Superheavy oil crude oil reverse-phase demulsifier preparation method
A reversed-phase demulsifier and super-heavy oil technology, applied in the direction of chemical dehydration/demulsification, etc., can solve the problems of high viscosity and high density of heavy oil, and achieve the requirements of low equipment requirements, simple operation and good demulsification effect. Effect
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Embodiment 1
[0013] Embodiment 1: the preparation of a kind of compound type inverse demulsifier, concrete operating steps are:
[0014] 1. Synthesis of multi-segment polyquaternary ammonium salts: Add starter glycerin and catalyst boron trifluoride ether solution into a three-necked flask equipped with an electric stirring rod, condenser tube and dropping funnel, turn on the electric stirring rod, and control temperature at 50°C, add epichlorohydrin drop by drop, after the dropwise addition, raise the temperature to 70°C and keep it warm for 4 hours to obtain brown multi-chain chlorinated polyether; add chlorinated polyether and triethyl Amine aqueous solution, ensure the equivalent of chlorine and amino group, pass nitrogen gas, raise the temperature to 70°C, keep stirring for 3 hours, and finally raise the temperature to 125°C to continue the reaction to obtain reddish-brown multi-segment cationic polyquaternary ammonium salt.
[0015] 2. Synthesis of dendritic polyamide-amine: under th...
Embodiment 2
[0017] Embodiment 2: the preparation of a kind of compound type inverse demulsifier, concrete operating steps are:
[0018] 1. The synthesis of multi-segment polyquaternium salt is the same as in Example 1.
[0019] 2. The synthesis of dendritic polyamide-amine is the same as in Example 1.
[0020] 3. Preparation of composite demulsifier: The synthesized polyquaternium salt, 3.0-generation polyamide-amine, polyaluminum chloride and ethanol are prepared into a water-soluble solution in an appropriate proportion to obtain a composite reverse demulsifier. The mass fraction ratio of polyquaternary ammonium salt, 3.0-generation polyamidoamine, polyaluminum chloride and solvent is 15:15:10:300.
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