Preparation method of foamless self-adhesive for KT board (foam board)
A technology of backing glue and rubber, which is applied in the field of preparation of non-foaming backing glue for KT boards, can solve problems such as insufficient adhesion of acrylate pressure-sensitive adhesives, achieve improved residual adhesion rate, excellent adhesion performance, and improve adhesion The effect of intensity
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Embodiment 1
[0056] Rubber / acrylate graft copolymer pressure-sensitive adhesives and non-polar group grafted acrylate pressure-sensitive adhesives are rolled to treat the release layer of the release paper as follows:
[0057] The synthesis process of rubber / acrylate graft copolymer pressure-sensitive adhesive is as follows: masticate natural rubber on an open mill, mix evenly and discharge the material, then use toluene to heat up and dissolve the mixed rubber cut into small pieces, and set aside ; Accurately weigh and dissolve 10 parts of vinyl acetate, 40 parts of ethyl acrylate, 1 part of methacrylic acid, 0.5 parts of dibenzoyl peroxide, 2 parts of propylene oxide, and 0.1 part of butyl titanate in 10 parts of ethyl acetate , mix evenly, and set aside; add the prepared rubber solution into the reactor, stir and heat up to the polymerization temperature of 50°C, take 1 / 5 of the above-mentioned mixed monomer with dibenzoyl peroxide added into the reactor Stir continuously, add the remai...
Embodiment 2
[0062] Rubber / acrylate graft copolymer pressure-sensitive adhesives and non-polar group grafted acrylate pressure-sensitive adhesives are rolled to treat the release layer of the release paper as follows:
[0063] The synthesis process of rubber / acrylate graft copolymer pressure-sensitive adhesive is as follows: masticate nitrile rubber on an open mill, then mix evenly and discharge the material, then use toluene to dissolve the mixed rubber cut into small pieces, Standby; Accurately weigh 10 parts of acrylamide, 40 parts of 2-ethylhexyl acrylate, 1 part of hydroxypropyl methacrylate, 0.5 parts of dibenzoyl peroxide, 3 parts of propylene oxide, and butyl titanate Dissolve 0.2 parts in 10 parts of toluene, mix well, and set aside; add the prepared rubber solution into the reactor, stir and heat up to the polymerization temperature of 50°C, take 1 / 5 was added to the reactor and stirred continuously, and after 1 hour, the remaining mixed monomers were added dropwise, and reacted...
Embodiment 3
[0068] Rubber / acrylate graft copolymer pressure-sensitive adhesives and non-polar group grafted acrylate pressure-sensitive adhesives are rolled to treat the release layer of the release paper as follows:
[0069] The synthesis process of rubber / acrylate graft copolymer pressure-sensitive adhesive is as follows: masticate styrene-butadiene rubber on an open mill, and then mix evenly before discharging, and then use toluene to heat up and dissolve the mixed rubber cut into small pieces. Standby; accurately weigh 30 parts of acrylonitrile, 60 parts of butyl acrylate, 5 parts of acrylic acid, 6 parts of dibenzoyl peroxide, 5 parts of propylene oxide, and 0.3 parts of butyl titanate in 30 parts of toluene, mix Uniform, ready for use; add the prepared rubber solution into the reactor, stir and heat up to the polymerization temperature of 100°C, take 4 / 5 of the above-mentioned mixed monomer with dibenzoyl peroxide added into the reactor and keep stirring, After 3 hours, add the rema...
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