231results about How to "Fast flocculation" patented technology

The invention discloses a method of preparing high-purity vanadium pentoxide from roasting-method vanadium solution. The method comprises the following steps: adding a purifying agent into the roasting-method vanadium solution, wherein the purifying agent is polyaluminium chloride, magnesium chloride or calcium chloride, or the purifying agent is polyaluminium chloride and magnesium chloride, or polyaluminium chloride and calcium chloride; uniformly stirring the roasting-method vanadium solution containing the purifying agent, standing for settling, then filtering, and adding ammonium salt into the filtrate to precipitate vanadium; and finally, calcining meta-ammonium and deaminizing to prepare vanadium pentoxide with the purity being higher than 99.5%. Polyaluminium chloride serving as the purifying agent can be used for polymerizing jellies with several molecules into large particles with several tens of thousands of molecules, even hundreds of thousands of molecules. The large-particle molecular polymer is easy to settle in the vanadium solution and can be separated from the solution. The method provided by the invention has the advantages that the consumption of polyaluminium chloride is low, the flocculation process is simple, the flocculation capacity is strong, the flocculation speed is high, pollution is hardly caused and the cost is low.

The invention provides a material and a method for repairing polluted water and bottom mud. Specifically, nontoxic and innoxious solid particulates are adopted and are loaded with microbes according to a certain method before preparing a composite material; the composite material is used for in-situ flocculation or adsorption of pollutants in water, and transfers the pollutants to the bottom mud, so as to realize in-situ collection and concentration of the pollutants in water and fast degradation in the bottom mud; and after settling to the bottom mud, the composite material can also degrade pollutants in the bottom mud, so as to improve the water quality bottom matter environment. The invention can be applied to the comprehensive repairing of shallow water type lakes, slow flow river channels, small-sized reservoirs, wetlands and ponds which are eutrophicated or seriously polluted by organic substances.

The invention relates to the technical field of wastewater treatment, and particularly relates to a dyeing wastewater treatment agent and a preparation method thereof. The dyeing wastewater treatment agent comprises the following raw materials in parts by weight: 2-10 parts of ferrous sulfate, 20-30 parts of magnesium sulfate, 0.5-2 parts of polyacrylamide, 10-20 parts of iron nitrate, 1-5 parts of nickel nitrate, 40-60 parts of polyaluminum chloride, 10-20 parts of modified kieselguhr, 8-22 parts of meerschaum powder, 10-20 parts of crosslinked rectorite, 5-10 parts of chitosan-graphene composite material and 1-3 parts of graphene nano layer/MnO2 compound. The dyeing wastewater treatment agent provided by the invention has the advantages of convenient production method, low investment, quick effect taking and no secondary pollution.

The invention discloses a dyeing wastewater treating agent and a manufacturing method thereof. The dyeing wastewater treating agent is prepared from the following raw materials in parts by mass: 70-100 parts of diatomite, 40-70 parts of attapulgite, 90-120 parts of modified starch, 15-40 parts of acrylamide, 2-10 parts of ferrous sulfate, 20-30 parts of magnesium sulfate, 10-25 parts of meerschaum powder, 10-20 parts of crosslinked rectorite, 0.5-2 parts of polyacrylamide, 20-30 parts of cationic monomer, 0.17-0.21 part of initiator and 0.09-0.1 part of crosslinking agent. The treating agent can perform the flocculating settling purification and disinfection functions on the dyeing wastewater, has the characteristics of wide raw material sources, lower cost and favorable treatment effect, and is convenient for popularization and application.

The invention discloses a composite reagent for deep removal of heavy metals in wastewater and a preparation method thereof. The composite reagent is prepared from the following raw materials in parts by weight: a component A including 20-30 parts of modified attapulgite powder, 30-50 parts of a modified natural high molecular polymer and 0-3 parts of a surfactant; a component B namely an inorganic flocculating agent, wherein the weight ratio of the component A to the component B is (2.5-8.3):1. The composite reagent disclosed by the invention has very strong adsorption, chelating and flocculation performances on heavy metal ions in water, has a plurality of effects of auxiliary reduction of COD (chemical oxygen demand), decoloration, dephosphorization and the like at the same time, and is good in treatment effect, and the preparation method is simple and easy.

