copolymer styrene, methacrylic acid, butyl acrylate and sodium sulfate of methacrylic acid ethylene oxide adduct), was prepared . The dispersion (1) has a volume average particle diameter of 110 nm, (measurement particle size distribution analyzer LA-920 (K...
Embodiment 2
[0229] The steps of preparing toner (1) were repeated except that the amount of organically modified montmorillonite was changed from 30 parts to 48 parts. Toner (6) is prepared.
PUM
| Property | Measurement | Unit |
|---|---|---|
| melting point | aaaaa | aaaaa |
| glass transition temperature | aaaaa | aaaaa |
| particle diameter | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More 