Boron-doping diamond film modification-based PEMFC (Proton Exchange Membrane Fuel Cell) bipolar plate and preparation method thereof
A technology of boron-doped diamond and diamond thin film, which is applied in the field of batteries, can solve the problems of battery life and performance reduction, pollution of proton exchange membranes, increase of battery internal resistance, etc., to reduce weight and cost, high oxygen evolution overpotential, eliminate loss live effect
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[0042] The main steps for preparing the fuel cell bipolar plate of the present invention include the pretreatment of the substrate and the deposition of the boron-doped diamond film. The deposition device of boron-doped diamond film consists of image 3 Shown.
[0043] 1. Substrate pretreatment
[0044] (1) Mechanically polish a 40×30×0.2mm stainless steel sheet to remove the oxide layer and pollutants on the surface.
[0045] (2) Surface ultrasonic treatment: ultrasonic treatment of the substrate surface in deionized water for 30 minutes.
[0046] (3) Use magnetron sputtering to deposit TI on stainless steel, and perform annealing treatment in an inert atmosphere such as argon to release the internal stress of the titanium film and avoid the passivation of the titanium film.
[0047] (4) For the mechanical grinding treatment of emery, the diamond powder with a size of 0.25 μm is used for mechanical grinding to cause scratches and defects on the surface of the titanium film.
[0048] 2....
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