Semi-passing honeycomb ceramic grain filter and preparation method thereof
A particulate filter and honeycomb ceramic technology, applied in the field of material science, can solve the problems such as the semi-pass type honeycomb ceramic particulate filter that has not been reported, and achieve the effect of large removal rate, uniform distribution of micropores, and energy saving.
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[0023] Example 1:
[0024] First prepare 27 parts of kaolin with an average particle size of 3 μm (parts by mass, the same below), 39 parts of flaky talc with an average particle size of 13 μm, 16 parts of alumina with an average particle size of 4 μm, and 8 parts of fused silica powder with an average particle size of 8 μm , 12 parts of methyl methacrylate pore-forming agent particles with an average particle size of 35 μm, and 6 parts of hydroxypropyl methylcellulose, 32 parts of water and other raw materials as the water-soluble binder used.
[0025] Then the prepared raw materials are fully mechanically mixed and kneaded to make them uniform, and then degassed and refined for 3 times under the vacuum degree of 95KPa, and aged for 24 hours to obtain plastic mud.
[0026] The plastic mud is made into a cylindrical wet body through a die mechanical extruder. The cross section of the die is circular, the outer diameter is 267mm, and the hole density is 300 holes / square inch; t...
Example Embodiment
[0031] Example 2:
[0032] The addition amount of the pore-forming agent particle methyl methacrylate in Example 1 was reduced from 12 parts to 6 parts, and the addition amount of other raw materials and the preparation process were the same as in Example 1, and the obtained sample detection results were:
[0033] The appearance size, wall thickness, etc. are the same as those of the sample in Example 1, but the porosity is 45%, the average pore diameter of the micropores is 9 μm, the wall thickness is 0.3 mm, the compressive strength is greater than 19 MPa, and the thermal expansion coefficient is 1.0 × 10 -6 / ℃, thermal shock resistance 550℃, removal rate of particulate matter in flue gas is 50%. It shows that reducing the addition amount of methyl methacrylate has a certain decrease in the porosity and average pore diameter of the sample, and also causes a decrease in the particle filtration rate.
Example Embodiment
[0034] Example 3:
[0035] The pore-forming agent in Example 1 is replaced by starch with methyl methacrylate, and its add-on, other raw materials and add-ons, and preparation techniques are the same as in Example 1, and the obtained sample detection results are:
[0036] The appearance size and wall thickness are the same as those of the sample in Example 1, but the porosity is 50%, the average pore diameter of micropores is 11 μm, the wall thickness is 0.3 mm, the compressive strength is 19 MPa, and the thermal expansion coefficient is 1.0×10 -6 / ℃, thermal shock resistance 560℃, removal rate of particulate matter in flue gas 55%. Compared with the measurement results of the sample in Example 1, it is shown that the effect of using starch as a pore-forming agent is not as good as that of methyl methacrylate.
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