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Pigment printing imitated reactive printing adhesive and preparation method thereof

A pigment printing and imitation activity technology, which is applied in the direction of adhesive type, ester copolymer adhesive, dyeing method, etc., can solve the problems that the production technology has not been reported, and the synthesis technology of pigment imitation activity printing adhesive is not involved. , to achieve the effect of improving adhesion fastness, good performance, and improving softness

Active Publication Date: 2012-08-01
LIAONING FIXED STAR FINE CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The Chinese journal "Printing and Dyeing" Volume 022, 2005, the article "Production Practice of Imitation Reactive Printing of Wide-width Paint" introduced the specific operation process and precautions in the production of imitation reactive printing of wide-width paint. Production process control and corresponding imitation reactive printing products do not involve the synthesis technology of pigment imitation reactive printing adhesives, and the adhesive production technology dedicated to pigment imitation reactive printing products has not been reported yet

Method used

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  • Pigment printing imitated reactive printing adhesive and preparation method thereof
  • Pigment printing imitated reactive printing adhesive and preparation method thereof

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] Raw material ratio: fatty alcohol polyoxyethylene ether (Pingping plus O-25) 5 . 8 g, sodium dodecylbenzene sulfonate 0 . 35 grams, butyl acrylate 25 grams, dimethylaminopropylmethacrylamide 1 . 1 g glycidyl methacrylate 4 . 3 grams, isooctyl acrylate 77 grams, methyl methacrylate 12 . 2 g, acrylic acid 3 . 5 g, ammonium persulfate 0 . 64 g, sodium bisulfite 0 . 32 grams, 146 grams of deionized water;

[0032] Process method:

[0033] 1) Add 25 grams of butyl acrylate and 1 dimethylaminopropyl methacrylamide to all monomers . 1 g, glycidyl methacrylate 4 . 3 grams, 77 grams of isooctyl acrylate, 12 grams of methyl methacrylate . 2 grams, acrylic acid 3 . Add 5 grams into the mixing tank and stir well;

[0034] 2) Add 44 grams of deionized water, fatty alcohol polyoxyethylene ether (Pingping plus O-25) 2 into the reaction kettle . 9 g and sodium dodecylbenzene sulfonate 0 . 12 grams, fully stirred to dissolve;

[0035] 3) Dissolving 0.64 grams of ammonium p...

Embodiment 2

[0043] Raw material ratio: fatty alcohol polyoxyethylene ether (Pingping plus O-25) 5 . 6 g, sodium dodecylbenzene sulfonate 0 . 4 g, butyl acrylate 26 g, dimethylaminopropylmethacrylamide 1 . 3 g, glycidyl methacrylate 4 .9 grams, isooctyl acrylate 75 grams, methyl methacrylate 12 . 5 g, acrylic acid 4 g, ammonium persulfate 0 . 7 g, sodium bisulfite 0 . 35 grams, 148 grams of deionized water;

[0044] Process method:

[0045] 1) Mix all the monomers, namely 26 grams of butyl acrylate, 1 dimethylaminopropyl methacrylamide . 3 grams, glycidyl methacrylate 4 . 9 grams, isooctyl acrylate 75 grams, methyl methacrylate 12 . Add 5 grams of acrylic acid and 4 grams of acrylic acid into the mixing kettle and stir thoroughly;

[0046] 2) Add 46 grams of deionized water, fatty alcohol polyoxyethylene ether (Pingping plus O-25) 2 into the reaction kettle . 5 g and sodium dodecylbenzene sulfonate 0 . 2 grams, fully stirred to dissolve;

[0047] 3) Dissolve 0.7 grams of ammoni...

Embodiment 3

[0055] Raw material ratio: fatty alcohol polyoxyethylene ether (Pingping plus O-25) 5 . 1 g, sodium dodecylbenzenesulfonate 0 . 47 grams, butyl acrylate 28 grams, dimethylaminopropylmethacrylamide 1 . 4 g, glycidyl methacrylate 4 . 5 grams, isooctyl acrylate 76 grams, methyl methacrylate 12 . 8 grams, acrylic acid 4 . 3 g, ammonium persulfate 0 . 78 g, sodium bisulfite 0 . 39 grams, 150 grams of deionized water;

[0056] Process method:

[0057] 1) Mix all the monomers, 28 grams of butyl acrylate, 1 dimethylaminopropyl methacrylamide . 4 grams, glycidyl methacrylate 4 . 5 grams, isooctyl acrylate 76 grams, methyl methacrylate 12 . 8 grams, acrylic acid 4 . Add 3 grams into the mixing tank and stir thoroughly;

[0058] 2) Add 47 grams of deionized water, fatty alcohol polyoxyethylene ether (Pingping plus O-25) into the reaction kettle . 7 g and sodium dodecylbenzene sulfonate 0 . 16 grams, fully stirred to dissolve;

[0059] 3) Dissolving 0.78 grams of ammonium pe...

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Abstract

The invention relates to pigment printing imitated reactive printing adhesive and a preparation method thereof. The pigment printing imitated reactive printing adhesive is polymer emulsion prepared from fatty alcohol-polyoxyethylene ether (peregal O-25), sodium dodecyl benzene sulfonate, butyl acrylate, dimethyl aminopropyl methacrylamide, glycidyl methacrylate, iso-octyl acrylate, methyl methacrylate, acrylic acid, ammonium persulphate, sodium hydrogensulfite and deionized water through polymerization by using seeded emulsion. The pigment printing imitated reactive printing adhesive product has obvious advantages in indexes such as softness, rub fastness and fastness to washing, and quality of the pigment printing imitated reactive printing product can be obviously improved.

Description

technical field [0001] The invention relates to a pigment printing imitation reactive printing adhesive and a preparation method thereof, which is an emulsion of an acrylic polymer, and is especially suitable for the paint imitative reactive printing finishing of various fabrics in medium and light colors. Background technique [0002] Textile printing and finishing is a common textile finishing technology, including dye printing and pigment printing. Dye printing includes reactive dye printing, disperse dye printing, acid dye printing, etc. Reactive dye printing is also referred to as reactive printing. The main application In pure cotton or polyester-cotton fabric printing, reactive dyes can directly react with active groups on cotton fibers to achieve color fixation, so reactive dye printed fabrics are popular for their soft touch and bright colors. However, its production process includes multiple processes such as printing, steaming, desizing, washing and floating, and ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06P1/52C09J133/08C08F220/18C08F220/14C08F220/06C08F220/60C08F220/32C08F2/30C08F2/26
Inventor 孙继昌宋明智李秀颖王冠中
Owner LIAONING FIXED STAR FINE CHEM
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