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Production method of Armeniaca sibirica biodiesel

A biodiesel and production method technology, applied in biofuels, chemical instruments and methods, petroleum industry, etc., can solve the problems of secondary pollution by-products, low catalytic efficiency, long reaction time, etc., to solve energy crisis and environmental pollution problems, high catalytic efficiency, and large reaction interface

Inactive Publication Date: 2016-06-15
GUANGXI KUONENGBA ENERGY TECH DEV CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the main method of preparing biodiesel from almonds is transesterification, but most of the traditional transesterification methods have low catalytic efficiency, low yield, deep color, easy deterioration, long reaction time, corrosion of equipment, complicated process, high reaction temperature, Disadvantages such as large energy consumption, easy to cause secondary pollution and by-product loss, and high cost

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] The magnetic nano-catalyst used in this embodiment is B 2 o 3 -Fe 3 o 4 . Its preparation method comprises the following steps:

[0023] a. Magnetic Fe 3 o 4 Preparation of nanospheres: FeCl with a mass ratio of 1:2 2 and FeCl 3 Dissolve in distilled water, feed in nitrogen, stir at 300r / min, add ammonia water drop by drop to pH 12; then control the temperature at 60°C and 100r / min, stir for 1h, cool to room temperature after reaction, use Magnetic adsorption to collect Fe 3 o 4 The particles were washed with distilled water until neutral, and dried in vacuum at 70°C for 3 hours to obtain magnetic Fe 3 o 4 Nano microspheres, the particle size of the microspheres is 58nm.

[0024] b.B 2 o 3 -Fe 3 o 4 Preparation of magnetic nano-catalyst: Add magnetic Fe3O4 nano-microspheres and boron nitrate solution with a mass ratio of 1:8 to an ultrasonic stirrer, then add ethanol with a mass ratio of 1:20 to the magnetic Fe3O4 nano-microspheres, at a speed of 300r / ...

Embodiment 2

[0031] The magnetic nano-catalyst used in this embodiment is ZrO 2 -Fe 3 o 4 . Its preparation method comprises the following steps:

[0032] a. Magnetic Fe 3 o 4 Preparation of nanospheres: FeCl with a mass ratio of 1:3 2 and FeCl 3Dissolve in distilled water, feed nitrogen, stir at 800r / min, add ammonia water drop by drop until the pH value is 11; then control the temperature to 78°C, rotate at 250r / min, stir for 1.5h, cool to room temperature after reaction, Fe collection by magnetite adsorption 3 o 4 The particles were washed with distilled water until neutral, and dried in vacuum at 80°C for 2 hours to obtain magnetic Fe 3 o 4 Nano microspheres, the particle size of the microspheres is 45nm.

[0033] b.ZrO 2 -Fe 3 o 4 Preparation of magnetic nanocatalysts: Add magnetic Fe3O4 nanospheres and zirconium nitrate solution with a mass ratio of 1:12 to an ultrasonic stirrer, and then add 3 o 4 Ethanol with a mass ratio of nanospheres of 1:25, at a speed of 400r / m...

Embodiment 3

[0039] The magnetic nano-catalyst used in this embodiment is Al 2 o 3 -Fe 3 o 4 . Its preparation method comprises the following steps:

[0040] a. Magnetic Fe 3 o 4 Preparation of nanospheres: FeCl with a mass ratio of 1:2.5 2 and FeCl 3 Dissolve in distilled water, feed nitrogen, stir at 500r / min, add ammonia water drop by drop to pH 12; then control the temperature at 70°C and 150r / min, stir for 1h, cool to room temperature after reaction, use Magnetic adsorption to collect Fe 3 o 4 The particles were washed with distilled water until neutral, and dried in vacuum at 75°C for 2 hours to obtain magnetic Fe 3 o 4 Nano microspheres, the particle size of the microspheres is 51nm.

[0041] b.Al 2 o 3 -Fe 3 o 4 Preparation of magnetic nanocatalysts: magnetic Fe with a mass ratio of 1:10 3 o 4 Nano-microspheres and aluminum sulfate solution were added to the ultrasonic stirrer, and then added with magnetic Fe 3 o 4 Add ethanol with a mass ratio of nanospheres of...

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Abstract

The invention discloses a production method of Armeniaca sibirica biodiesel. The method comprises the following steps: adding an active aluminum oxide adsorbent, and carrying out pretreatment for Armeniaca sibirica kernel oil in order to obtain pure Armeniaca sibirica kernel oil; adding pure Armeniaca sibirica kernel oil, methanol and a magnetic nano-catalyst according to a weight ratio 100:30-40:1.2-1.5 into a reaction vessel in order to carry out an esterification reaction; and separating a biodiesel crude product and carrying out purification in order to obtain the biodiesel. The magnetic nano-catalyst is introduced into the esterification reaction with high catalysis efficiency and substantial catalysis effects, reaction time is shortened, and yield of biodiesel is increased; on the other hand, the magnetic nano-catalyst can be conveniently and rapidly separated and recycled by means of an exterior magnetic field, and multitime cycle and utilization are carried out. The method also has the advantages of simple preparation technology, energy saving, environmental protection, short reaction time, high yield, high product purity, etc.; the method has good social efficiency, ecological benefits, and economic benefits; large scale and industrial production are easy to realize.

Description

technical field [0001] The invention relates to the technical field of biomass energy, in particular to a production method of apricot biodiesel. Background technique [0002] At present, the contradiction between the continuous growth of global oil demand and the depletion of fossil energy is becoming increasingly prominent, the energy supply situation is becoming more and more tense, the price of crude oil in the international market continues to rise sharply, and the diversification, renewable and clean energy has become the development of human society. It is an inevitable choice. The development of biomass energy is one of the directions to solve the global energy crisis. As a new alternative energy source, biodiesel is developing rapidly in countries all over the world. Biodiesel refers to oil crops such as soybeans, rapeseed, cotton, palm, etc., wild oil plants and engineering microalgae and other aquatic vegetable oils, animal fats, and catering waste oils, etc. Ren...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11C3/10C11C3/04C11B3/10C11B3/00C10L1/02B01J23/745
CPCB01J23/745C10L1/02C10L2290/542C11B3/001C11B3/10C11C3/04C11C3/10Y02E50/10
Inventor 梁杰锋杨云蒋小平李建华
Owner GUANGXI KUONENGBA ENERGY TECH DEV CO LTD
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