Extracting method of D-xylose and L-arabinose
An extraction method, the technology of arabinose, applied in the field of functional sugar preparation, can solve the problems of reducing the crystallization yield of D-xylose, high water consumption and resin consumption, and long hydrolysis cycle, so as to improve the quality and crystallization yield, equipment The effect of reduced investment and short cycle
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Embodiment 1
[0026] (1) Take 200g of corn cobs with a size of about 1 cm square, put them into a 2L beaker, add 1500ml of oxalic acid 0.9% by weight, soak at room temperature for 17 hours, and separate the corn cobs from the acid solution with a filter bag , the water content of the obtained acidified corn cob is about 46% of its dry weight, and the separated acid solution can be reused;
[0027] (2) Put the obtained acidified corncobs into the prepared intermittent steam explosion equipment, boost the steam pressure to 1.2Mpa, keep the pressure for 5 minutes, open the discharge solenoid valve, and discharge the material steam explosion by the high pressure inside the system;
[0028] (3) Add water equivalent to 10 times its dry weight to the obtained steam-exploded corncob mud, stir at 80°C for 60 minutes, and obtain 1820ml of extract by suction filtration; put the obtained filter residue into a beaker, and then add equivalent Carry out secondary extraction in the water of 5 times of ...
Embodiment 2
[0031] (1) Take 200g of ground bagasse, put it into a 2L beaker, add 1500ml of sulfuric acid 0.1% by weight, soak it at 70°C for 0.3h, and separate the corn cob from the acid solution with a filter bag to obtain The water content of acidified bagasse is about 40% of its dry weight, and the separated acid can be reused;
[0032] (2) Put the obtained acidified bagasse into the prepared intermittent steam explosion equipment, boost the steam pressure to 0.6Mpa, keep the pressure for 20 minutes, open the discharge solenoid valve, and discharge the material steam explosion by the high pressure inside the system;
[0033] (3) Add water equivalent to 15 times its dry weight to the obtained steam-exploded bagasse mud, stir and extract at 80°C for 20 minutes, and obtain 1460ml of extract by suction filtration; put the obtained filter residue into a beaker, and then Add water equivalent to 3 times its dry weight for secondary extraction. During continuous production, this extraction...
Embodiment 3
[0036] (1) Take 200g of cane pith, put it into a 2L beaker, add 1500ml of sulfuric acid 1.0% by weight, soak it at 20°C for 20h, separate the cane pith from the acid solution with a filter bag, and obtain the acidified cane pith The water content is about 80% of its dry weight, and the separated acid can be reused;
[0037] (2) Put the obtained acidified cane pith into the prepared intermittent steam explosion equipment, boost the steam pressure to 0.6Mpa, keep the pressure for 3 minutes, open the discharge solenoid valve, and discharge the material by steam explosion by the high pressure inside the system;
[0038] (3) Add water equivalent to 5 times its dry weight to the obtained steam-exploded sugarcane pith mud, stir and extract at 20°C for 80 minutes, and obtain 1000ml of extract by suction filtration; put the obtained filter residue into a beaker, and then Add water equivalent to 6 times its dry weight for secondary extraction. During continuous production, this extr...
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