Preparation method of modified epoxy resin anticorrosive paint directly applied to rusty scales
A technology of epoxy resin and anti-corrosion coating, applied in the field of coatings, can solve the problems of poor adhesion and low anti-corrosion performance of water-based epoxy resin paint, and achieve the effect of good anti-corrosion performance and good adhesion
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Embodiment 1
[0024] The first step, the preparation of modified terpene resin: put 120g of organic solvent into the reaction kettle and heat to reflux state; 5g of 1-trifluoromethyl-1,3-butadiene, 10g of hydroxypropyl acrylate, styrene 15g and 10g of initiator are mixed evenly and dropped into the organic solvent; after the dropwise addition, the temperature is lowered to 70°C, 80g of terpene resin is added, and the reaction is carried out. The reaction time is 2 hours, and then filtered and dried in vacuum to obtain the modified terpene vinyl resin; the organic solvent is ethylene glycol, and the initiator is azobisisobutyronitrile;
[0025] Step 2. Preparation of modified filler: Dissolve 20g of alkyd resin in 120g of tetrahydrofuran as the first mixed solution; then take 15g of calcium silicate and 14g of potassium sulfate whiskers and disperse them in 150g of tetrahydrofuran as the second mixed solution liquid; the first mixed solution was mixed with the second mixed solution, stirred ...
Embodiment 2
[0030] The first step, the preparation of modified terpene resin: put 140g of organic solvent into the reaction kettle and heat to reflux state; 10g of 1-trifluoromethyl-1,3-butadiene, 20g of hydroxypropyl acrylate, styrene 20g and initiator 15g are mixed evenly and added dropwise to the organic solvent; after the dropwise addition, the temperature is lowered to 80°C, and 90g of terpene resin is added for reaction. The reaction time is 4 hours, and then filtered and dried in vacuum to obtain modified terpene vinyl resin; the organic solvent is ethylene glycol, and the initiator is azobisisobutyronitrile;
[0031] Step 2. Preparation of modified filler: Dissolve 30g of alkyd resin in 140g of tetrahydrofuran as the first mixed solution; then take 30g of calcium silicate and 24g of potassium sulfate whiskers and disperse them in 200g of tetrahydrofuran as the second mixed solution liquid; the first mixed solution was mixed with the second mixed solution, stirred for 3 hours under...
Embodiment 3
[0036] The first step, the preparation of modified terpene resin: put 130g of organic solvent into the reaction kettle and heat to reflux state; 7g of 1-trifluoromethyl-1,3-butadiene, 15g of hydroxypropyl acrylate, styrene 17g and initiator 12g were mixed evenly and dropped into the organic solvent; after the dropwise addition, the temperature was lowered to 75°C, and 85g of terpene resin was added to react. The reaction time was 3 hours, and then filtered and vacuum-dried to obtain modified terpene vinyl resin; the organic solvent is ethylene glycol, and the initiator is azobisisobutyronitrile;
[0037] Step 2. Preparation of modified filler: Dissolve 25g of alkyd resin in 130g of tetrahydrofuran as the first mixed solution; then take 18g of calcium silicate and 18g of potassium sulfate whiskers and disperse them in 170g of tetrahydrofuran as the second mixed solution liquid; the first mixed solution was mixed with the second mixed solution, stirred for 2 hours under the acti...
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