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Processing method of pearl liquid, pearl ginseng liquid and pearl powder easily absorbed by human body

A processing method and technology of pearl powder, which can be used in pharmaceutical formulations, medical raw materials derived from molluscs, plant raw materials, etc., can solve the problems of expensive, polluting the environment, and reducing the hydrolysis effect

Inactive Publication Date: 2015-12-23
陈贵卿
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The methods for producing amino acids include hydrochloric acid hydrolysis, enzymatic hydrolysis, chemical synthesis and microbial fermentation, etc. Among them, hydrochloric acid hydrolysis has a long history, and its advantages are high production efficiency, cheap and easy-to-obtain raw materials, simple equipment, and can produce almost all amino acids at the same time. Types of amino acids, the disadvantages are: (1) It is difficult to separate and remove the hydrochloric acid after hydrolysis from the amino acid; the salt produced by neutralization is too salty as an amino acid solution, and it is very laborious and expensive to remove the salt by using ion exchange resins and other methods
(2) The hydrolysis odor produced by hydrochloric acid hydrolysis is difficult to eliminate and pollutes the environment
In fact, the amount of water added has little effect on the hydrolysis effect, but too thick or too thin a solution will reduce the hydrolysis effect
②This theory fails to reflect the relationship between the amount of hydrolyzed acid and the different nitrogen content of a certain type of hydrolyzate (Pearl oyster martensii, Triangle clam, scallop, prawn, various fish...)
③This theory fails to reflect the relationship between the amount of hydrolyzed acid and different types of protein (fish, meat, cartilage, tendon, hair, silk)

Method used

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  • Processing method of pearl liquid, pearl ginseng liquid and pearl powder easily absorbed by human body
  • Processing method of pearl liquid, pearl ginseng liquid and pearl powder easily absorbed by human body

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0178] Using a 5000mL conical flask, use citric acid to reflux and hydrolyze the keratin of 2000g of Martens pearl layer powder to produce "Martens pearl liquid, Martens pearl ginseng liquid and Martens pearl powder easily absorbed by the human body". Martens nacre powder contains 3.74% keratin.

[0179] Add 200g of Marshmallow pearl layer powder to hydrochloric acid such as [A] Formula (I): V 盐酸31% = M 马氏珍珠层粉 × 2.0605 = 200 × 2.0605 = 412.10mL, dissolve it until the pH is 6.4-6.6. Dilute to 3000mL, filter through filter paper, and discard the liquid. Then use filtered water to thoroughly wash the pearl keratin on the filter paper. Merge 10 parts of keratin of total 2000g Marshmallow's nacre powder.

[0180] Calculate the citric acid used for hydrolysis. from [B] In formula (Ⅱ-1), choose CC=3.0:

[0181] m 柠檬酸 = Raw material protein amount×3.0×2.1947=Raw protein amount×6.5841.

[0182] Martens nacre powder contains keratin 3.74%, M 壳蛋白 = M 马氏珍珠层 x 3.74% = 2000 x 3....

Embodiment 2

[0192] Using a 10L stainless steel reaction kettle, citric acid is used to hydrolyze 5000g of the horn shell protein of the spinosa pearl powder to produce "the spinosa pearl liquid, the spinosa pearl ginseng liquid and the human body can easily absorb the spinosa pearl powder". Triangle clam pearls contain 3.2% keratin.

[0193] Add 200g of spinosa clam pearl powder to hydrochloric acid such as [A] Formula (I): V 盐酸31% = M 冠蚌珍珠粉 × 2.0605 = 200 × 2.0605 = 412.10mL, dissolve it until the pH is 6.4-6.6. Dilute to 3000mL, filter through filter paper, and discard the solution. Then use filtered water to thoroughly wash the pearl keratin on the filter paper. Merge 25 parts of keratin shell proteins of 5000g Hypophylla mussel pearl powder in total.

[0194] Calculate the citric acid used for hydrolysis. from [B] In formula (Ⅱ-1), choose CC=2.8:

[0195] m 柠檬酸 = Raw protein amount×2.8×2.1947=Raw protein amount×6.1452.

[0196] Triangle clam pearls contain keratin 3.2%, M 壳...

Embodiment 3

[0207] Using a 10L stainless steel reactor, citric acid is used to hydrolyze 5000g of pleat clam pearl powder's keratin shell protein to produce "pleat clam pearl liquid, pleat clam pearl ginseng liquid and pleat clam pearl powder that can be easily absorbed by the human body". The pleated crown clam pearl contains 3.4% keratin.

[0208] Add 200g of pleated crown clam pearl powder to hydrochloric acid such as [A] Formula (I): V 盐酸31% = M 冠蚌珍珠粉 × 2.0605 = 200 × 2.0605 = 412.10mL, dissolve it until the pH is 6.4-6.6. Dilute to 3000mL, filter through filter paper, and discard the solution. Then use filtered water to thoroughly wash the pearl keratin on the filter paper. Merge 25 parts of keratin of total 5000g pleated crown clam pearl powder.

[0209] Calculate the citric acid used for hydrolysis. from [B] In formula (Ⅱ-1), choose CC=2.8:

[0210] m 柠檬酸 = Raw protein amount×2.8×2.1947=Raw protein amount×6.1452.

[0211] Pleated Crown Mussel Pearl Contains 3.4% Keratin, ...

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Abstract

The invention relates to a method of producing a pearl liquid, a pearl ginseng liquid and pearl powder easily absorbed by a human body by using pearl powder as a traditional Chinese medicinal material, which belongs to the technical field of production of the pearl liquid. The method comprises the following steps of firstly, preparing the pearl powder or pearl layer powder; secondly, dissolving with hydrochloric acid until the PH value reaches 6.4 to 6.6; thirdly, diluting, and filtering with filter paper to obtain conchiolin; fourthly, combining a plurality of parts of the conchiolin in the third step, and hydrolyzing the combined conchiolin with citric acid; fifthly, neutralizing until the PH value reaches 4.4 to 4.6 to obtain liquid A; sixthly, continuously neutralizing the liquid A until the PH value reaches 8, and precipitating the liquid for 3 to 4 hours; seventhly, filtering with filter paper to obtain liquid B and filter residues C; eighthly, adding the liquid B into a blending formula for conditioning according to the weight percentage of the preset volumetric yield of products; ninthly, filtering with filter paper to discharge the residues; tenthly, filling with the liquid and sterilizing to obtain a pearl liquid or pearl liquid ginseng liquid product; eleventhly, drying, crushing and packaging the filter residues C to obtain a calcium citrate supplementing agent; twelfthly, drying, crushing and packaging the liquid A.

Description

technical field [0001] The invention relates to a method for producing pearl liquid, pearl ginseng liquid and pearl powder easily absorbed by human body by using pearl powder and ginseng, which are traditional Chinese medicinal materials, and belongs to the technical field of pearl production. Background technique [0002] Pearl has been a precious traditional Chinese medicine since ancient times. It has the functions of calming the nerves, calming convulsions, strengthening the body, clearing away heat and detoxification, and improving eyesight. It has a good curative effect on the treatment of fever and convulsions in children, and bleeding in women. It is an important medicine in various departments of traditional Chinese medicine. Modern ESR technology has proved that pearls have the ability to scavenge superoxide anion free radicals and hydroxyl free radicals, and indeed have the effect of delaying aging. Pearls are also great for skin care. [0003] Ginseng function:...

Claims

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Application Information

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IPC IPC(8): A61K35/618A61K36/258
Inventor 陈贵卿陈俊豪
Owner 陈贵卿
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