Modified cereal dietary fiber and preparation method thereof
A technology of dietary fiber and composite dietary fiber, which is applied in food science, food ingredients, and the functions of food ingredients, can solve the problems of low conversion efficiency and long time consumption, and achieve improved modification effects, higher purity, higher hydrolysis efficiency and Effect
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Embodiment 1
[0058] Embodiment 1 Utilizes enzymatic method to prepare modified composite dietary fiber
[0059] (1) Pretreatment: use rice bran ( as table 1 Said) is that after screening, removing impurities, pulverizing, and passing through a 60-mesh sieve, the raw material is placed in 6 times the volume of vegetable oil extraction solvent (for a commercially available vegetable oil extraction solvent, see People's Republic of China Country Standard, "Vegetable Oil Extraction Solvent", Standard No. GB16629-2008, published by China Standards Press, September 2008, Beijing), stirred and soaked for 2 hours, centrifuged, and the precipitate was air-dried to remove the solvent to obtain a degreased raw material.
[0060] (2) Separation and extraction: immerse the degreasing raw material in 10 times the volume of 0.3% NaOH solution by mass, stir and soak for 2 hours, then centrifuge, and remove the lower layer of precipitate. Immerse the lower sediment in 4 times the volume of water, adjust...
Embodiment 2
[0065] Embodiment 2 Utilizes mechanical force-compound enzyme method to prepare modified composite dietary fiber
[0066] The unmodified dietary fiber slurry prepared in Example 1 is soaked in the 0.08mol / L-0.1mol / L citric acid solution that the pH value of 3 times volume is 6, and the cellulase of 1.0u / g and Mix 50u / g xylanase evenly, and then grind in a ball mill (preferred parameters: ball milling medium is zirconia, filling rate 70%, radius 0.6-0.8mm, speed 500r / min) for 3 hours, and the temperature is controlled at 50°C or use a grinding disc refiner (preferred parameters: rotating speed 3000r / min, multi-element alloy grinding disc), grind and react for 2h at 50°C, obtain mechanical force-compound enzyme modified dietary fiber slurry after filtering, and mix the material Boil the slurry for 10min at 100°C, add 5 times the volume of 95% ethanol and let it stand for 2h, filter to obtain the dietary fiber slurry modified by mechanical force-composite enzyme, and dry the resu...
Embodiment 3
[0071] Embodiment 3 utilizes different methods to prepare water-soluble dietary fiber and water-insoluble dietary fiber
[0072] The enzyme-modified dietary fiber slurry prepared in Example 1 and Example 2 and the mechanical force-enzyme-modified dietary fiber slurry were heated at 100° C. for 10 min, centrifuged, and the precipitate was washed 3 times with hot water at 60° C. Collect the liquid (a) and the precipitate (b) respectively; the collected liquid (a) is concentrated under reduced pressure to 1 / 3 times the volume under the conditions of a pressure of 0.5 MPa (absolute pressure) and a temperature of 50°C. Add 5 times of volume of 95% ethanol in the liquid (a) after mixing, leave standstill for 5h after mixing, and filter; the filter residue is dried for 10min in a fluidized bed with a wind speed of 1m / s and a temperature of 80°C, and the water content is measured as 12.8%, crushed and passed through a 60-mesh sieve to obtain water-soluble dietary fiber (SDF);
[0073...
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