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228results about How to "Reduce acid content" patented technology

Method for deacidification of alkylation reaction product

The invention relates to a method for deacidification of an alkylation reaction product. In the method, after being subject to gravity settling, mixed emulsified liquid of the alkylation reaction product (hydrocarbon oil) and sulfuric acid passes through a component with hydrophobic modified ceramic membrane at a membrane surface speed of 0.01-5m/s for separation, and the deacidification of oil is achieved in a cross current filtration mode under the operation pressure of 0.01-0.3MPa and at the operation temperature of 0-40 DEG C. Under the push of pressure, the oil passes through the ceramic membrane, acid in the oil is trapped, and the acid content in the obtained oil is lower than 100ppm, thereby greatly reducing alkaline usage and waste water generation amount in an acid-base refine system of an alkylation technology and reducing the use of electrostatic precipitation; and the ceramic membrane surface is subject to hydrophobic modification, thus the contact angle of water droplet on the membrane surface is 70 degrees-16 degrees. The method is suitable for removal of polar liquid in various oils, has the advantages of simple process, low energy consumption, high separation precision, no environment pollution and high economic and practical value, and is easy to achieve industrial application.
Owner:NANJING UNIV OF TECH

Method for preparing hawthorn fruit vinegar

The invention relates to a method for preparing hawthorn fruit vinegar, which comprises the following steps: extracting hawthorn juice containing rich biological effective constituent flavone by an enzymatic method extracting process; deacidifying the hawthorn juice by weakly basic anion exchange resin; adding wine active dried yeast into the deacidified hawthorn juice to ferment at low temperature so as to brew hawthorn wine; and further brewing the hawthorn wine into the hawthorn fruit vinegar by an acetic acid bacterium deep liquid fermentation method. Ecipients, such as malt-dextrin, lactose, and the like are added into a by-product after hawthorn processing to be mixed, stirred, granulated, dried, tabletted, classified and packaged to be capable of obtaining a hawthorn fiber sheet. The invention adopts a full juice low-temperature second deep liquid fermentation method, improves a comprehensive development industrial chain of the hawthorn, realizes no pollution production, and provides an effective path for enriching the deep processing and the comprehensive utilization of high-quality hawthorn resources, not only can enrich the variety of juice beverage and meet the market requirement but also can directly protect and simulate the development of forest fruit and improve an additional value of a product.
Owner:TIANJIN UNIV OF SCI & TECH

Organic and inorganic biological compound fertilizer and preparation method

The invention discloses an organic and inorganic biological compound fertilizer and a preparation method. The organic and inorganic biological compound fertilizer consists of a nitrogen fertilizer, a phosphatic fertilizer, a potassic fertilizer, chicken manure and vinasse fermented fertilizer, an adsorbent, an enveloping agent and a bioremediating inoculant. Organic matters, inorganic nutrition and functional microorganisms are processed and mixed according to own different functional effects through specific equipment and a technology; after being applied, the three fertilizers jointly generate action and cannot influence the effect; the synergism and the effect improving effect of the biological fertilizer, the stable and long-time effect of the inorganic fertilizer and the quick-acting effect of the inorganic fertilizer are combined with one another; and the organic and inorganic biological compound fertilizer has the characteristics of urgent and delayed supplementation, advantage complementation, comprehensive nutrition, durable balance, high efficiency and the like. The same-fertilizer-price comprehensive experiment result shows that the yield of food crops is increased by 9-14 percent when being compared with the common compound fertilizer; the yield of economical crops is increased by 12-30 percent.
Owner:SINO AGRI SHUNTIAN ECOLOGICAL FERTILIZER CO LTD

Process for reducing the naphthenic acidity of petroleum oils or their fractions

A process for reducing the naphthenic acidity of petroleum oils or their fractions is described, said process comprising providing a hydrocarbon feed 103/203/303 having between 0.1 and 99 wt % of emulsified/dispersed water in oil, said feed containing salts and a content of naphthenic acids measured as TAN between 0.1 and 10 mg KOH/g oil; directing the said petroleum oil feed and emulsified/dispersed water towards an energy emitter device in the microwave range and submitting said feed 103/203/303 in liquid phase, under pressure between 0.7 and 4.5 MPa at temperatures between 50° C. and 350° C. to the microwave radiation, applied in the range of 1 mm to 30 cm to said feed so that the presence of salts, the applied temperature and the high dielectric constant of the water droplets make that the heat is absorbed on the spot by the water and heat said water preferentially to the oil, while the naphthenic compounds at the interface between the droplets and the oil catch said heat; effecting the decomposition of the carboxylic acids responsible for the naphthenic acidity in the petroleum feed at temperatures around 320° C. and generating CO2; separating with the aid of any known device 106/106′/112/117/208/208′/214/219/310/310′/316/321 any gas phase generated, water and oil; and recovering the hydrocarbon oil stream 108/113/119/210/215/221/312/317/323 having a reduced content in naphthenic acids. The process is designed to be applied to the reduction of naphthenic acids in feeds of petroleum oils and their fractions in the oil production step, in refineries or any industrial installation.
Owner:PETROLEO BRASILEIRO SA (PETROBRAS)

