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A kind of preparation method of rare earth foam ceramic filter

A foamed ceramics and filter technology, applied in the field of preparation of rare earth foamed ceramics filters, can solve the problems of inability to meet the filtration requirements of metals and their alloy melts, uneven distribution of slurry, easy damage to polyurethane foam, etc., and avoid damage. , The effect of uniform paste adhesion and not easy to fall off

Active Publication Date: 2017-10-13
青岛铸英特陶科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, due to the limitation of pore size and flow rate, it is difficult to effectively filter and purify a large number of small inclusions and harmful impurities in metal and alloy melts, which makes the ceramic foam filter an important role in the filtration and purification technology of metal alloy melts. The promotion and application are greatly restricted, and it cannot meet the requirements of a large number of products that are demanding on the filtration of metals and their alloy melts
[0004] Chinese patent application 201010511259.4 discloses a method for preparing a yttrium oxide foam ceramic filter. The third foam ceramic filter blank is immersed in the component B ceramic slurry prepared in step 2, and taken out after immersion for 1 to 5 minutes to obtain The second impregnated body; then the second impregnated body is installed on the centrifuge, and the excess B component ceramic slurry in the second impregnated body is removed under the condition of centrifugal slurry rejection, so as to obtain the fourth foam ceramic filter green body; followed by drying After sintering and centrifugation, the slurry inside the embryo body is not evenly distributed, and the structure of polyurethane foam is easily damaged during the centrifugation process

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] The preparation method of the rare earth foam ceramic filter of the present embodiment comprises the following steps:

[0025] Step 1: Prepare Ceramic Slurry

[0026] Weigh the ceramic slurry components by the following parts by weight, including rare earth, ceramic aggregate and binder,

[0027] The rare earths include: 20 parts of cerium group rare earths, 15 parts of yttrium group rare earths;

[0028] The ceramic aggregate includes: 10 parts of silica fume, 20 parts of alumina, 30 parts of green silicon carbide, 50 parts of black silicon carbide, and 2 parts of fiber cotton;

[0029] The binder includes: 5 parts of polyvinyl alcohol, 5 parts of silica sol with a mass fraction of 40%;

[0030] Grind and sieve the rare earth to obtain rare earth powder below 300 mesh, mix the rare earth powder with ceramic aggregate and binder, add water and stir to obtain ceramic slurry A with a viscosity of 3000CP; add water and stir to obtain ceramic slurry The viscosity of mate...

Embodiment 3

[0052] The preparation method of the rare earth foam ceramic filter of the present embodiment comprises the following steps:

[0053] Step 1: Prepare Ceramic Slurry

[0054] Weigh the ceramic slurry components by the following parts by weight, including rare earth, ceramic aggregate and binder,

[0055] The rare earths include: 25 parts of cerium group rare earths, 12 parts of yttrium group rare earths;

[0056] The ceramic aggregate includes: 12 parts of silica fume, 18 parts of alumina, 25 parts of green silicon carbide, 45 parts of black silicon carbide, and 4 parts of fiber cotton;

[0057] The binder includes: 4 parts of polyvinyl alcohol, 8 parts of silica sol with a mass fraction of 40%;

[0058] Grind and sieve the rare earth to obtain rare earth powder below 300 mesh, mix the rare earth powder with ceramic aggregate and binder, add water and stir to obtain ceramic slurry A, the viscosity is 3500CP; add water and stir to obtain ceramic slurry The viscosity of materi...

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Abstract

The invention belongs to the technical field of a method for preparing a ceramic filter for casting, and relates to a method for preparing a rare earth foam ceramic filter, comprising the following steps: preparing a ceramic slurry, mixing rare earth, ceramic aggregate and a binder by weight , prepared into ceramic slurry A and ceramic slurry B; to prepare the embryo body, immerse the polyurethane foam carrier into the ceramic slurry A, fully absorb the ceramic slurry A, and roll it through the rolling forming equipment to obtain the embryo body, After drying the embryo body, the upper and lower surfaces and the core of the embryo body are strengthened twice by the glaze throwing equipment; the high temperature sintering, secondary strengthening and drying embryo body is put into a high temperature sintering furnace for sintering to obtain a rare earth foam ceramic filter; The sintering cycle is short and energy is saved; the damage of the embryo body is avoided, and the slurry adhesion is more uniform; the embryo body is strengthened by two glaze rejections, the internal slurry is evenly distributed, and it is not easy to fall off, and the properties of the product are stable after firing.

Description

technical field [0001] The invention belongs to the technical field of preparation methods of ceramic filters for casting, and in particular relates to a preparation method of rare earth foam ceramic filters. Background technique [0002] Rare earth elements refer to Group IIIB in the periodic table of elements. Rare earth elements have a unique arrangement of extranuclear electrons, which can effectively improve the performance of metals and alloy materials. In recent years, the research and development of new rare earth materials and their application in high-tech industries have been regarded as a standard for the development of a country's high-tech level. Studies have shown that the influence of rare earths on the structure of metals and their alloys is mainly reflected in three functions: (1) Purification: First, the affinity between rare earths and oxygen, sulfur, and hydrogen is very strong, forming a high melting point and thermal stability. Rare earth compounds wi...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B38/08C04B38/06C04B35/565C04B35/66
Inventor 田国庆冯培敏徐洪森
Owner 青岛铸英特陶科技有限公司