Efficient preparation method of methyl salicylate
A high-efficiency technology for methyl salicylate, applied in the field of high-efficiency preparation of methyl salicylate, can solve problems such as affecting processing efficiency and product quality, poor recycling, and low product purity, so as to improve processing efficiency and product quality. The effect of quality, short production cycle time, and shortened reaction time
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[0025] Example 1
[0026] An efficient preparation method of methyl salicylate, the preparation method is as follows:
[0027] (1) Pretreatment
[0028] ① Put the diatomaceous earth into the acetic acid aqueous solution, the volume ratio of the diatomaceous earth and the acetic acid aqueous solution is 1:1.2, the pH of the acetic acid aqueous solution is 3, soak for 5 hours, then pour the acetic acid aqueous solution, and remove the diatom with water. The soil is washed to a pH of 6.5 to make modified diatomite;
[0029] ② Stir and mix the modified diatomaceous earth, hydroxypropyl cellulose, carboxymethyl cellulose and water to obtain the total material. The modified diatomaceous earth, hydroxypropyl cellulose, carboxymethyl cellulose and water The mass ratio is 10:3:1:4, and then put into the extruder to make strips, dry the strips for 30 minutes, and control the drying temperature to 60℃; then put the strips into the pelletizer to make pellets For particles with a diameter of 3mm...
Example Embodiment
[0040] Example 2
[0041] An efficient preparation method of methyl salicylate, the preparation method is as follows:
[0042] (1) Pretreatment
[0043] ① Put the diatomaceous earth into the acetic acid aqueous solution, the volume ratio of the diatomaceous earth to the acetic acid aqueous solution is 1:1.3, the pH of the acetic acid aqueous solution is 3.6, soak for 5.2 hours, then pour the acetic acid aqueous solution, and remove the diatom with water. The soil is washed to a pH of 6.8 to make modified diatomite;
[0044] ② Stir and mix the modified diatomaceous earth, hydroxypropyl cellulose, carboxymethyl cellulose and water to obtain the total material. The modified diatomaceous earth, hydroxypropyl cellulose, carboxymethyl cellulose and water The mass ratio is 10:3:1:4, and then it is put into the extruder to make the strips, and the strips are dried for 45 minutes, and the drying temperature is controlled to 73℃; then the strips are put into the granulator to make granules Fo...
Example Embodiment
[0055] Example 3
[0056] An efficient preparation method of methyl salicylate, the preparation method is as follows:
[0057] (1) Pretreatment
[0058] ① Put the diatomaceous earth into the acetic acid aqueous solution, the volume ratio of the diatomaceous earth to the acetic acid aqueous solution is 1:1.4, the pH of the acetic acid aqueous solution is 3.5, soak for 5.1 hours, then pour the acetic acid aqueous solution, and remove the diatom with water The soil is washed to a pH of 6.5 to make modified diatomite;
[0059] ② Stir and mix the modified diatomaceous earth, hydroxypropyl cellulose, carboxymethyl cellulose and water uniformly to obtain the total material. The mass ratio is 10:3:1:4, and then it is put into the extruder to make the strips, and the strips are dried for 42 minutes, and the drying temperature is controlled to 76℃; then the strips are put into the granulator to make granules For particles with a diameter of 5mm, put the particles into a muffle furnace at 500℃...
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