Super-capacitor high-conductive active carbon electrode manufacturing method
A supercapacitor and activated carbon technology, applied in the field of electrodes, can solve the problems of high equipment requirements, no contribution to specific capacity, and high production costs, and achieve the effects of improving internal structure, reducing equivalent internal resistance, and increasing conductivity
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Embodiment 1
[0019] A method for preparing a highly conductive activated carbon electrode for a supercapacitor includes the following steps:
[0020] 1) Preparation of graphene oxide / activated carbon mixture:
[0021] Add the activated carbon raw materials to the graphene oxide solution, the mass ratio of activated carbon to graphene oxide is 19:1, and react at 100°C for 1 hour under ultrasonic conditions. After the reaction, the mixture solution is obtained; the graphene oxide solution is the HUMMERS method Prepared with a concentration of 0.1%. The activated carbon raw material is a combination of wooden activated carbon and straw activated carbon.
[0022] 2) Preparation of graphene / activated carbon electrode:
[0023] Add the mixture solution obtained in 1) into a polytetrafluoroethylene container, and then add a catalyst, seal and react at 80°C for 10 hours, wash thoroughly with distilled water after the reaction, and dry at 80°C for 24 hours to obtain a highly conductive activated carbon el...
Embodiment 2
[0025] A method for preparing a highly conductive activated carbon electrode for a supercapacitor includes the following steps:
[0026] 1) Preparation of graphene oxide / activated carbon mixture:
[0027] Add the activated carbon raw material to the graphene oxide solution. The mass ratio of activated carbon to graphene oxide is 99:1. Under ultrasonic conditions, react at 80°C for 10 hours. After the reaction, the mixture solution is obtained; the graphene oxide solution is the HUMMERS method Prepared with a concentration of 3%. The activated carbon raw material is straw activated carbon.
[0028] 2) Preparation of graphene / activated carbon electrode:
[0029] Add the mixture solution obtained in 1) into a polytetrafluoroethylene container, and then add a catalyst, seal and react at 200°C for 1h, wash thoroughly with distilled water after the reaction, and dry at 80°C12 to obtain a highly conductive activated carbon electrode. The catalyst is anhydrous ethanol, and its addition amou...
Embodiment 3
[0031] A method for preparing a highly conductive activated carbon electrode for a supercapacitor includes the following steps:
[0032] 1) Preparation of graphene oxide / activated carbon mixture:
[0033] Add the activated carbon raw materials to the graphene oxide solution, the mass ratio of activated carbon to graphene oxide is 49:1, and react at 100°C for 6 hours under ultrasonic conditions. After the reaction, the mixture solution is obtained; the graphene oxide solution is the HUMMERS method Prepared with a concentration of 2%, the activated carbon raw material is wooden activated carbon.
[0034] 2) Preparation of graphene / activated carbon electrode:
[0035] Add the mixture solution obtained in 1) into a polytetrafluoroethylene container, and then add a catalyst, seal and react at 130°C for 6h, wash thoroughly with distilled water after the reaction, and dry at 100°C for 14h to obtain a highly conductive activated carbon electrode. The catalyst is ethanol, and its addition amo...
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