The invention relates to a magnetic flocculant and a preparation method thereof, wherein the magnetic flocculant is cationic polyacrylamide-modified magnetic nanometer Fe3O4 particles. The magnetic flocculant provided by the invention retains the advantages of low dosage of organic high molecular flocculant, high flocculation speed, coexistence of salts, low pH value and temperature influence, low total amount of flocculating constituent and the like; and the superparamagnetism of the flocculant enables the flocculant to quicken the precipitation under the effect of an applied magnetic field and to realize quick and efficient separation of residual flocculant and flocculation. The magnetic flocculant provided by the invention has the advantages of simple preparation technique, low cost, easiness in amplification and no secondary pollution, and facilitates realizing efficient and economic flocculation operation.

The efficient flocculant consists of hydroxide colloid 0.5-15 wt%, acrylamide 50-95 wt% and cationic monomer 0-45 wt%. The hydroxide colloid may be aluminum other, iron hydroxide, magnesium hydroxide or zinc other, and has colloid size of 10-200 nm. The cationic monomer includes DMDAAC or DMC. The organic-inorganic hetero efficient flocculant has in-situ polymerized acrylamide/cationic monomer copolymer linked to the surface of charged inorganic colloid particle, so that it has the synergistic effect of electrically neutralizing effect of inorganic flocculant and the bridging effect of organic polymer and greatly raised flocculating efficiency.

The invention discloses a dephosphorization flocculating agent and a preparation method thereof. The dephosphorization flocculating agent is formed by compounding an inorganic flocculating agent and an organic flocculating agent. The raw materials of the inorganic flocculating agent comprise sodium ferrate, borax, ferrous sulfate, silicate or aluminate; the raw materials of the organic flocculating agent comprise modified chitosan or modified polyacrylamide. The preparation process comprises the following steps: firstly adding a non-oxidizing acid into the silicate or aluminate to obtain a polysilicate colloid or an aluminum hydroxide colloid, then adding a borax solution and a sodium ferrate solution sequentially while stirring, further dropping a ferrous sulfate solution, mixing to form the inorganic flocculating agent, standing, then adding the modified polyacrylamide or modified chitosan into the inorganic flocculating agent, curing and adding the acid till the pH value is less than 7 to obtain the finished dephosphorization flocculating agent. The flocculating agent is suitable for a wide range of water quality, is little affected by co-existing salts, the pH value of sewage and temperature and is particularly effective for dye wastewater, oilfield sewage and the like.

The invention discloses a waste water treatment process which comprises the following steps that 1) waste water enters a primary sedimentation tank through a grid to remove suspended matters; 2) the waste water overflows from the primary sedimentation tank into a regulating tank after the suspended matters are removed, and lime milk is added to adjust the pH value of the waste water to be neutral; 3) the waste water of which the pH value is adjusted to be neutral naturally flows into a neutral aeration tank and is mixed with compressed air in the aeration tank, and Fe<2+> in the waste water is converted to Fe<3+>; 4) the waste water in the aeration tank is injected to a flocculation reaction tank, polyacrylamide flocculant is added to the waste water, and then the waste water is pumped to an inclined tube sedimentation tank; and 5) supernate of the waste water in the inclined tube sedimentation tank overflows into a contact oxidation tank and is mixed with the compressed air filled into the contact oxidation tank, organic matters in the waste water are subjected to oxygenolysis, and the waste water in the contact oxidation tank is deposited through a sedimentation tank and then overflows into a clean water tank. After being treated by the waste water treatment process, the waste water can reach the standard of Integrated Waste Water Discharge Standard (GB 8978-1996); and in addition, the operating cost of a waste water treatment system is lower, and the waste water treatment volume is large .

