Textile auxiliary containing antibiotic constituents and preparation method thereof
A technology of textile auxiliaries and antibacterial ingredients, which is applied in the field of textile auxiliaries containing antibacterial ingredients and its preparation, and can solve the problems of large doses required, unsatisfactory textiles, and single action objects
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[0009] The preparation method of the textile auxiliary agent containing antibacterial composition comprises the following steps:
[0010] (1) Weigh each raw material according to parts by weight;
[0011] (2) Sodium dioctyl sulfosuccinate, polyvinylpyrrolidone, sodium dodecylsulfonate, isethionate, ethylene glycol salicylate, lupeyl palmitate, styrene maleic anhydride Mix the resins, add 10% NaOH solution to adjust the pH to 8.5, and stir at 7500-8500r / m for 6-10h;
[0012] (3) Heat the stirred mixture to 65-75°C, then add trichlorodiphenylurea, ethyl vanillin, and zinc oxide, conduct the first ultrasonic wave in an ultrasonic machine, and then add crosslinking agent, softening agent, carry out the second ultrasonic to obtain the finished product.
[0013] Preferably, in the step (3), the first ultrasonic power is 800w, and the ultrasonic time is 6-7h, and the second ultrasonic power is 950w, and the ultrasonic time is 4-5h.
[0014] Compared with the prior art, the present...
Embodiment 1
[0020] (1) Weigh 50 parts of dioctyl sodium sulfosuccinate, 45 parts of polyvinylpyrrolidone, 40 parts of sodium dodecyl sulfonate, 30 parts of isethionate, and ethylene glycol salicylate in parts by weight 30 parts, 25 parts of lupeyl palmitate, 25 parts of styrene maleic anhydride resin, 15 parts of trichlorodiphenylurea, 15 parts of ethyl vanillin, 5 parts of zinc oxide, 5 parts of polyisocyanate, silicone oil softener 5 copies;
[0021] (2) Sodium dioctyl sulfosuccinate, polyvinylpyrrolidone, sodium dodecylsulfonate, isethionate, ethylene glycol salicylate, lupeyl palmitate, styrene maleic anhydride Mix the resins, add 10% NaOH solution to adjust the pH to 8.5, and stir for 6 hours at 7500r / m;
[0022] (3) Heat the stirred mixture to 65°C, then add trichlorodiphenylurea, ethyl vanillin, and zinc oxide, and conduct the first ultrasonic wave in an ultrasonic machine with an ultrasonic power of 800w and an ultrasonic time of After 6 hours, polyisocyanate and silicone oil so...
Embodiment 2
[0025] (1) Weigh 55 parts of dioctyl sodium sulfosuccinate, 50 parts of polyvinylpyrrolidone, 45 parts of sodium dodecyl sulfonate, 35 parts of isethionate, and ethylene glycol salicylate in parts by weight 35 parts, 30 parts of lupeyl palmitate, 30 parts of styrene maleic anhydride resin, 20 parts of trichlorodiphenyl urea, 20 parts of ethyl vanillin, 8 parts of zinc oxide, polyether amino modified polysiloxane 8 parts of alkane, 8 parts of ester quaternary ammonium salt;
[0026] (2) Sodium dioctyl sulfosuccinate, polyvinylpyrrolidone, sodium dodecylsulfonate, isethionate, ethylene glycol salicylate, lupeyl palmitate, styrene maleic anhydride Mix the resins, add 10% NaOH solution to adjust the pH to 8.5, and stir for 8 hours at 8000r / m;
[0027] (3) Heat the stirred mixture to 70°C, then add trichlorodiphenylurea, ethyl vanillin, and zinc oxide, and conduct the first ultrasonic wave in an ultrasonic machine with an ultrasonic power of 800w and an ultrasonic time of After 6...
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