Preparation method for colored glass beads

A technology of colored glass and glass beads, applied in glass manufacturing equipment, glass molding, glass production, etc., can solve the problems of unsatisfactory process, high production cost, unstable color, etc., and achieve excellent decorative effect and production Cost reduction, good coloring effect

Inactive Publication Date: 2013-01-30
SHAANXI UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, industrial production uses colorless and transparent glass beads, which have a single color and poor decorative effect.
Most of the preparation of colored glass beads is to prepare colored glass powder first, and then pr

Method used

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  • Preparation method for colored glass beads

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] Embodiment 1, the first step: the preparation of matrix glass microspheres

[0028] 1) First, 68.5% SiO 2 , 9% CaO, 16% Na 2 O, 2% K 2 O, 2% Al 2 o 3 , 2% ZnO and 0.5% Sb 2 o 3 After the powder is mixed evenly, a batch material is formed;

[0029] The SiO 2 Introduced through quartz sand, the purity is 99.9%, the particle size is 150 mesh, CaO, Na 2 O, K 2 O, Al 2 o 3 , ZnO, Sb 2 o 3 They are respectively introduced by analytically pure calcium carbonate, sodium carbonate, potassium carbonate, aluminum hydroxide, zinc oxide, and antimony trioxide;

[0030]2) It will add half of the batch materials into the corundum crucible that has been heated to 1300 °C; then, heat up to 1450 °C in 10 minutes and keep it warm for 20 minutes; then add the remaining batch materials into the corundum crucible and heat up to 10 minutes 1400°C, after 60 minutes of heat preservation, pour the melted glass into water and quench it;

[0031] 3) Then, fish out the glass slag aft...

Embodiment 2

[0042] Embodiment 2, the first step: the preparation of matrix glass microsphere

[0043] 1) First, 63% SiO 2 , 9% CaO, 18% Na 2 O, 3% K 2 O, 3% Al 2 o 3 , 3% ZnO and 31% Sb 2 o 3 After the powder is mixed evenly, a batch material is formed;

[0044] The SiO 2 Introduced through quartz sand, the purity is 99.9%, the particle size is 150 mesh, CaO, Na 2 O, K 2 O, Al 2 o 3 , ZnO, Sb 2 o 3 They are respectively introduced by analytically pure calcium carbonate, sodium carbonate, potassium carbonate, aluminum hydroxide, zinc oxide, and antimony trioxide;

[0045] 2) It will add half of the batch materials into the corundum crucible that has been heated to 1300 °C; then, heat up to 1450 °C in 10 minutes and keep it warm for 20 minutes; then add the remaining batch materials into the corundum crucible and heat up to 10 minutes 1420°C, after holding for 60 minutes, pour the molten glass into water and quench it;

[0046] 3) Then, fish out the glass slag after water que...

Embodiment 3

[0056] Embodiment 3, the first step: the preparation of matrix glass microsphere

[0057] 1) First, mix 70% SiO by mass fraction 2 , 5% CaO, 15% Na 2 O, 3% K 2 O, 3% Al 2 o 3 , 3% ZnO and 1% Sb 2 o 3 After the powder is mixed evenly, a batch material is formed;

[0058] The SiO 2 Introduced through quartz sand, the purity is 99.9%, the particle size is 150 mesh, CaO, Na 2 O, K 2 O, Al 2 o 3 , ZnO, Sb 2 o 3 They are respectively introduced by analytically pure calcium carbonate, sodium carbonate, potassium carbonate, aluminum hydroxide, zinc oxide, and antimony trioxide;

[0059] 2) It will add half of the batch materials into the corundum crucible that has been heated to 1300 °C; then, heat up to 1450 °C in 10 minutes and keep it warm for 20 minutes; then add the remaining batch materials into the corundum crucible and heat up to 10 minutes 1410°C, after 60 minutes of heat preservation, pour the melted glass into water and quench it;

[0060] 3) Then, fish out t...

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Abstract

The invention provides a preparation method for colored glass beads; and the preparation method comprises the following steps of: after uniformly mixing SiO2 powder, CaO powder, Na2O powder, K2O powder, Al2O3 powder, ZnO powder and Sb2O3 powder, forming a batch material; pouring a glass liquid after the batch material is melted into water, quenching the glass liquid in the water; grinding water-quenched glass fragments to a particle size of 10-200 microns; and then nodulizing the ground glass fragments in a bead forming furnace, so as to obtain a parent glass bead; pouring water, glycerol and dextrin into a beaker; after uniformly mixing the water, the glycerol and the dextrin, adding a mixture to a mixture of AgNO3, CuCl, Cu2O, SnO, FeSO4.7H2O, zinc powder and pulverized coal; uniformly mixing the two mixtures; and ball-milling the mixtures so as to obtain a coloring ion diffusion slurry for a colored glass bead; and mixing the parent glass bead and the coloring ion diffusion slurry so as to form a mixed material; pouring the mixed material into a stainless steel mold; heating the stainless steel mold to 550-650 DEG C; preserving the heat of the stainless steel mold for 5-10 minutes; and cooling the stainless steel mold so as to obtain ion diffused and colored glass bead. According to the invention, defects of single color, instable color, high production cost and the like in the traditional preparation method are avoided.

Description

technical field [0001] The invention relates to a method for preparing glass microspheres, in particular to a method for preparing colored glass microspheres. Background technique [0002] Glass beads are a new type of material developed in recent years with wide applications and special properties. The product is processed from silicate raw materials, with a particle size of 10-250 microns. The product has the advantages of light weight, low thermal conductivity, high strength, and good chemical stability. Its surface has been specially treated to have lipophilic and hydrophobic properties, and it is very easy to disperse in organic material systems. Glass beads have been widely used in the derusting of aerospace machinery, in the night reflective devices of zebra crossings, no-stop lines, and double yellow lines in urban traffic roads, and in the night reflective devices of traffic signs. [0003] At present, the preparation methods of glass microspheres mainly include: ...

Claims

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Application Information

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IPC IPC(8): C03B19/10C03C12/00
CPCY02P40/57
Inventor 郭宏伟王顺逆刘盼高档妮
Owner SHAANXI UNIV OF SCI & TECH
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