The invention relates to a method for processing wastewater containing heavy metal ions, and belongs to the chemical field. The method comprises the following steps: 1, discharging the wastewater to a pH adjustment tank at normal temperature in order to adjust the pH value of the wastewater to a predetermined value; 2, discharging the wastewater obtained after step 1 to a curing precipitation reactor, adding a polysulfide precipitating agent to covert the heavy metal ions in the wastewater into insoluble substances of the heavy metal ions, and precipitating the insoluble substances of the heavy metal ions while precipitating elementary sulfur; 3, discharging the wastewater obtained after step 2 to a flocculating tank, adding a flocculating agent to flocculate the insoluble substances of the heavy metal ions and the elementary sulfur; and 4, discharging the wastewater obtained after step 3 to a precipitating tank, precipitating, and discharging the obtained supernatant. The method has the advantages of high removal rates of a plurality of the heavy metal ions, no secondary pollution, low cost, and easy realization.

The invention provides a preparation method of modified polyferric sulfate. Kaolin and talcum are utilized to perform modification treatment on the polyferric sulfate. When the modified polyferric sulfate is used in a waste paper papermaking advanced wastewater treatment technique, the pollutant removal ratio is high, and the chroma removal effect is good: the removal ratio of the modified polyferric sulfate for COD (chemical oxygen demand) in wastewater is up to 71.9-75%, the SS (suspended sediment) removal ratio is up to 64-75%, and the chroma removal ratio is up to 88.3-96.9%. Under the same conditions, compared with the polyferric sulfate, the COD removal ratio is enhanced by 8.3-11.2%, the SS removal ratio is enhanced by 9-12.5%, and the chroma removal ratio is enhanced by 6.9-8.3%. The modified polyferric sulfate has high flocculation speed and has the same decolorization effect; and the consumption of the modified polyferric sulfate is greatly lower than that of the polyferric sulfate, so the generated chemical sludge quantity is low, thereby saving the cost and simplifying the technique.

The invention discloses a method to prepare bio-flocculant. The invention is characterized in that aspergillus fermentating cultivation is adopted. The aspergillus is agitated and fermented (28-30 DEG C, pH6-7, under ventilating condition) for 48-60 hours; the fermentation broth is filtered and condensed, and then proper amount of ethanol is added into the condensed broth and centrifugal separation is conducted after stewing; the deposition is washed with ethanol and dried in vacuum to achieve a crude product of fawn flocculant. The prevention method has the advantages of simple condition of production and low cost. The bio-flocculant prepared by the method is applicable to disposing sewage containing granular contaminants or filth, and the dosage generally drops in 0.1 to 0.3 per mill. It is proved by flocculation treatment that, compared with the prior art, the invention has sound flocculation effect, low flocculant speed and small dosage; besides, the invention is environment-friendly and harmless to human body.

The invention relates to a heavy metal wastewater treatment medicament. The heavy metal wastewater treatment medicament comprises the following raw materials by weight: 1 part of cationic polyacrylamide, 3 to 8 parts of anionic polyacrylamide, 10 to 30 parts of an inorganic flocculating agent, 1 to 3 parts of a heavy metal chelating agent, and 58 to 85 parts of an absorbent. The invention further provides a heavy metal wastewater treatment method which comprises the following steps: taking 1 L of chemical wastewater; adding a NaOH solution into the wastewater till the pH of the obtained solution is 8.0 to 9.0; adding the heavy metal wastewater treatment medicament into the obtained solution, wherein the addition volume of the heavy metal wastewater treatment medicament is 0.04 to 0.08 percent of the weight of the chemical wastewater; stirring fast for 10 seconds; stirring slowly for 20 minutes; stopping stirring; allowing the obtained liquid to stand still for 10 minutes for layering. The heavy metal wastewater treatment medicament and the heavy metal wastewater treatment method have the benefits that 1, the preparation is simple; 2, the molecular weight of cationic polyacrylamide is low, and positive charge groups of cationic polyacrylamide can adsorb negative charges of bentonite, so that a filtration aiding system of a tight structure is formed; 3, anionic polyacrylamide is high in molecular weight, so as to subside fast and generate thick floc.

The invention relates to a flocculant for sewage treatment. The flocculant is prepared by compounding the raw materials of polyacrylamide, starch, sodium hypochlorite, sodium carboxymethylcellulose, sodium silicate, potassium peroxydisulfate, sodium sulfite and water. The prepared flocculant has the advantages of green and environmental protection, low cost, small addition amount, quick flocculation speed, little sludge, convenience and safety in use and the like.

