A kind of polylactic acid filter stick paper core and its manufacturing method
A manufacturing method and polylactic acid technology, which are applied in the directions of smoke oil filter element, single-component polyester rayon, melt spinning method, etc., can solve the problem of low rod yield, difficulty in cigarette tip fitting, and long filter rod curing time. and other problems, to achieve the effect of saving forest resources and petroleum resources, good biodegradability, and good recyclability
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Embodiment 1
[0030] Example 1: The polylactic acid filter plug paper core is made from the following raw materials by melt spinning, in parts by weight: the ratio of the levorotatory isomer: 95%; the melt index at 190°C under a load of 2.16 kg: 3.0g / 10 min; Intrinsic viscosity: 1.5; Melting point: 173°C, 100 parts of polylactic acid with an average molecular weight of 330,000, 15 parts of tapioca starch, 0.10% of the mass percentage of substituted aryl phosphate lithium salt NA-03 in polylactic acid, nanocarbonic acid The mass percentage of calcium in polylactic acid is: 0.15%.
[0031] Prepare as follows:
[0032] A. Raw material drying: vacuum dry the polylactic acid raw material at 75°C for 9 hours, so that the moisture content of the polylactic acid raw material is below 30ppm; Drying under temperature conditions for 5.5 hours; the dried polylactic acid and the nucleating agent are mixed uniformly to obtain a mixture;
[0033] B. Melt extrusion: Pour the mixture obtained in step A i...
Embodiment 2
[0041] Example 2: The polylactic acid filter plug paper core is prepared by melt spinning the following raw materials, in parts by weight: the ratio of the levorotatory isomer: 99%; the melt index at 190°C and a load of 2.16 kg: 2.0g / 10 min; Intrinsic viscosity: 1.7; Melting point: 165°C, 100 parts of polylactic acid with an average molecular weight of 330,000, 5 parts of a mixture of guar gum and potato starch, the mass percentage of substituted aryl phosphate lithium salt NA-03 in polylactic acid The mass percentage of nano-calcium carbonate in polylactic acid is 0.1%.
[0042] Prepare as follows:
[0043] A. Raw material drying: vacuum dry the polylactic acid raw material at 75°C for 7 hours, so that the moisture content of the polylactic acid raw material is below 30ppm; Drying under temperature conditions for 4 hours; the dried polylactic acid and the nucleating agent are mixed uniformly to obtain a mixture;
[0044] B. Melt extrusion: Pour the mixture obtained in step...
Embodiment 3
[0052] Example 3: The polylactic acid filter plug paper core is made from the following raw materials by melt spinning, in parts by weight: the ratio of the levorotatory isomer: 97%; the melt index at 190°C under a load of 2.16 kg: 4.0g / 10 min; Intrinsic viscosity: 1.0; Melting point: 170°C, 100 parts of polylactic acid with an average molecular weight of 330,000, 10 parts of tapioca starch, 0.30% of the mass percentage of substituted aryl phosphate lithium salt NA-03 in polylactic acid, nanocarbonic acid The mass percentage of calcium in polylactic acid is: 0.05%.
[0053] Prepare as follows:
[0054] A. Raw material drying: vacuum dry the polylactic acid raw material at 80°C for 8 hours, so that the moisture content of the polylactic acid raw material is below 30ppm; Drying under temperature conditions for 4 hours; the dried polylactic acid and the nucleating agent are mixed uniformly to obtain a mixture;
[0055] B. Melt extrusion: Pour the mixture obtained in step A int...
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