Soybean meal-based adhesive for wood and preparation method thereof

A technology of adhesives and soybean meal, which is applied in the field of soybean meal-based adhesives for wood and its preparation, can solve the problems of prolonged curing time, increased difficulty of production process, and increased production cost, so as to increase the water-resistant handover performance, increase the added value of products, and save The effect of production costs

Inactive Publication Date: 2014-12-03
BEIJING FORESTRY UNIVERSITY
View PDF5 Cites 13 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

For example: 1) Although the use of low molar ratio modified urea-formaldehyde resin adhesives can effectively reduce the formaldehyde emission of wood-based panel products, the bonding strength of the products is often reduced, which cannot meet the requirements of use; and it can lead to prolonged curing time and reduced production efficiency; 2) Adding formaldehyde scavenger to urea-formaldehyde resin adhesives for wood-based panels can effectively reduce the release of free formaldehyde from wood-based panels, but it often reduces the bonding strength of wood-based panels at the same time; at the same time, the price of general formaldehyde scavenger is often much higher than that of urea-formaldehyde resin adhesives. Adding improves product cost and reduces product competitiveness; 3) Carry out post-processing to wood-based panels, as the invention patent application with publication number CN1526528 discloses a method for preparing E1 / EO grade environment-friendly wood-based panels using ammonia vacuum method. Manufacturing process; the utility model patent with publication number CN2394770 discloses a treatment device for reducing formaldehyde emission from wood-based panels. These post-processing methods not only make the manufacturing process of wood-based panels complicated, but also require huge investment in post-processing equipment and significantly increase production costs. ; 4) The use of other environmentally friendly adhesives, such as isocyanate adhesives, has led to a substantial increase in the production cost of wood-based panels and increased difficulty in the production process, which is difficult for enterprises and users to accept; Unglue
In summary, although the above measures can effectively reduce the release of free formaldehyde from wood-based panels, they cannot completely solve the problem of formaldehyde release, or cannot be popularized due to reasons such as high production costs.
[0005] In addition, the currently widely used wood-based panel adhesives also have the problem of dependence on fossil resources of raw materials, which do not meet the requirements of sustainable development

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Soybean meal-based adhesive for wood and preparation method thereof
  • Soybean meal-based adhesive for wood and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] A soybean meal-based adhesive for wood, prepared from the following raw materials by weight:

[0028] Demineralized water 68kg

[0029] Sodium dodecylbenzenesulfonate 1 kg

[0030] Defatted Soy Protein Powder 26kg

[0031] Cross-linking enhancer 3 kg

[0032] Sodium Benzoate 2kg

[0033] A preparation method of the above-mentioned soybean meal-based adhesive for wood, comprising the following steps:

[0034] 1) Weigh each raw material according to the above weight ratio;

[0035] 2) Add all the demineralized water, soy protein powder and sodium dodecylbenzenesulfonate into the reaction kettle equipped with agitator, thermometer and condensing device, and stir evenly;

[0036] 3) Heat in a water bath to 40-45°C and keep warm for 3 hours;

[0037] 4) The temperature of the reactant is lowered to 30°C to obtain a uniform soy protein mucus;

[0038] 5) Add the enhancer to the obtained soybean protein mucilage, mix well, and then add sodium benzoate to make the soybea...

Embodiment 2

[0043] A soybean meal-based adhesive for wood, prepared from the following raw materials by weight:

[0044] Demineralized water 64 kg

[0045] Sodium dodecylbenzenesulfonate 2 kg

[0046] Defatted Soy Protein Powder 29 kg

[0047] Enhancer 5kg

[0048] Sodium Benzoate 4kg

[0049] A preparation method of the above-mentioned soybean meal-based adhesive for wood, comprising the following steps:

[0050] 1) Weigh each raw material according to the above weight ratio;

[0051] 2) Add all the demineralized water, soy protein powder and sodium dodecylbenzenesulfonate into the reaction kettle equipped with agitator, thermometer and condensing device, and stir evenly;

[0052] 3) Heat in a water bath to 40-45°C and react for 6 hours;

[0053] 4) The temperature of the reactant is lowered to 30°C to obtain a uniform soy protein mucus;

[0054] 5) Add the enhancer to the obtained soybean protein mucilage, mix well, and then add sodium benzoate to make the soybean protein adhesiv...

Embodiment 3

[0059] A soybean meal-based adhesive for wood, prepared from the following raw materials by weight:

[0060] Demineralized water 62 kg

[0061] Sodium dodecylbenzenesulfonate 2 kg

[0062] Defatted Soy Protein Powder 29 kg

[0063] Enhancer 7kg

[0064] Sodium Benzoate 3kg

[0065] A preparation method of the above-mentioned soybean meal-based adhesive for wood, comprising the following steps:

[0066] 1) Weigh each raw material according to the above weight ratio;

[0067] 2) Add all the demineralized water and soybean protein powder into the reaction kettle equipped with agitator, thermometer and condensing device, and stir evenly;

[0068] 3) Heat in a water bath to 65-70°C and react for 5 hours;

[0069] 4) The temperature of the reactant is lowered to 30°C to obtain a uniform soy protein mucus;

[0070] 5) Add the enhancer to the obtained soybean protein mucilage, mix well, and then add sodium benzoate to make the soybean protein adhesive.

[0071] The cross-linki...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention discloses a soybean meal-based adhesive for wood and a preparation method thereof. The soybean meal-based adhesive is prepared from the following materials in parts by weight: 60-70 parts of dispersing medium, 20-35 parts of defatted soybean protein powder, 0.5-2 parts of sodium dodecyl benzene sulfonate, 1-8 parts of cross-linking reinforcing agent and 1-8 parts of sodium benzoate. The preparation method comprises the following steps: adding the defatted soybean protein powder and the sodium dodecyl benzene sulfonate to a dispersing medium; uniformly stirring, and keeping temperature at 60-80 DEG C for 3-6 hours; and then reducing the temperature of an obtained mixture to 25-35 DEG C, adding the cross-linking reinforcing agent and the sodium benzoate, and uniformly stirring. The preparation method disclosed by the invention has the advantages of simple process and convenience for operation; and the produced adhesive is free of formaldehyde, and main raw materials are derived from renewable substances, and thus safety and environmental friendliness are achieved.

Description

technical field [0001] The invention relates to an adhesive, in particular to a soybean meal-based adhesive for wood and a preparation method thereof, belonging to the field of adhesives. Background technique [0002] With the improvement of people's living standards and the continuous and stable development of construction, decoration, packaging and other industries, the output of wood-based panels in my country has grown rapidly. In 2013, the total output of wood-based panels in my country was 272 million m 3 , accounting for about 50% of the world's total production. Among them, the particle board is 13.58 million m 3 , a year-on-year increase of 5.3%; fiberboard 59.83 million m 3 , a year-on-year increase of 4.0%; plywood 157 million m 3 , an increase of 10.5% year-on-year. The total output of wood-based panels, plywood, furniture, and wood flooring has ranked first in the world for many years in a row. [0003] The adhesives commonly used in the production of wood...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Applications(China)
IPC IPC(8): C09J189/00C09J133/26C09J11/06C08J3/24C08L33/26C08K5/07
Inventor 罗晶高强李建章张世锋周文瑞张伟陈惠
Owner BEIJING FORESTRY UNIVERSITY
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products