The invention discloses a sewage treatment flocculating agent and a using method thereof. The flocculating agent comprises the following components in part by weight: 690 to 700 parts of alkali solution of which pH range is 8 to 9, 25 to 40 parts of aluminium polychloride, 10 to 15 parts of sodium silicate and 1 part of polyacrylamide. In the sewage treatment flocculating agent and the using method thereof provided by the invention, because the alkali solution of a novel formulation is adopted, the agent cost is reduced, the treatment effect is improved, the preparation process is simple, the raw material source is convenient, the wastewater treatment efficiency is high, the effect of purifying the water is good, the flocculating speed is high, the produced sludge is little, and the flocculating agent and the using method are particularly suitable for treating the mixed discharged sewage in the industries of printing and dyeing, food and the like and have great popularization and application values in the aspects of purification and treatment of printing and dyeing wastewater and other industrial wastewater.

The invention relates to the technical field of spraying waste gas treatment, in particular relates to a paint mist treatment method and a spraying tank. The paint mist treatment method comprises the following steps: (1) carrying out spraying adsorption on spraying waste gas by a water curtain formed by circulating water on a water screen baffle plate; (2) enabling the spraying waste gas to enter a rotary washing drum, carrying out rotary washing on the spraying waste gas, and carrying out spraying absorption on the spraying waste gas by a spraying device arranged at the top part of the rotary washing drum; (3) exhausting the spraying waste gas after treating the spraying waste gas through a demisting layer, wherein a paint mist decomposer and a paint mist catcher are added in the circulating water which is used for treating the spraying waste gas. According to the paint mist treatment method disclosed by the invention, the technologies of water screen spraying, rotary washing and spraying adsorption are combined, and a good paint mist removing effect is obtained; the paint mist decomposer and the paint mist catcher are matched with each other to be added in the circulating water, so that paint mist can be effectively prevented from sticking on the inner wall of the spraying tank; the paint mist in the circulating water is enabled to be flocculated and floats up, so that cleaning of floating paint mist scum is facilitated, the service cycle of the circulating water is prolonged, and the damage to equipment is reduced.

The invention discloses a preparation method for yogurt lump. The method comprises the steps of fermenting, acidization, curdling, whey discharging, water washing, storing, forming, sealing, after-ripening and packaging by adopting special lactic acid bacteria to inoculate milk or goat milk which is standardized and pasteurized. The invention can not only lead the traditional yogurt lump product to be safer and more sanitary with stable quality, subtle taste and modest hardness. And since the step of the after-ripening is controlled appropriately, the prepared yogurt lump is of fuller flavor with little cream precipitated, high yielding rate and can meet popular taste and be used for producing yogurt lump with different water content, tastes and textural quality, which has more market competitiveness and can greatly enrich the processing technology and flavor of traditional yogurt lump.

The invention relates to a modified natural polymer combined flocculating agent and a using method thereof. The flocculating agent is the combination of modified natural polymer and complexing agent, wherein the modified natural polymer is prepared by carrying out phosphorylation modification, sulfonation modification or etherification modification on one or combination of two in shells of shelled animals such as shrimps, crabs and insects, cotton, straw, bagasse and starch; the complexing agent is combination of at least two in magnesium chloride, calcium chloride, sodium hydroxide, potassium hydroxide, aluminium chloride, aluminum sulfate, aluminium potassium sulfate, calcium oxide, sodium tetraborate, ferric chloride, ferrous sulfate, ferrous chloride, ferric sulfate, boric acid, hydrochloric acid and sulfuric acid. After the modified natural polymer is added, the complexing agent can be added into the natural polymer at any time within 12h according to the need of flocculation, and the flocculation reaction can be immediately finished. The invention has the advantages of controllable flocculation, rapid flocculation speed, large and firm flocculating body, low water content, safety, non-toxicity and wide temperature adaptation range.

