Preparation method of preserved flower for early CO warning
A technology for preserved flowers and fresh-cut flowers, which is applied in botany equipment and methods, preservation of plants, and material analysis through observation of the influence of chemical indicators, etc. It can solve the problems of lack of other functions, improve sensitivity, improve Dispersibility, anti-agglomeration effect
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[0026] The embodiment of the present invention discloses a method for preparing a permeate, comprising the following steps: mixing an acidic palladium salt solution, a solvent and polyvinylpyrrolidone (PVP), and stirring to obtain a first mixed solution; adding the orthosilicate solution dropwise In the first mixed solution, the mixture is statically aged after stirring to obtain a second mixed solution; phosphomolybdic acid and a preservative are added dropwise to the second mixed solution, and a permeate solution is obtained after stirring.
[0027] According to the present invention, the solvent is preferably a hydrophilic solvent with 2-8 carbon atoms; the orthosilicate is ethyl orthosilicate, methyl orthosilicate or propyl orthosilicate. The preferred dosage of raw materials in the permeate is as follows:
[0028]
[0029] More preferably, in the described permeate, the raw material consumption is as follows:
[0030]
[0031] More preferably, in the described perm...
Embodiment 1
[0061] The fresh cut flowers selected in this example are white gardenias. The preservative, ethyl p-hydroxybenzoate, was purchased from Zhengzhou Lvbo Chemical Products Co., Ltd.
[0062] A preserved flower with carbon monoxide warning function, the preparation method thereof is as follows:
[0063] 1) Fresh cut flowers are washed and arranged, placed in ethanol for dehydration for 24 hours to remove tissue fluid in cut flower cells, and a small amount of molecular sieve is added to the dehydrating agent to improve water removal efficiency;
[0064] 2) immerse the fresh cut flowers after dehydration in permeate at room temperature for 24 hours;
[0065] 3) Arrange the infiltrated fresh cut flowers, remove the surface liquid, and place them in a 50°C oven to dry slowly.
[0066] The preparation method of above-mentioned permeate is as follows:
[0067] 1) Dissolving 0.2g palladium chloride with 0.5ml mass concentration of 15% hydrochloric acid, adding 17.5ml ethanol, 8.7g p...
Embodiment 2
[0073] The fresh cut flowers selected in this embodiment are pink camellias. Potassium sorbate, a preservative, was purchased from Ningbo Wanglong Group Co., Ltd., and polyethylene glycol (PEG) was purchased from Sinopharm Reagent.
[0074] A preserved flower with carbon monoxide warning function, the preparation method thereof is as follows:
[0075] 1) fresh cut flowers are washed and arranged, placed in n-butanol for dehydration for 24 hours to remove tissue fluid in the cut flower cells, and anhydrous calcium chloride is added in the dehydrating agent to improve water removal efficiency;
[0076] 2) immerse the fresh cut flowers after dehydration in permeate at room temperature for 24 hours;
[0077] 3) Arrange the infiltrated fresh cut flowers, remove the surface liquid, and place them in a 55°C oven to dry slowly.
[0078] The preparation method of above-mentioned permeate is as follows:
[0079] 1) dissolve 0.5g palladium chloride with 0.8ml mass concentration of 20%...
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