Detection reagent for fast detecting cyanide in water and preparation method of detection reagent
A technology for detecting reagents and water, which is applied in the direction of material analysis by observing the influence of chemical indicators, and analysis by making materials undergo chemical reactions, which can solve the problems of inconvenient carrying and storage, small detection range, and high price. Achieve the effects of long shelf life, wide detection range, convenient carrying and storage of reagents
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Embodiment 1
[0040] A detection reagent for rapidly detecting cyanide in water, comprising a release reagent and a chromogenic reagent, the mass ratios of the components of the release reagent are respectively:
[0041] Potassium dihydrogen phosphate 0.52g;
[0042] Methylcellulose 0.03g;
[0043] Deionized water 2ml;
[0044] Lactic acid, acetone mixed solvent 2ml;
[0045] Chloramine T 0.02g;
[0046] The volume ratio of lactic acid and acetone in the mixed solvent of lactic acid and acetone is 1:9.
[0047] The preparation of described releasing reagent comprises the following steps:
[0048] (1) Mix and grind potassium dihydrogen phosphate 0.52g, methylcellulose 0.03g and 2ml deionized water evenly to make a paste;
[0049] (2) Transfer the paste prepared in step (1) to a watch glass, then place it in a vacuum drying oven, and dry it at 60°C for 2 hours;
[0050] (3) Take out the dried product in step (2) from the vacuum drying oven, cool it at room temperature for 10 minutes, an...
Embodiment 2
[0055] A detection reagent for rapidly detecting cyanide in water, comprising a release reagent and a chromogenic reagent, the mass ratios of the components of the release reagent are respectively:
[0056] Potassium dihydrogen phosphate 0.66g;
[0057] Methylcellulose 0.06g;
[0058]3ml deionized water;
[0059] Lactic acid, acetone mixed solvent 3ml;
[0060] Chloramine T 0.03g;
[0061] The volume ratio of lactic acid and acetone in the mixed solvent of lactic acid and acetone is 1:9.
[0062] The preparation of described releasing reagent comprises the following steps:
[0063] (1) Mix and grind 0.66g of potassium dihydrogen phosphate, 0.06g of methylcellulose and 3ml of deionized water to make a paste;
[0064] (2) Transfer the paste prepared in step (1) to a watch glass, then place it in a vacuum drying oven, and dry it at 90°C for 2 hours;
[0065] (3) Take out the dried product in step (2) from the vacuum drying oven, cool it at room temperature for 15 minutes, a...
Embodiment 3
[0070] A detection reagent for rapid detection of cyanide in water, comprising a release reagent and a chromogenic reagent, the mass ratios of the raw materials of the chromogenic reagent components are respectively:
[0072] Isonicotinic acid 1.7g;
[0073] Barbituric acid 0.8g;
[0074] Methylcellulose 0.2g;
[0075] 1ml of deionized water.
[0076] The preparation of described chromogenic reagent comprises the following steps:
[0077] (1) Add 0.8g of sodium hydroxide, 1.7g of isonicotinic acid, 0.8g of barbituric acid, and 0.2g of methylcellulose into a mortar, add 1ml of deionized water and grind them evenly. prepared paste;
[0078] (2) Transfer the paste prepared in step (1) to a watch glass, then place it in a vacuum drying oven, and dry it at 60°C for 2 hours;
[0079] (3) Take out the dried product in step (2) from the vacuum drying oven, cool it at room temperature for 10 minutes, and then place it in a mortar and grind it evenl...
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