Clean technology for producing D-xylose with screw pressure producing flashing spray explosion method

The invention belongs to the field of biochemical engineering and relates to a clean technology for producing D-xylose with a screw pressure producing flashing spray explosion method. According to the clean technology, pretreatment is performed on wood fiber raw materials at first, then, a traditional sulfuric acid hydrolysis technology is replaced by the screw pressure producing flashing spray explosion technology to produce spray explosion materials rich in the D-xylose, feed liquid of the D-xylose is extracted through filter-press dehydration in a high concentration mode, therefore, subsequent decoloration, ion exchange, concentration, crystal separation technological processes are improved according to the characteristics of the feed liquid, and D-xylose products are obtained finally. Compared with a traditional sulfuric acid hydrolysis technology, the clean technology has the advantages of being capable of achieving continuous production, small in acid-base dosage, small in waste water discharge amount and low in energy consumption and cost. The obtained feed liquid is high in concentration of the D-xylose and extremely low in acid content, the complicated neutralization process of the technology can be removed, meanwhile, the decoloration, concentration and ion exchange technological processes are simplified, and the burdens in later-stage purification processing are greatly reduced. The clean technology for producing the D-xylose with the screw pressure producing flashing spray explosion method is simple, simple in industrial production, and capable of greatly improving the quality and the yield of D-xylose products.
Owner:BEIJING UNIV OF CHEM TECH

High-temperature proton exchange membrane fuel cell membrane electrode and preparation method thereof

The invention provides a high-temperature proton exchange membrane fuel cell membrane electrode, which an acid-doped high-temperature proton exchange membrane and acid-doped gas diffusion electrodes, wherein the acid-doped gas diffusion electrodes are arranged at two sides of the acid-doped high-temperature proton exchange membrane; the mass percentage of the acid doping amount in the high-temperature proton exchange membrane is 150-200wt.%; the acid doping amount of the unit electrode area in the gas diffusion electrodes is 1-10mg / cm<2>; and the preparation method of the high-temperature proton exchange membrane fuel cell membrane electrode comprises the following steps: carrying out acid soaking treatment and aftertreatment of the membrane to constant weight; uniformly arranging the acid-doped solution on the surface of each gas diffusion electrode and removing a solvent through vacuum drying; and carrying out hot-pressing and cooling on the acid-treated gas diffusion electrodes and the acid-doped membrane and then obtaining the high-temperature proton exchange membrane fuel cell membrane electrode. According to the method, the problem of the uncertainty of the effective acid doping amount in the proton exchange membrane can be effectively solved; and the membrane electrode preparation consistency is ensured.
Owner:DALIAN INST OF CHEM PHYSICS CHINESE ACAD OF SCI

Oil well acidification process and device for increasing oil-gas well yield

The invention discloses an oil well acidification process and device for increasing oil-gas well yield. The oil well acidification device comprises an acid liquid tank and a waste liquid tank, whereina stirring tank is arranged in the acid liquid tank, a stirring device is arranged in the stirring tank, an acidification pipe column penetrates through a wellhead device and then extends into the bottom of a casing pipe, a nozzle is arranged at the bottom of the acidification pipe column, and pulse supercharging devices are arranged on the two sides of the acidification pipe column above the nozzle; and the waste liquid tank is connected with a liquid outlet of the wellhead device. The acidification process comprises the following steps that S1, acidification pretreatment is conducted; S2, preposed acid liquid is injected; S3, reaction acid liquid is injected; and S4, a neutralizer is injected in a pulse pressurization mode, so that the acid liquid enters an oil layer in a fluctuation mode, the swept area is enlarged, the injection effect of the acid liquid is effectively enhanced, residual acid liquid is neutralized in sections at the bottom of a well, the content of the acid liquidin flowback fluid is reduced, components of preposed acid liquid, reaction acid liquid and the neutralizer are optimized, the problem of oil layer blockage can be effectively solved, and the purposeof increasing the yield is achieved.
Owner:西安石油大油气科技有限公司
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