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Method for preparing nanometer surface coating

A surface coating and nanotechnology, applied in the coating, metal material coating process, etc., can solve the problems of inability to ensure high density and high adhesion of the coating, depositing a dense coating, and difficulty in direct spraying, etc. Achieve the effect of low cost, increased diffusion depth and high adhesion

Inactive Publication Date: 2013-12-25
CHONGQING ACADEMY OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The advantage of the outer coating method is that the process is simple and easy to implement, but the following problems need to be solved: first, the small momentum cannot deposit a dense coating on the surface of the substrate, and it is difficult to spray directly; second, it is necessary to ensure that the nanoparticles do not sinter during the spraying process , to maintain the nanocrystalline structure in the final coating; the third is that the equipment is more complicated and the energy consumption is higher
However, due to the characteristics of the self-propagating high-temperature reaction, even if a certain external pressure is applied when coating the self-propagating reactant, the high density and high adhesion of the coating cannot be ensured.

Method used

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  • Method for preparing nanometer surface coating

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Embodiment 1

[0024] The method for preparing nanometer surface coating of the present embodiment, comprises the following steps:

[0025] 1) After ball milling the self-propagating reaction nickel-aluminum mixed powder for 6 hours, coat it on the surface of the metal plate (carbon steel plate) with a coating thickness of 2mm, such as figure 1 shown;

[0026] 2) Use a resistance wire to ignite the nickel-aluminum mixed powder coating coated on the surface of the metal plate, and the nickel-aluminum mixed powder coating undergoes a self-propagating reaction, figure 2 Shown is the self-propagating reaction mechanism of the powder coating in the depth direction, while the depth reaction, the self-propagating reaction will expand in the plane direction;

[0027] 3) The nickel-aluminum mixed powder coating is subjected to shot peening within 30s after the self-propagating reaction occurs, such as image 3 As shown, the shot peening angle is 90 degrees, the shot peening speed is 100m / s, the sh...

Embodiment 2

[0029] The method for preparing nanometer surface coating of the present embodiment, comprises the following steps:

[0030] 1) After ball milling the self-propagating reaction nickel-titanium mixed powder for 4 hours, it is coated on the surface of the metal plate (carbon steel plate) with a coating thickness of 2mm, such as figure 1 shown;

[0031] 2) Use a resistance wire to ignite the nickel-titanium mixed powder coating coated on the surface of the metal plate, and the nickel-titanium mixed powder coating will undergo a self-propagating reaction;

[0032] 3) The nickel-titanium mixed powder coating is subjected to shot peening within 15s after the self-propagating reaction occurs, such as image 3 As shown, the shot peening angle is 90 degrees, the shot peening speed is 100m / s, the shot peening type is carbon steel ball, and the shot peening size is 20μm; after the self-propagating reaction and shot peening treatment, the nanometer surface coating is obtained .

Embodiment 3

[0034] The method for preparing nanometer surface coating of the present embodiment, comprises the following steps:

[0035] 1) After ball milling the self-propagating reaction titanium-carbon mixed powder for 2 hours, coat it on the surface of the metal plate (carbon steel plate) with a coating thickness of 2 mm, such as figure 1 shown;

[0036] 2) Ignite the titanium-carbon mixed powder coating coated on the surface of the metal plate with a resistance wire, and the titanium-carbon mixed powder coating undergoes a self-propagating reaction;

[0037] 3) The titanium-carbon mixed powder coating is subjected to shot peening within 25s after the self-propagating reaction occurs, such as image 3 As shown, the shot peening angle is 90 degrees, the shot peening speed is 100m / s, the shot peening type is carbon steel ball, and the shot peening size is 20μm; after the self-propagating reaction and shot peening treatment, the nanometer surface coating is obtained .

[0038] In the ...

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Abstract

A disclosed method for preparing a nanometer surface coating comprises the following steps: 1) performing ball milling on a self-propagation reaction metal mixed powder, coating on the surface of a metal plate; 2) igniting the metal mixed powder coating on the surface of the metal plate to make the metal mixed powder coating have a self-propagation reaction; and 3) performing shot blasting on the metal mixed powder coating subjected to the self-propagation reaction, to obtain the nanometer surface coating after the self-propagation reaction and shot blasting are finished. According to the method, shot blasting is performed on the coating after the self-propagation reaction is carried out for a certain time, so that the coating metal powder is increased in diffusion depth in the metal surface, and the bonding force between the coating and the matrix metal is increased; by shot blasting, the density of the coating is improved substantially, and shot blasting has surface nanocrystallization effect; the prepared coating has high density and high viscosity; and the preparation method of the invention is simple in equipment, low in energy consumption and low in cost.

Description

technical field [0001] The invention relates to a method for preparing a nano surface coating, in particular to a method for preparing a nano surface coating with high compactness and high adhesion. Background technique [0002] Using nanotechnology to process metal nano surface coatings on key components such as machinery (such as bearings, gears, springs, etc.), can improve the wear resistance, hardness and life of the equipment. At present, the methods for preparing nano surface coatings are mainly outer coating method and internal diffusion generation method. External coating methods include physical vapor deposition, thermal spraying or plasma spraying, coating methods, etc.; internal diffusion methods include chemical vapor deposition, electrodeposition or electroplating, self-assembly methods, etc. The advantage of the outer coating method is that the process is simple and easy to implement, but the following problems need to be solved: first, the small momentum cann...

Claims

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Application Information

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IPC IPC(8): C23C24/10C21D7/06C22F1/00
Inventor 王开阳薛雯娟刘林森杨锦姜山蒋显全潘复生
Owner CHONGQING ACADEMY OF SCI & TECH
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