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Mo-Si-B-W multi-phase composite material and preparation method thereof

A technology of mo-si-b-w and composite materials, which is applied in the field of composite materials, can solve the problems of high energy consumption and long cycle time, and achieve the effects of low energy consumption, short cycle time, and improved high-temperature strength

Active Publication Date: 2012-04-25
NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Moreover, in order to isolate and refine the primary Moss dendrites and eliminate casting defects in the material, the heat-treated material must be subjected to hot extrusion treatment. This method has the disadvantages of high energy consumption and long cycle time.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] The Mo-Si-B-W multi-phase composite material of this embodiment is made of the raw materials with the following atomic percentages: 11% silicon, 9% tungsten, 16% boron, and the balance is molybdenum; the mass purity of the silicon is not less than 98% , the mass purity of tungsten is not less than 99%, the mass purity of boron is not less than 99%, and the mass purity of molybdenum is not less than 99%; the silicon is silicon powder with a particle size not greater than 8 μm, and the tungsten is tungsten Boron is boron powder with a particle size not greater than 7 μm, and molybdenum is molybdenum powder with a particle size not greater than 6 μm.

[0022] The preparation method of the composite material of the present embodiment comprises the following steps:

[0023] Step 1. Weigh the raw materials according to atomic percentage, then place the weighed raw materials in a planetary ball mill, use absolute ethanol as a dispersant, and ball mill and mix under the conditi...

Embodiment 2

[0028] This embodiment is the same as Embodiment 1, except that the Mo-Si-B-W multiphase composite material is made of the following atomic percentages of raw materials: 5% silicon, 10% tungsten, 30% boron, and the balance is molybdenum.

[0029] The Mo-Si-B-W multiphase composite material prepared in this example has a tensile strength of 430 MPa at 1400° C. and a tensile elongation of 180%.

Embodiment 3

[0031] This embodiment is the same as Embodiment 1, except that the Mo-Si-B-W multiphase composite material is made of the following atomic percentages of raw materials: 15% silicon, 6% tungsten, 10% boron, and the balance is molybdenum.

[0032] The Mo-Si-B-W multiphase composite material prepared in this example has a tensile strength of 435 MPa at 1400° C. and a tensile elongation of 165%.

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Abstract

The invention discloses a Mo-Si-B-W multi-phase composite material, which is prepared with raw materials of the following atom percentages: 5-25 percent of silicon, 1-10 percent of tungsten, 5-30 percent of boron, and the resting being molybdenum. The mass purity of the silicon is no less than 98 percent, the mass purity of the tungsten is no less than 99 percent, the mass purity of the boron is no less than 99 percent, and the mass purity of the molybdenum is no less than 99 percent. The invention also discloses a preparation method of the Mo-Si-B-W multi-phase composite material. Mechanicalalloy and hot pressure sintering are adopted in the method to prepare the Mo-Si-B-W composite material, the method has the advantages of low energy consumption, short cycle and the like, and tungstenpowder is introduced into an Mo-Si-B composite material system so as to increase the high-temperature strength of the material and improve the reliability of the material in use. The composite material prepared in the method has a uniform and fine microstructure, the tensile strength of the composite material at 1400 DEG C is 400-460MPa, and the tensile elongation of the composite material is up to 400 percent.

Description

technical field [0001] The invention belongs to the technical field of composite materials, and in particular relates to a Mo-Si-B-W multiphase composite material and a preparation method thereof. Background technique [0002] The development of high-performance aircraft depends on the matching of advanced engines. Modern aerospace engines not only have high thrust, but also continuously improve the thrust-to-weight ratio. As engine thrust and efficiency increase, the turbine inlet temperature of the engine needs to be continuously increased. Among the turbine engine components, the working conditions of the turbine blades are the most severe. They must bear high stress in a high temperature and corrosive environment above 1000°C, and also require a long service life. This requires the turbine blade material to have high creep resistance. Good corrosion resistance, high high temperature durability, fracture toughness and fatigue properties, etc. The nickel-based and cobal...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C27/04C22C30/00C22C1/05C22C1/10
Inventor 喻吉良李中奎郑欣刘辉王晖王东辉张建军
Owner NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH
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