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A kind of preparation method of anti-mite fabric

An anti-mite and fabric technology, which is applied in the field of fabric manufacturing, can solve the problems of poor anti-mite durability of fabrics, high human toxicity and skin irritation, and complicated preparation process, and achieve improved anti-mite persistence, good drug slow-release effect, Small skin irritation effect

Active Publication Date: 2018-02-02
GUANGDONG XINHUI MEIDA NYLON
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] In existing patents and documents, when preparing anti-mite microcapsules, the wall materials used are mostly polymers such as urea-formaldehyde resin, methyl methacrylate, polyurethane, and polyamide. The preparation process is relatively complicated, and the used formaldehyde, acid chloride The toxicity is also relatively high, especially the strength of these organic wall materials is not high, so that the microcapsule drug is easily broken during the finishing process and the drug is released, failing to achieve the effect of protecting the drug and drug sustained release
Among the anti-mite agents currently used, many drugs are highly toxic to the human body and irritating to the skin, which is not conducive to environmental protection and human health.
In addition, although the anti-mite drug is prepared into microcapsules and finished on the fabric, the weak binding force between the microcapsule and the fabric makes it not resistant to washing, which eventually leads to poor anti-mite durability of the fabric, which is also a significant deficiency in the preparation of anti-mite fabrics by post-finishing methods.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0034] Preparation of anti-mite nylon 6 fabric

[0035] Step 1: CaCO 3 Preparation of anti-mite microcapsules coated with benzyl benzoate

[0036] Take 3g of sodium dodecylbenzenesulfonate and 2g of sodium oleate in a 500mL three-necked flask, add 100mL of distilled water, and dissolve them under stirring, then add 12g of benzyl benzoate into the three-necked flask, and stir at high speed until a stable After the emulsion of oil-in-water structure, the CaCl 2 The solution was slowly added to the emulsion and continued high-speed stirring for 3h, and finally the Na 2 CO 3 The solution was quickly added to a three-necked flask, stirred for 30 minutes, filtered, and the resulting microcapsules were washed three times with absolute ethanol and distilled water, and then vacuum-dried at 60°C for 24 hours to obtain CaCO 3 Coated with benzyl benzoate anti-mite microcapsules, the anti-mite microcapsules are spherical, with an average particle diameter of 3 μm, and the mass fraction...

Embodiment 2

[0046] Preparation of anti-mite cotton fabric

[0047] Step 1: CaCO 3 Preparation of coated eugenol anti-mite microcapsules

[0048] Take 2g of sodium laurate in a 500mL three-necked flask, add 100mL of distilled water, and dissolve it under stirring. CaCl 2 The solution was slowly added to the emulsion and continued high-speed stirring for 3h, and finally the Na 2 CO 3 The solution was quickly added to a three-necked flask, stirred for 30 minutes, filtered, and the resulting microcapsules were washed three times with absolute ethanol and distilled water, and then vacuum-dried at 60°C for 24 hours to obtain CaCO 3 Coated with eugenol anti-mite microcapsules, the anti-mite microcapsules are irregular spherical, with an average particle size of 18 μm, and the mass fraction of anti-mite drugs in the microcapsules is 30%.

[0049] Step 2: Containing CaCO 3 Preparation of anti-mite finishing solution coated with eugenol anti-mite microcapsules

[0050] CaCO as prepared in st...

Embodiment 3

[0058] Preparation of anti-mite polyester PET fabric

[0059] Step 1: CaCO 3 Preparation of anti-mite microcapsules coated with natural cypress essential oil and methyl eugenol

[0060] Take 4g of sodium lauryl sulfate in a 500mL three-necked flask, add 100mL of distilled water, and dissolve it under stirring, then add 5g of natural cypress essential oil and 4g of methyl eugenol into the three-necked flask, and stir at a high speed until a stable water bag is formed. After the emulsion of the oil structure, the CaCl 2 The solution was slowly added to the emulsion and continued high-speed stirring for 3h, and finally the Na 2 CO 3 The solution was quickly added to a three-necked flask, stirred for 30 minutes, filtered, and the resulting microcapsules were washed three times with absolute ethanol and distilled water, and then vacuum-dried at 60°C for 24 hours to obtain CaCO 3 Anti-mite microcapsules coated with natural cypress essential oil and methyl eugenol, the anti-mite ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Abstract

The invention relates to the technical field of fabric manufacturing, and discloses a method for preparing a mite-preventing fabric. The method comprises the steps that firstly, CaCO3 is adopted as a wall material, mite-preventing medicine is adopted as a core material, and mite-preventing microcapsules covered with CaCO3 are prepared; then mite-preventing finishing liquid is prepared, and contains the mite-preventing microcapsules and a waterborne polyurethane adhesive; finally, a fabric is soaked in the mite-preventing finishing liquid, and the mite-preventing fabric is obtained after drying. The mite-preventing microcapsules prepared from CaCO3 as the wall material are free of toxins and high in strength, the situation that the mite-preventing microcapsules are broken in the finishing process, and consequently the medicine is released and leaked is not prone to happen, and the good medicine slow release effect is achieved. When the mite-preventing finishing liquid is prepared, the waterborne polyurethane adhesive is added, the bonding force of the mite-preventing microcapsules and the fabric is improved, and therefore the mite-preventing durability of the fabric is remarkably improved. The selected mite-preventing medicine has the good mite resisting effect, and is low in toxicity to the human body and small in skin irritation. The method can be widely applied to various fabrics prepared from natural fibers or synthetic fibers.

Description

technical field [0001] The invention relates to the technical field of fabric manufacturing, in particular to a preparation method of an anti-mite fabric. Background technique [0002] Dust mites are tiny arthropods invisible to the naked eye. They are widely distributed in household textiles such as clothing, bedding, carpets, cushions, and plush toys, and mainly feed on human dander. Dust mites not only transmit bacteria and viruses themselves, but also their secretions, metabolites and dead insects are strong allergens, which can cause allergic rhinitis, infant eczema and chronic urticaria, and even cause bronchial urticaria in severe cases. diseases such as asthma. Since mites mainly live in household textiles, the preparation of anti-mite fibers and fabrics has gradually attracted the attention of academia and industry. [0003] At present, the preparation methods of anti-mite fiber fabrics mainly include three methods: fabric finishing method, functional fiber method...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D06M23/12D06M15/564
CPCD06M15/564D06M23/12
Inventor 宋明何卓胜刘芳陈欣魏文君谌继宗余彪李细林何经纬李沛荣汤友好
Owner GUANGDONG XINHUI MEIDA NYLON
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