The invention discloses a permeability-increasing and coagulation-accelerating wetting agent for wet-type dust control. The permeability-increasing and coagulation-accelerating wetting agent comprises 0.5%-2% of cocamidopropyl betaine, 0.15%-0.8% of butylnaphthalenesulfonic acid sodium salt, 0.2%-1% of trimethyl-1-propanaminium iodide, 0.2%-1% of sucrose fatty acid ester, 1%-3% of corn starch grafting sodium acrylate, 0.5%-1.5% of isooctanol phosphate, 0.06%-0.35% of sodium alcohol ether sulphate, 0.5%-1.3% of sodium diethylhexyl sulfosuccinate, 0.2%-1.2% of polyacrylamide, 0.1%-0.8% of chitin derivative-carboxymethyl chitosan, 0.1%-0.2% of polyaspartic acid, 0.3%-0.6% of calcium chloride and the balance water. The ermeability-increasing and coagulation-accelerating wetting agent for wet-type dust control has the advantages that wetting ability of water for coal is enhanced and water molecules can wrap coal dust particles quickly, so that coagulation and falling of the coal dust particles are facilitated.

An auto-precipitation pretreatment method of high-salt wastewater comprises steps as follows: 1) a proper amount of dispersant is added to the high-salt wastewater, and then the wastewater enters a primary membrane separation system for treatment via a high-pressure pump; 2) concentrated water of the membrane separation system is collected, and a small amount of magnesium removing agent and a compound flocculant are added, so that the concentrated water is destabilized to produce precipitates; 3) the concentrated water of the membrane separation system is subjected to solid-liquid separation with an efficient precipitation technology, high-salt water returned by a supernatant and incoming water reenters the membrane separation system for treatment to form circulation, precipitates are products mainly comprising CaSO4 and Mg(OH)2 and are recycled to be used as desulfurizers; 4) the salt of water produced by the membrane separation system contains monovalent ions, the salt content is decreased, the water is classified, evaporated and treated after being subjected to membrane concentration and recycled to be used as fresh water, and salts mainly containing monovalent NaCl and KCl are recycled.

The invention discloses a modified water-soluble chitosan flocculating agent and a preparation method thereof. The preparation method comprises the following steps: a carboxymethyl reaction step: dispersing chitosan into a mixed solution of isopropanol and sodium hydroxide, stirring for alkalization so as to obtain a reaction mixture, dissolving monochloro acetic acid into isopropanol to obtain asolution, dropwise adding the solution into the reaction mixture, reacting for 3-5 hours, adding an ethanol water solution to terminate the reaction, washing, and drying, so as to obtain carboxymethylchitosan; and a cross-linking reaction step: dissolving carboxymethyl chitosan into hydrochloric acid, adjusting the pH value to 5, dissolving 3,4-dihydroxyphenylacetic acid into a certain amount ofwater to obtain a solution, adding the solution into a carboxymethyl chitosan solution, dissolving a mixture of EDC and NHS into mixed liquid of water and ethanol to obtain a solution, adding the solution into a reaction solution, adding hydrogen peroxide into the reaction solution, stirring to maintain the pH value of the reaction solution at 4.5-5.0, and reacting at the room temperature for 9-11hours, so as to obtain the modified water-soluble chitosan flocculating agent. The flocculating agent disclosed by the invention has good water solubility and flocculating property.

The invention discloses a multifunctional efficient decolorizing flocculant and a preparation method thereof. The decolorizing flocculant includes 15-25% of formaldehyde, 12-20% of dicyandiamide, 22-28% of ammonium chloride, 13-18% of urea and 20-30% of inorganic salt; and the inorganic salt is one or more selected from aluminum salt, iron salt and silicon salt. The preparation is as below: adding formaldehyde accounting for 3/5-2/3 of the total formaldehyde in a reactor, then adding urea and dicyandiamide in turn for dissolving, heating to 40+/-2 DEG C-50 +/-2 DEG C, and conducting a polymerization reaction; adding ammonium chloride and the remaining formaldehyde, controlling the temperature at 80+/-2 DEG C-90+/-2 DEG C, conducting a second polymerization, and insulating for 2-4 h; and adding inorganic salt and stirring uniformly to obtain the flocculant. The decolorization flocculant has the advantages of solid content of more than 55%, wide application, decolorization rate of more than 95%, high flocculation speed and COD removal rate reaching more than 65%, improves the process requiring repeated addition of different organic and inorganic flocculants in water treatment, and solves the problem of influence of different order of operations on wastewater treatment effects.