Polyester fiber and preparation method thereof

A technology of polyester fiber and polyethylene terephthalate, which is applied in the field of polyester fiber and its preparation, can solve the problems of polyester fiber static electricity and flame retardancy that cannot be effectively solved, and achieve a simple and controllable preparation process, Ease of industrialization, effect of improving hygroscopic performance

Inactive Publication Date: 2014-10-01
JIANGSU YINGXIANG FIBER
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

Although the above method has a positive effect on improving the hygroscopicity of fibers, it cannot effectively solve the problems of static electricity and flame retardancy in polyester fibers. Therefore, it is important to develop new multifunctional polyester fibers with flame retardancy, antistatic and high hygroscopicity. significance

Method used

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  • Polyester fiber and preparation method thereof
  • Polyester fiber and preparation method thereof
  • Polyester fiber and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] (1) Preparation of polyurea-formaldehyde-coated aligned carbon nanotube bundles: In a container equipped with a stirrer, weigh 30g of urea and 60g of formaldehyde solution (mass concentration 37-40%). After the urea is fully dissolved, slowly Heating and using triethanolamine to adjust the pH value of the solution to 8, and keeping it warm at 50°C for 1 hour to obtain a urea-formaldehyde prepolymer solution, and then adding 30g of sodium lauryl sulfate, 3000g of deionized water and 50g of oriented multi-walled carbon nano Tube bundle, after ultrasonic dispersion and mechanical stirring, set a certain stirring speed (10000rpm), adjust the pH value of the solution to 2 with hydrochloric acid solution, slowly raise the temperature, wait until the temperature rises to 45-50°C, keep it warm for 3h, and end the reaction. washing the product several times with water, suction filtering and drying to obtain polyurea-formaldehyde-coated aligned carbon nanotube bundles;

[0029] (...

Embodiment 2

[0031] (1) Preparation of polyurea-formaldehyde-coated aligned carbon nanotube bundles: In a container equipped with a stirrer, weigh 20g of urea and 40g of formaldehyde solution (mass concentration 37-40%). After the urea is fully dissolved, slowly Heating and using sodium carbonate solution to adjust the pH value of the solution to 9, keeping it warm at 70°C for 0.5h to obtain a urea-formaldehyde prepolymer solution, and then adding 5g sodium dodecylbenzenesulfonate, 2000g deionized water and 6g orientation Multi-wall carbon nanotube bundles, after ultrasonic dispersion and mechanical stirring, set a certain stirring speed (10000rpm), adjust the pH value of the solution to 4 with sulfuric acid solution, slowly raise the temperature, wait until the temperature rises to 45-50 ° C, keep it warm for 4 hours, and end reaction. washing the product several times with water, suction filtering and drying to obtain polyurea-formaldehyde-coated aligned carbon nanotube bundles;

[0032...

Embodiment 3

[0034](1) Preparation of polyurea-formaldehyde-coated aligned carbon nanotube bundles: In a container equipped with a stirrer, weigh 10% urea and 20g formaldehyde solution (mass concentration 37-40%). After the urea is fully dissolved, slowly Heating and using sodium hydroxide solution to adjust the pH value of the solution to 8, keeping it warm at 60°C for 1 hour to obtain a urea-formaldehyde prepolymer solution, and then adding 0.5g styrene-maleic anhydride copolymer, 100g deionized water and 2g Oriented multi-walled carbon nanotube bundles, after ultrasonic dispersion and mechanical stirring, set a certain stirring speed (10000rpm), adjust the pH value of the solution to 4 with citric acid solution, slowly raise the temperature, wait until the temperature rises to 45 ~ 50 ° C, keep warm for 4 hours , to end the reaction. washing the product several times with water, suction filtering and drying to obtain polyurea-formaldehyde-coated aligned carbon nanotube bundles;

[0035...

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Abstract

The invention relates to a polyester fiber and a preparation method thereof. An oriented carbon nanotube bundle coated by polyethylene terephthalate and polyurea formaldehyde is mainly used as a raw material; and an oriented carbon nanotube bundle / polyester fiber coated by the polyurea formaldehyde is obtained through the spinning and the thermal stretching. The method has a simple operation process; the prepared polyester fiber contains rich hydrophilic radicals, and the interior thereof is a porous structure; and the polyester fiber has potential high moisture adsorptivity, flame retardance and antistatic performance.

Description

technical field [0001] The invention belongs to the field of polymer fiber preparation, and in particular relates to a polyester fiber and a preparation method thereof. Background technique [0002] In the past two decades, my country has made great progress in the chemical fiber industry, including polyester, nylon, spandex and other fiber varieties. The production technology is becoming more and more mature. Among them, polyester fiber is the most important and fastest growing fiber variety. Polyester fiber is usually Refers to polyethylene terephthalate fiber. [0003] Polyethylene terephthalate (PET) fiber has the advantages of high strength, good elasticity, good processing performance, excellent textile performance and wearing performance. It is the world's largest output and most widely used synthetic fiber variety, which can be used in Clothing, bedding, various decorative fabrics, special fabrics for national defense and other industrial fiber products, etc. [000...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01F6/92D01F1/10
Inventor 袁莉陈国强高永明王国柱梁国正顾嫒娟管新海沈家康钮真荣
Owner JIANGSU YINGXIANG FIBER
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