The present application belongs to the field of
dimethyldichlorosilane concentrated
acid hydrolysis reaction in the organic
silicon industry, and particularly relates to a
dimethyldichlorosilane concentrated acid two-stage
hydrolysis reaction process. The process comprises the following specific steps:
dimethyldichlorosilane is subjected to a first-stage
hydrolysis reaction with recycled saturated
hydrochloric acid and water, and an additive is added; purification and
drying are performed, and the purified
siloxane is subjected to a second-stage reaction in a second-stage reactor; after the second-stage reaction is completed, the mixture is subjected to oil-water separation, and the hydrolyzate is subjected to a washing section to obtain a final product. The dimethyldichlorosilane provided by the present application is subjected to two-stage
hydrolysis reaction, the content of
chlorine-terminated groups in the generated hydrolyzate is greatly reduced, the
acid content is low, and the quality of the hydrolysis product is high. The new process provided by the present application adopts a two-stage
reaction system, solves the problems of high
chlorine-terminated group content,
hydrogen chloride gas containing dimethyl and hydrolyzate, and obtains high-quality hydrolyzate, and the
reaction system maintains a slight
positive pressure, which does not inhibit the dimethyl hydrolysis reaction.