Inorganic cured foam material for surface leaking stoppage of shallow buried coal seam mining area and preparation method of inorganic cured foam material

A technology of inorganic curing and foam materials, which is applied in ceramic products, solid waste management, sustainable waste treatment, etc. The effect of high temperature and thermal insulation performance, adjustable setting time and wide applicability

Inactive Publication Date: 2013-11-20
CHINA UNIV OF MINING & TECH +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, these technologies have some shortcomings: large-area surface backfilling can only initially fill up the obvious large cracks, which consumes a lot of manpower and material resources; during the grouting process, the grout leaks along the cracks to the underground working face and roadway, and the effect is poor; ammonium salt gel At room temperature, it will decompose and produce ammonia gas, which seriously pollutes the environment of mining areas; polymer gels are expensive and easy to crack; polyurethane foam is easy to burn at high temperatures and high in cost; light paste materials have general compressive strength and are easy to Small cracks are generated; high water sealing materials have good permeability and can penetrate deep into the coal gap, but the compressive strength is not high, and the thermal stability of organic components is poor

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0012] Embodiment 1: first add 35 parts by weight of water, 100 parts by weight of fly ash, 20 parts by weight of cement, 0.8 parts by weight of hydroxypropyl methylcellulose, 3 parts by weight of steel fiber, and 5 parts by weight of slaked lime in the special mixing container A , the stirrer rotates at a speed of 5000±200 rpm, and the stirring time is 2min to form a fly ash substrate slurry; then add 5 parts of water and 0.15 parts by weight of ox horn powder to the special mixing container B, and the stirrer rotates at a speed of 10000±500 Rev / min rotating speed rotates, stirring time is 3min, forms mucus; Then, the ox horn powder mucus in the special mixing vessel B is added in the fly ash base material slurry in the special mixing vessel A, and the special mixing vessel A stirrer is with 12000± Rotate at a speed of 500 rev / min, and the stirring time is 3min to form a mixed liquid; then, a mixture of 1 weight part of copper oxide prepared in proportion, 0.4 weight part of p...

Embodiment 2

[0013] Embodiment 2: First, add 50 parts by weight of water, 100 parts by weight of fly ash, 20 parts by weight of cement, 1.0 parts by weight of hydroxypropyl methylcellulose, 3 parts by weight of steel fiber, and 5 parts by weight of slaked lime in the special mixing container A , the agitator rotates at a speed of 5000±200 rpm, and the stirring time is 2min to form a fly ash substrate slurry; then add 5 parts of water and 0.25 parts by weight of ox horn powder to the special mixing container B, and the agitator rotates at a speed of 10000±500 Rev / min rotating speed rotates, stirring time is 3min, forms mucus; Then, the ox horn powder mucus in the special mixing vessel B is added in the fly ash base material slurry in the special mixing vessel A, and the special mixing vessel A agitator beats at 12000± Rotate at a speed of 500 rpm / min, and the stirring time is 3min to form a mixed solution; then, a mixture of 2 parts by weight of copper oxide, 0.8 parts by weight of polyphosp...

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PUM

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Abstract

The invention discloses an inorganic cured foam material for surface leaking stoppage of a shallow buried coal seam mining area and a preparation method of the inorganic cured foam material, which belong to the inorganic cured foam material and the preparation method thereof. The leaking-stoppage cured foam comprises water, coal ash, slaked lime, cement, ox horn powder, aluminum powder, copper oxide, polyphosphoric acid, aluminum hydroxide, hydroxypropyl methyl cellulose and steel fiber. The preparation method of the inorganic cured foam material comprises the following steps of: firstly, adding the coal ash, the cement, the hydroxypropyl methyl cellulose, the steel fiber and the slaked lime in water to form a coal ash substrate serous fluid; secondly, adding the ox horn powder into a little water for stirring to form prefabricated mucus, and sufficiently stirring the coal ash substrate serious fluid and the prefabricated mucus to form a mixed solution; thirdly, adding an inorganic adhesive system into the mixed solution and sufficiently stirring to form a mixed adhesive solution; and finally, adding the aluminum powder for sufficiently stirring uniformly, foaming the serious fluid by utilizing an organic self-foaming system, and preparing the inorganic cured foam material for surface leaking stoppage of the shallow buried coal seam mining area. According to the invention, the seam infiltration capacity is strong, the compressive strength is large, the high temperature resistance and the heat insulation performance are good, and the substrate is purely inorganic and pollution-free.

Description

technical field [0001] The invention relates to an inorganic solidified foam material and a preparation method, in particular to an inorganic solidified foam material and a preparation method for plugging leaks on the surface of a shallow coal seam mining area. Background technique [0002] Spontaneous coal combustion is one of the most important disasters faced by my country's coal mine safety production, which seriously threatens the safety of underground workers and the normal mining of working faces, resulting in significant economic losses. In recent years, the focus of my country's energy strategy has shifted to the west, and coal seams in shallow-buried mining areas in the west are prone to spontaneous combustion, buried shallow (generally at a depth of 30-250m), and have serious air leakage from surface fissures. To prevent air leakage from surface fissures, on the basis of obtaining the law of air leakage from fissures, it is one of the most effective means to preven...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B38/02
CPCC04B28/02C04B28/342C04B2111/00724Y02W30/91C04B14/30C04B14/303C04B14/48C04B18/06C04B22/04C04B22/064C04B22/165C04B24/14C04B24/383C04B38/02C04B40/0028C04B7/02
Inventor 秦波涛鲁义张雷林贾玉威李磊
Owner CHINA UNIV OF MINING & TECH
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