AZO transparent conductive film paint, glass plated with the paint and preparation method thereof
A transparent conductive film and coating technology, applied in the direction of conductive coatings, coatings, etc., can solve the problems of high equipment cost, difficult production stability control, etc., achieve high conductivity, good aging resistance, and meet the effect of use requirements
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Embodiment 1
[0017] Add 10 kg of 0.1 mol zinc acetate into 50 kg of 50% (wt%) ethanol and mix, stir evenly, then add 0.5 kg of methyl ethyl ether, 0.2 kg of ethanolamine, and 1.0 kg of nitric acid in sequence, and stir thoroughly to obtain stable and transparent zinc oxide after 3 hours Sol. Then add 2 kg of 0.05 mol of aluminum nitrate and 0.01 kg of 0.1 mol of tin chloride solution to the sol, and stir thoroughly to obtain a composite AZO sol. Finally, 0.2 kg of sodium dodecylbenzenesulfonate was added and stirred thoroughly to obtain an AZO sol with negative charges on the surface.
[0018] Apply negatively charged AZO sol on the surface of ultra-clear float or solar ultra-clear embossed glass by electrostatic spraying method, dry at 80°C for 10 minutes, and then temper at 550°C to 700°C for 5 minutes to 12 minutes to obtain AZO transparent conductive film glass.
[0019] After testing, the transmittance in the visible light region reaches 83.0%-85.0%, and the film resistivity is 10 ...
Embodiment 2
[0021] Add 15 kg of zinc nitrate with a concentration of 0.2 mol into 50 kg of 60% (wt%) ethanol and 10 kg of acetic acid solution and mix, stir evenly, add 0.5 kg of dimethyl ethyl ether and 0.2 kg of triethanolamine, stir well, and obtain a stable solution after 2-3 hours Transparent zinc oxide sol. Then add 2kg of 0.01mol of aluminum nitrate and 0.1kg of 0.01mol of cerium chloride, and fully stir to obtain a composite AZO coating. Add 0.3 kg of sodium dodecylbenzenesulfonate and stir thoroughly to obtain an AZO sol with a negatively charged surface.
[0022] Electrostatically spray the negatively charged AZO sol on the surface of ultra-clear float or solar ultra-clear embossed glass, dry at 100°C for 8 minutes, and then temper at 550°C to 700°C for 5 minutes to 10 minutes to obtain transparent conductive film glass.
[0023] After testing, the transmittance in the visible light region reaches more than 85.0%, and the film resistivity is 10 -4 Ω·cm, with a haze of 12%, can...
Embodiment 3
[0025] Add 10 kg of zinc sulfate with a concentration of 0.1 mol into 50 kg of 60% (wt%) ethanol, add 8 kg of acetic acid solution and mix, stir evenly, add 0.3 kg of ethyl alcohol ether, 0.3 kg of diethanolamine, stir well, and obtain a stable and transparent solution after 3 hours zinc oxide sol. Then add 2 kg of 0.1 mol of aluminum nitrate, 0.01 kg of 0.1 mol of yttrium chloride solution, and 0.1 kg of 0.01 mol of molybdenum nitrate, and stir thoroughly to obtain a composite AZO coating. Add 0.2 kg of sodium cetyl sulfonate and stir thoroughly to obtain an AZO sol with a negatively charged surface.
[0026] Electrostatically spray the negatively charged AZO sol on the surface of ultra-clear float or solar ultra-clear embossed glass, dry at 80°C for 10 minutes, and then temper at 550°C to 700°C for 8 minutes to 12 minutes to obtain transparent conductive film glass.
[0027] After testing, the transmittance in the visible light region reaches 82.0%-85.0%, and the film resis...
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