Preparation method of hydrocracking catalyst
A hydrocracking and catalyst technology, applied in physical/chemical process catalysts, molecular sieve catalysts, chemical instruments and methods, etc., can solve the problems of limited metal content in the preparation of catalysts, low effective utilization of active metals, and limited catalyst pore structure, etc. Achieve the effect of weakening capillary resistance, reducing pore size and specific surface area, and stable properties
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0036] Taking the tungsten-nickel system as an example, the preparation of the catalyst is carried out.
[0037] Prepare a metal impregnation solution, in which the concentration of metal is 25.6g metal (calculated as oxide) / 100mL solution, the concentration of ammonium citrate is 4g / 100mL solution, the impregnation temperature is 30°C, and the liquid-solid ratio is 6mL solution / g powder, Immerse the mixed powder of 66 grams of silicon-modified alumina and 200 grams of Y-1 molecular sieve for 2.5 hours, and dry at 120°C for 8 hours, and pulverize into 180 meshes to obtain a mixed material containing metal components (dry base is 76.6wt%).
[0038] Take 370 grams of the above-mentioned metal-containing component mixture and 259 grams of binder (5.8wt% on a dry basis, the molar ratio of nitric acid to small-pore alumina is 0.5) and put them into a roller compactor for mixing and rolling to form a paste. Extrude into a cylinder with a diameter of 1.8 mm. After drying at 120°C f...
Embodiment 2
[0040] Taking the tungsten-nickel system as an example, the preparation of the catalyst is carried out.
[0041] Prepare a metal impregnation solution, in which the metal concentration is 25.6g metal (calculated as oxide) / 100mL solution, the ammonium citrate concentration is 6g / 100mL solution, the immersion temperature is 30°C, and the liquid-solid ratio is 6mL solution / g powder, Immerse the mixed powder of 66 grams of silicon-modified alumina and 200 grams of Y-2 molecular sieves for 2.5 hours, and dry at 120°C for 8 hours, and pulverize into 180 meshes to obtain a mixed material containing metal components (dry base is 76.6wt%).
[0042] Take 370 grams of the above-mentioned metal-containing component mixture and 259 grams of binder (5.8wt% on a dry basis, the molar ratio of nitric acid to small-pore alumina is 0.5) and put them into a roller compactor for mixing and rolling to form a paste. Extrude into a cylinder with a diameter of 1.8 mm. After drying at 120°C for 5 hou...
Embodiment 3
[0044] Taking the tungsten-nickel system as an example, the preparation of the catalyst is carried out.
[0045] Prepare a metal impregnation solution, wherein the metal concentration is 27.2g metal (calculated as oxide) / 100mL solution, the ammonium citrate concentration is 8g / 100mL solution, the immersion temperature is 40°C, and the liquid-solid ratio is 8mL solution / g powder, Immerse the mixed powder of 133 grams of silicon-modified alumina and 134 grams of Y-1 molecular sieves for 4 hours, and dry at 120°C for 8 hours, and pulverize into 180 meshes to obtain a mixed material containing metal components (dry base is 75.1wt%).
[0046] Take 380 grams of the above-mentioned metal-containing component mixture and 259 grams of binder (5.8wt% on a dry basis, the molar ratio of nitric acid to small-pore alumina is 0.5) and put them into a roller compactor for mixing and grinding to form a paste. Extrude into a cylinder with a diameter of 1.8 mm. After drying at 120°C for 5 hour...
PUM
Property | Measurement | Unit |
---|---|---|
specific surface area | aaaaa | aaaaa |
specific surface area | aaaaa | aaaaa |
specific surface area | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com