Organic light emitting diode device and preparation method thereof

An electroluminescent device and a luminescent technology, which are applied in the direction of electric solid-state devices, semiconductor/solid-state device manufacturing, electrical components, etc., to achieve the effects of prolonging the life of the device, good buffering effect, and small internal stress

Inactive Publication Date: 2015-04-15
OCEANS KING LIGHTING SCI&TECH CO LTD +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

The method of the invention is especially suitable for encapsulating flexible organic electroluminescent devices

Method used

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  • Organic light emitting diode device and preparation method thereof

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Embodiment 1

[0050] Such as figure 1 The schematic diagram of the structure of the organic electroluminescent device is shown. This embodiment provides a method for preparing an organic electroluminescent device, which includes the following steps:

[0051] (1) Prepare the light-emitting functional layer 20 and the cathode layer 30 on the anode substrate

[0052] a. Pretreatment of conductive glass substrate

[0053] Take the ITO glass substrate 10, and perform acetone cleaning→ethanol cleaning→deionized water cleaning→ethanol cleaning in sequence, all cleaning with an ultrasonic cleaning machine, washing and cleaning for 5 minutes, then blowing dry with nitrogen, and drying in an oven for later use; The cleaned ITO glass also needs surface activation treatment to increase the oxygen content of the conductive surface layer and improve the work function of the conductive layer surface; the thickness of ITO is 100nm;

[0054] b. Preparation of luminescent functional layer 20 and cathode la...

Embodiment 2

[0071] A method for preparing an organic electroluminescent device, comprising the following steps:

[0072] (1) Prepare the luminescent functional layer and the cathode layer on the anode substrate as in Example 1;

[0073] (2) Prepare the encapsulation layer on the cathode layer

[0074] a. Fabrication of germanium carbonitride barrier layer:

[0075] Depositing a germanium carbonitride barrier layer on the surface of the cathode layer by plasma enhanced chemical vapor deposition (PECVD), the material of the germanium carbonitride barrier layer is germanium carbonitride, and the deposited germanium carbonitride barrier layer The thickness is 140nm. In the process of depositing the germanium carbonitride barrier layer, the deposition temperature is 40°C, and the gas sources used are methylgermane (MMG), ammonia (NH 3) and hydrogen (H 2 ), wherein the flow rate of the MMG is 8sccm, the NH 3 / MMG ratio is 24, the H 2 The flow rate is 205sccm;

[0076] b. Fabrication of in...

Embodiment 3

[0081] A method for preparing an organic electroluminescent device, comprising the following steps:

[0082] (1) Preparation of luminescent functional layer and cathode layer on the anode substrate

[0083] With embodiment one;

[0084] (2) Prepare the encapsulation layer on the cathode layer

[0085] a. Fabrication of germanium carbonitride barrier layer:

[0086] Depositing a germanium carbonitride barrier layer on the surface of the cathode layer by plasma enhanced chemical vapor deposition (PECVD), the material of the germanium carbonitride barrier layer is germanium carbonitride, and the deposited germanium carbonitride barrier layer The thickness is 140nm. In the process of depositing the germanium carbonitride barrier layer, the deposition temperature is 50°C, and the gas sources used are methylgermane (MMG), ammonia (NH 3 ) and hydrogen (H 2 ), wherein the flow rate of the MMG is 6sccm, the NH 3 / MMG ratio is 21, the H 2 The flow rate is 210sccm;

[0087] b. Fab...

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Abstract

The invention provides an organic light emitting diode device. The organic light emitting diode device include an anode electric conduction substrate, a light-emitting functional layer, a cathode layer and an encapsulation layer which are stacked to one another sequentially; the encapsulation layer includes germanium carbonitride barrier layers and inorganic barrier layers which are stacked sequentially, wherein the germanium carbonitride barrier layers are made of a germanium carbonitride compound, and the inorganic barrier layers are made of B2O3:Cl, Al2O3:Cl, Ga2O3:Cl, In2O3:Cl and Tl2O3:Cl. According to the organic light emitting diode device, multi-layer material alternate encapsulation is adopted, so that the organic light emitting diode device has high density, and erosion of the organic light emitting diode device, which is caused by oxygen and water vapor, can be effectively reduced, and therefore, the service life of the organic light emitting diode device can be greatly prolonged. The invention also provides a preparation method of the organic light emitting diode device.

Description

technical field [0001] The invention relates to an organic electroluminescent device, in particular to an organic electroluminescent device and a preparation method thereof. Background technique [0002] Organic electroluminescent device (OLED) is a current-mode semiconductor light-emitting device based on organic materials. Its typical structure is that a multi-layer organic material film (hole injection layer, hole transport layer, light emitting layer, electron transport layer and electron injection layer) is sandwiched between the transparent anode and cathode layers. When a certain voltage is applied between the electrodes , the luminescent layer will emit light. In recent years, due to its low production cost, short response time, high luminance, wide viewing angle, low driving voltage, energy saving and environmental protection, organic electroluminescent devices have received extensive attention in the fields of full-color display, backlight and lighting. And it is...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01L51/52H01L51/54H01L51/56
CPCH10K50/8445H10K50/844H10K71/00
Inventor 周明杰钟铁涛王平张振华
Owner OCEANS KING LIGHTING SCI&TECH CO LTD
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