High molecular synthetic cement grinding aid
A technology for synthesizing cement and grinding aids, which is applied in the field of polymer synthetic cement grinding aids. It can solve the problems of unsatisfactory grinding aids, failure to enhance the strength of cement in the later stage, and endanger the performance of concrete, so as to achieve good development and application prospects and stable coagulation. Hardening time, the effect of improving the utilization rate of waste residue
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Embodiment 1
[0027] 1. Raw material preparation: 55 parts of allyl polyether, 5 parts of sodium methacrylic acid sulfonate, 15 parts of methacrylic acid, 7 parts of acrylamide, 15 parts of self-provided polymeric polyol and 3 parts of initiator ammonium persulfate.
[0028] 2. Polymerized polyol preparation: Mix 3 parts of ethylene glycol, 3 parts of diethylene glycol, 2 parts of triglycerin and 2 parts of sodium fatty acid to obtain a mixed liquid that is a mixed polyol.
[0029] 3. Connect the external device of the pressure reactor, add allyl polyether, sodium methacrylate and acrylamide in proportion to the reactor, heat and stir in a water bath, control the temperature to about 70°C until completely dissolved, and then Add methacrylic acid, polymer polyol and initiator ammonium persulfate dropwise in sequence, and the dropping time is controlled within 2 to 3 hours; after dropping, keep warm for 3 hours, cool to room temperature and add water twice the weight of the product to dilute t...
Embodiment 2
[0031] 1. Raw material preparation: 60 parts of allyl polyether, 5 parts of sodium methacrylate, 10 parts of methacrylic acid, 5 parts of acrylamide, 15 parts of self-provided polymeric polyol and 5 parts of initiator ammonium persulfate.
[0032] 2. Polymerized polyol preparation: Mix 3 parts of ethylene glycol, 3 parts of diethylene glycol, 2 parts of triglycerin and 2 parts of sodium fatty acid to obtain a mixed liquid that is a mixed polyol.
[0033] 3. Connect the external device of the pressure reactor, add allyl polyether, sodium methacrylate and acrylamide in proportion to the reactor, heat and stir in a water bath, control the temperature to about 70°C until completely dissolved, and then Add methacrylic acid, polymer polyol and initiator ammonium persulfate dropwise in sequence, and the dropping time is controlled within 2 to 3 hours; after dropping, keep warm for 3 hours, cool to room temperature and add water twice the weight of the product to dilute to obtain Prod...
Embodiment 3
[0035] 1. Raw material preparation: 50 parts of allyl polyether, 10 parts of sodium methacrylic acid sulfonate, 10 parts of methacrylic acid, 6 parts of acrylamide, 10 parts of self-provided polymeric polyol and 4 parts of initiator ammonium persulfate.
[0036] 2. Polymerized polyol preparation: Mix 3 parts of ethylene glycol, 3 parts of diethylene glycol, 2 parts of triglycerin and 2 parts of sodium fatty acid to obtain a mixed liquid that is a mixed polyol.
[0037] 3. Connect the external device of the pressure reactor, add allyl polyether, sodium methacrylate and acrylamide in proportion to the reactor, heat and stir in a water bath, control the temperature to about 70°C until completely dissolved, and then Add methacrylic acid, polymerized polyols and initiator ammonium persulfate dropwise in sequence, and the dropping time is controlled within 2 to 3 hours; after dropping, keep warm for 3 hours, cool to room temperature and add 2 times the weight of the product to dilute...
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