Preparation method for electrode material used for supercapacitor and application of electrode material
A technology for supercapacitors and electrode materials, which is applied in the manufacture of hybrid capacitor electrodes and hybrid/electric double layer capacitors. It can solve problems such as nickel cobalt oxide that has not yet been discovered, and achieve excellent supercapacitor performance, good process repeatability, and stable product quality. Effect
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[0022] Example 1
[0023] Nickel cobaltate powder and sodium hypophosphite were placed in a tube furnace according to (Ni+Co) / P molar ratio of 1:5, under nitrogen atmosphere, with 1 o The heating rate of C / min is raised to 300 o C was calcined for 5 h, and then naturally cooled to room temperature to obtain the phosphorus-doped nickel cobalt oxide electrode material.
[0024] Note: (Ni+Co) / P molar ratio represents nickel cobaltate (NiCo 2 o 4 ) The molar ratio of the sum of the moles of Ni and Co contained in sodium hypophosphite to the P element contained in sodium hypophosphite, the same below.
Example Embodiment
[0025] Example 2
[0026] Nickel cobaltate powder and sodium hypophosphite are placed in a tube furnace according to (Ni+Co) / P molar ratio of 1:10, under nitrogen atmosphere, with 5 o The heating rate of C / min is raised to 400 o C was calcined for 2 h, and then naturally cooled to room temperature to obtain the phosphorus-doped nickel cobalt oxide electrode material.
Example Embodiment
[0027] Example 3
[0028] Nickel cobaltate powder and sodium hypophosphite are placed in a tube furnace according to (Ni+Co) / P molar ratio of 1:15, under nitrogen atmosphere, with 2 o The heating rate of C / min is raised to 350 o C was calcined for 3 h, and then naturally cooled to room temperature to obtain the phosphorus-doped nickel cobalt oxide electrode material.
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