Nano TiO2/nano ZnO compounded lubricating oil additive and preparation method thereof
A lubricating oil additive and nanotechnology, applied in the field of lubrication, can solve problems such as the great influence of the physical properties of the liquid, the increase of the friction coefficient of the friction surface, and the maintenance of the bearing capacity of the liquid film, so as to improve the continuous stability, reduce the friction coefficient, and transfer the friction. The effect of coefficients
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Embodiment 1
[0020] A kind of nano TiO 2 / Nano ZnO composite lubricating oil additive, the nano TiO 2 / The addition of nanometer ZnO is 0.02%.
[0021] The nano-TiO 2 The particle size of ZnO is 10nm, the particle size of nano-ZnO is 20nm, and the weight ratio of the two is 1:1.
[0022] The above nano-TiO 2 The preparation method of / nano ZnO composite lubricating oil additive, comprises the steps:
[0023] (1) Preparation of nano-ZnO: with NaOH and Zn(NO 3 ) 2 In order to react the former yield body, a ZnO powder with a size of 40nm was prepared;
[0024] (2) Nano-TiO 2 Preparation: metal titanium is placed in a tungsten boat, heated and evaporated under 200Pa of He gas, the fine particles solidified from the supersaturated steam are collected on the liquid nitrogen cooling jacket, and then 5000Pa of pure oxygen is injected into the reaction chamber, Make titanium particles rapidly and completely oxidize TiO 2 into powder;
[0025] (3) Oleic acid coating: the above nano-ZnO and...
Embodiment 2
[0029] A kind of nano TiO 2 / Nano ZnO composite lubricating oil additive, characterized in that the nano TiO 2 / The addition of nanometer ZnO is 1%.
[0030] The nano-TiO 2 The particle size of ZnO is 20nm, the particle size of nano-ZnO is 2040nm, and the weight ratio of the two is 1:2.
[0031] The above nano-TiO 2 The preparation method of / nano ZnO composite lubricating oil additive, comprises the steps:
[0032] (1) Preparation of nano-ZnO: with NaOH and Zn(NO 3 ) 2 In order to react the precursor, ZnO powder with a size of 80nm was prepared;
[0033] (2) Nano-TiO 2 The preparation of metal titanium is placed in a tungsten boat, heated and evaporated under 1000Pa of He gas, and the fine particles solidified from the supersaturated steam are collected on the liquid nitrogen cooling jacket, and then 5000Pa of pure oxygen is injected into the reaction chamber. Make titanium particles rapidly and completely oxidize TiO 2 into powder;
[0034] (3) Oleic acid coating: t...
Embodiment 3
[0037] A kind of nano TiO 2 / Nano ZnO composite lubricating oil additive, characterized in that the nano TiO 2 / The addition of nanometer ZnO is 0.1%.
[0038] The nano-TiO 2 The particle size of ZnO is 15nm, the particle size of nano-ZnO is 30nm, and the weight ratio of the two is 2:1.
[0039] The above nano-TiO 2 The preparation method of / nano ZnO composite lubricating oil additive, comprises the steps:
[0040] (1) Preparation of nano-ZnO: with NaOH and Zn(NO 3 ) 2 In order to react the former yield body, a ZnO powder with a size of 60nm was prepared;
[0041] (2) Nano-TiO 2The preparation of metal titanium is placed in a tungsten boat, heated and evaporated under 600Pa of He gas, and the fine particles solidified from the supersaturated steam are collected on the liquid nitrogen cooling jacket, and then 5000Pa of pure oxygen is injected into the reaction chamber. Make titanium particles rapidly and completely oxidize TiO 2 into powder;
[0042] (3) Oleic acid c...
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