Method for synthesizing nano flower-shaped spherical In2Se3 diethylenetriamine (DETA) hybrid material by means of solvothermal
A hybrid material and solvothermal technology, applied in chemical instruments and methods, nanotechnology, nanotechnology, etc., can solve the problems of rarely reported indium selenide hybrid materials, and achieve high yield, strong controllability, Simple to use effects
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0017] (1) Use an electronic balance to weigh 0.0764g (0.2mmol) indium nitrate hydrate and 0.0237g (0.3mmol) selenium powder respectively in a 25ml reaction kettle lined with polytetrafluoroethylene;
[0018] (2) Use a 10ml pipette to accurately measure 11ml of diethylenetriamine twice, and use a 5ml pipette to accurately measure 4ml of ethylene glycol into the reaction kettle in (1). At this time, the volume of the solution is the volume of the reaction kettle 60%, using a magnet with a diameter of 1cm to stir for 10min at 600rpm;
[0019] (3) Seal the reaction kettle, put it in an oven at 160°C for 12 hours, cool it down to room temperature naturally, wash it with absolute ethanol for 6 times, and dry it in a vacuum oven at 60°C for 6 hours to obtain yellow In 2 Se 3 (DETA) powder.
[0020] figure 1 is the prepared nanoflower spherical In 2 Se 3 XRD patterns of (DETA) hybrid materials;
[0021] figure 2 is the prepared nanoflower spherical In 2 Se 3 The low-magnif...
Embodiment 2
[0024] (1) Use an electronic balance to weigh 0.0442g (0.2mmol) indium chloride and 0.0237g (0.3mmol) selenium powder in a 25ml reactor lined with polytetrafluoroethylene;
[0025] (2) Use a 10ml pipette to accurately measure 11ml of diethylenetriamine twice, and use a 5ml pipette to accurately measure 4ml of ethylene glycol into the reaction kettle in (1). At this time, the volume of the solution is the volume of the reaction kettle 60%, using a magnet with a diameter of 1cm to stir for 10min at 600rpm;
[0026] (3) Seal the reaction kettle, put it in an oven at 160°C for 12 hours, cool it down to room temperature naturally, wash it with absolute ethanol for 6 times, and dry it in a vacuum oven at 60°C for 6 hours to obtain yellow In 2 Se 3 (DETA) powder.
Embodiment 3
[0028] (1) Use an electronic balance to weigh 0.071g (0.2mmol) indium bromide and 0.0237g (0.3mmol) selenium powder in a 25ml reactor lined with polytetrafluoroethylene;
[0029] (2) Use a 10ml pipette to accurately measure 11ml of diethylenetriamine twice, and use a 5ml pipette to accurately measure 4ml of ethylene glycol into the reaction kettle in (1). At this time, the volume of the solution is the volume of the reaction kettle 60%, using a magnet with a diameter of 1cm to stir for 10min at 600rpm;
[0030] (3) Seal the reaction kettle, put it in an oven at 160°C for 12 hours, cool it down to room temperature naturally, wash it with absolute ethanol for 6 times, and dry it in a vacuum oven at 60°C for 6 hours to obtain yellow In 2 Se 3 (DETA) powder.
PUM
Property | Measurement | Unit |
---|---|---|
diameter | aaaaa | aaaaa |
thickness | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com