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Method for controlling atmospheric plasma spraying of easily-oxidized coating under atmosphere open environment

A technology for controlling atmosphere and plasma spray gun, applied in coating, metal material coating process, melting spray plating, etc., can solve the problems of easy change of substrate performance, limited change of coating composition, easy oxidation of powder, etc. Anti-oxidation and anti-ablation properties of the coating, ensuring purity and performance, and inhibiting the effect of oxidation

Active Publication Date: 2014-12-17
BEIJING INSTITUTE OF TECHNOLOGYGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The embedding method requires long-term diffusion at high temperature, the size of the sample is limited, and the properties of the substrate are prone to change; the composition of the coating prepared by chemical vapor deposition is limited, and the thickness of the surface coating is too thin; the coating formed by laser cladding is poor. , with many holes, it is not suitable for workpieces with complex shapes; the coating prepared by plasma spraying technology has the advantages of small substrate deformation, controllable coating composition in a wide range, easy control of thickness, and easy operation, etc. Under certain conditions, the powder is prone to oxidation, which affects the coating performance, and cannot be sprayed in the atmosphere, resulting in limited use of the environment

Method used

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  • Method for controlling atmospheric plasma spraying of easily-oxidized coating under atmosphere open environment

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] The spraying powder is a composite powder of zirconium boride and silicon carbide, the mass ratio of the two is 1:1, and the particle size range is 20 μm to 80 μm.

[0034] (1) Firstly, the surface of the substrate material is pre-sandblasted with a dry sandblasting machine. The blasting material is No. 24 white corundum particles with a particle size of 850 μm, so as to ensure the bonding strength and coating quality between the coating and the substrate.

[0035] (2) Open the argon gas bottle connected to the above-mentioned protective gas flow channel, expansion gas flow channel and vortex channel, control the pressure of the protective gas argon to 0.5MPa, and the flow rate to be 15SCFH. A protective atmosphere environment is formed between the materials, and the argon gas from the expansion airflow channel expands the range of the formed protective atmosphere environment, while the argon gas from the vortex channel forms a vortex protective atmosphere outside the sp...

Embodiment 2

[0039] The spraying powder is a composite powder of hafnium boride and zirconium carbide, the mass ratio of the two is 2:1, and the particle size range is 5 μm to 63 μm.

[0040] (1) Firstly, the surface of the substrate material is pre-sandblasted with a dry sandblasting machine. The blasting material is No. 24 white corundum particles with a particle size of 850 μm, so as to ensure the bonding strength and coating quality between the coating and the substrate.

[0041] (2) Open the argon gas bottle connected to the above-mentioned protective gas flow channel, expansion gas flow channel and vortex channel, control the pressure of the protective gas argon to 0.3MPa, and the flow rate to be 5SCFH. A protective atmosphere environment is formed between the materials, and the argon gas from the expansion airflow channel expands the range of the formed protective atmosphere environment, while the argon gas from the vortex channel forms a vortex protective atmosphere outside the spra...

Embodiment 3

[0045] The spraying powder is a composite powder of zirconium boride and zirconium carbide, the mass ratio of the two is 1:3, and the particle size range is 45 μm to 100 μm.

[0046] (1) Firstly, the surface of the substrate material is pre-sandblasted with a dry sandblasting machine. The blasting material is No. 24 white corundum particles with a particle size of 850 μm, so as to ensure the bonding strength and coating quality between the coating and the substrate.

[0047] (2) Open the argon gas bottle connected to the above-mentioned protective gas flow channel, expansion gas flow channel and vortex channel, control the pressure of the protective gas argon to 1.0MPa, and the flow rate to be 30SCFH. A protective atmosphere environment is formed between the materials, and the argon gas from the expansion airflow channel expands the range of the formed protective atmosphere environment, while the argon gas from the vortex channel forms a vortex protective atmosphere outside the...

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Abstract

The invention discloses a method for controlling atmospheric plasma spraying of an easily-oxidized coating under the atmosphere open environment. According to the method, in the plasma spraying process, powder can be effectively prevented from being oxidized, the purity and the property of the coating are ensured, the oxidation-resisting property and the ablation-resisting property of the coating are improved, and the service life of the coating is prolonged. The method specifically comprises the points that before plasma spraying is carried out, an air flow channel is arranged outside a plasma spraying gun muzzle; the air flow channel is connected with a protection air bottle, and therefore the aim that the protection atmosphere environment is formed between the spraying gun opening and a base material can be achieved. Before the coating is sprayed, the protection air bottle is opened in advance, the protection atmosphere environment is formed, and then plasma spraying equipment is controlled to carry out spraying of the easily-oxidized coating. According to the method, manufacturing of a silicide coating under the atmospheric pressure open environment can be achieved, the process is easy to operate, parameters are easy to regulate and control, and the method is a high-efficiency low-cost coating manufacturing process.

Description

technical field [0001] The invention relates to a method for preparing an easily oxidizable coating, in particular to a method for controlling an atmosphere plasma spraying an easily oxidizable coating in an open atmosphere environment, and belongs to the technical field of surface engineering. Background technique [0002] With the progress and development of current science and technology, the new generation of carrier aircraft has become the main development direction of aerospace with its main basic features of hypersonic speed, high maneuverability, and remote precise control, and will play an important role in future national security. . C / C composites have become a hot topic in the research of hypersonic vehicle materials in recent years because of their excellent properties such as high temperature strength, high thermal conductivity, low thermal expansion coefficient, low density, high temperature stability, and corrosion resistance. [0003] Borides have the advan...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23C4/12C23C4/10C23C4/134C23C4/137
Inventor 柳彦博王全胜王皓魏思豪赵云郝斐
Owner BEIJING INSTITUTE OF TECHNOLOGYGY
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