Reduced graphene oxide and nano cerium oxide composite microwave absorbing material and preparation method thereof

A microwave absorbing material, nano-cerium oxide technology, applied in chemical instruments and methods, other chemical processes, etc., can solve the problems of thin, light, wide, strong, insufficient absorption strength, and narrow absorption frequency band of microwave absorbing materials. Achieve the effect of low cost, strong microwave absorption and wide absorption frequency

Active Publication Date: 2016-01-20
ANHUI UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The main disadvantages of traditional absorbing materials, such as ferrite, graphite, and ceramic materials, are high density, narrow absorption

Method used

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  • Reduced graphene oxide and nano cerium oxide composite microwave absorbing material and preparation method thereof
  • Reduced graphene oxide and nano cerium oxide composite microwave absorbing material and preparation method thereof
  • Reduced graphene oxide and nano cerium oxide composite microwave absorbing material and preparation method thereof

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Embodiment Construction

[0036] Below in conjunction with embodiment, the present invention will be further described.

[0037] The raw materials used and their sources are as follows:

[0038] (1) Natural graphite flakes: 325 mesh, purity ≥ 99%, Qingdao Huatai Durable Sealing Co., Ltd.

[0039] (2) Potassium permanganate: Purity AR, Sinopharm Chemical Reagent Co., Ltd.

[0040] (3) Hydrogen peroxide: Purity AR, Sinopharm Chemical Reagent Co., Ltd.

[0041] (4) Concentrated sulfuric acid: purity 95-98%, Tianjin Bodi Chemical Co., Ltd.

[0042] (5) Concentrated phosphoric acid: purity ≥ 85%, Tianjin Bodi Chemical Co., Ltd.

[0043] (6) Hydrochloric acid: purity 36-38%, Tianjin Bodi Chemical Co., Ltd.

[0044] (7) Ammonia water: 25% purity, Sinopharm Chemical Reagent Co., Ltd.

[0045] (8) Cerium nitrate hexahydrate: Purity AR, Aladdin's reagent

[0046] (9) Ethanol: Purity AR, Sinopharm Chemical Reagent Co., Ltd.

[0047] The specific operation steps for preparing the composite microwave absorbi...

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Abstract

The invention specifically relates to a reduced graphene oxide and nano cerium oxide composite microwave absorbing material and a preparation method thereof. The method comprises the following steps: preparing graphene oxide by using an improved Hummers method; mixing a graphene oxide aqueous solution with cerium nitrate in a mass ratio of 1:25, and adjusting the pH value to 10; and by using a one-step hydrothermal method, simultaneously generating nano cerium oxide and reducing the graphene oxide, so that a reduced graphene oxide and nano cerium oxide composite microwave absorbing material is obtained. The microwave absorption parameters of the composite material are tested by using a vector network analyzer, and the microwave reflection loss of the composite material is calculated by using a classical coaxial line theory. Results show that the reduced graphene oxide and nano cerium oxide composite microwave absorbing material has excellent microwave absorbing properties, high absorption strength and wide absorption band, and compared with nano cerium oxide, the microwave absorbing properties are greatly improved. Thus, the reduced graphene oxide and nano cerium oxide composite microwave absorbing material disclosed by the invention has broad application prospects, and is of great significance to the expansion of industrial application of rare earth oxides and the national defense construction.

Description

technical field [0001] The invention belongs to the technical field of functional materials, and in particular relates to a microwave absorbing material and a preparation method. Background technique [0002] With the development of military stealth technology and civilian anti-electromagnetic interference technology, microwave absorbing materials (referred to as absorbing materials) have become a research hotspot, and this type of material has gradually become an important branch of applied functional materials. Absorbing materials refer to a class of materials that can absorb and attenuate incident electromagnetic waves, convert their electromagnetic energy into heat or other forms of energy and dissipate them, or make electromagnetic waves disappear due to interference. [0003] The main disadvantages of traditional absorbing materials, such as ferrite, graphite, and ceramics, are high density, narrow absorption frequency band, and insufficient absorption strength, so the...

Claims

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Application Information

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IPC IPC(8): C09K3/00
Inventor 邢宏龙尹清刘振峰王磊
Owner ANHUI UNIV OF SCI & TECH
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