Microwave dielectric ceramic and preparation method thereof
A microwave dielectric ceramic and a new technology, applied in the field of microwave dielectric ceramics, can solve the problems of difficult large-scale production, damage to the performance of ceramic materials, and density of volatile materials.
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Embodiment 1
[0034] Weigh the raw materials according to the molecular formula of the formula: the molecular formula is K 0.5 Dy 4.5 Ti 4 o 15 , the molecular weight is 1182.3902, the mass of ingredients is 118.2390 g, and the molar number of ingredients is 0.10;
[0035] Weigh the required raw material K 2 CO 3 Mass is 3.490 g; Dy 2 o 3 Mass is 84.216 g, TiO 2 The amount is 36.227 g.
[0036] The preparation method is:
[0037] (1) Put the weighed raw materials into a ball mill jar and mill for 4-48 hours, then put them in a dry box at 80-180 o Tumble dry at C.
[0038] (2) The obtained mixed powder is pre-fired at high temperature to obtain superfine powder. It needs to be heated for 16 hours during pre-burning, and the required temperature is 1100 o C, keep warm for 4 hours.
[0039] (3) After grinding and sieving, add the prepared polyvinyl alcohol glue to the powder, the amount of polyvinyl alcohol added is 10% of the total mass of the raw material design; after pre-pressi...
Embodiment 2
[0041] According to the general formula, the raw materials potassium carbonate, titanium dioxide and holmium oxide were weighed.
[0042] Molecular formula is K 0.5 Ho 4.5 Ti 4 o 15 , the molecular weight is 1193.19, the mass of ingredients is 119.319 g, and the molar number of ingredients is 0.10mol;
[0043] The preparation method is:
[0044] (1) Weigh the required raw material K 2 CO 3 Mass is 3.490 g; Ho 2 o 3 Mass is 85.061 g, TiO 2 The amount is 36.227 g.
[0045] (2) Put the weighed raw materials into a ball mill jar for ball milling for 48 hours, and then put them in a drying oven at 180 o Tumble dry at C.
[0046] (3) The obtained mixed powder is pre-fired at high temperature to obtain superfine powder. During pre-burning, the temperature needs to be raised for 20 hours, and the temperature is raised to the required temperature of 900 o After C, keep warm for 5 hours.
[0047] (4) After grinding and sieving, add the prepared polyvinyl alcohol glue to th...
Embodiment 3
[0049] Weigh the raw materials potassium carbonate, titanium dioxide and erbium oxide according to the general formula.
[0050] Molecular formula is K 0.5 Er 4.5 Ti 4 o 15 , the molecular weight is 1203.8102, the mass of ingredients is 120.3810 g, and the molar number of ingredients is 0.10mol;
[0051] The preparation method is:
[0052] (1) Weigh the required raw material K 2 CO 3 Mass is 3.490 g; Er 2 o 3 Mass is 86.076 g, TiO 2 The amount is 36.227 g.
[0053] (2) Put the weighed raw materials into a ball mill jar and mill them for 4 hours.
[0054] (3) The raw materials after ball milling are placed in a drying oven at 180 o C drying, after drying, pulverization, pre-calcination, grinding, and sieving to obtain powder materials; the obtained mixed powder is pre-calcined at high temperature to obtain ultra-fine powder materials. During pre-calcination, the temperature needs to be raised for 12 hours, and the temperature is raised to 1200 °C. o After C, keep wa...
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