Preparation method and application of single-layer mica sheet and nanoporous electronic device thereof
A technology of electronic devices and mica sheets, which is applied in the direction of chemical instruments and methods, biochemical equipment and methods, instruments, etc., can solve the problems of force to destroy the mica layer, long preparation time, and high cost, so as to avoid shrinkage effect and improve Effects of sequencing speed, no reagent cost
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[0043] (1) Preparation of single-layer mica: Dissolve 5g of potassium hydroxide (KOH) in 50mL of organic solvent tetrahydrofuran (THF), stir at room temperature for 24h; add 1g of sericite powder to the above solution, place in a stainless steel pot, 250 Treat at ℃ for 72 hours, stir with a magnetic stirrer; use microwave radiation to process the solution (60Hz, 1000W) for 5-8min, and centrifuge at 10000rpm for 5min to precipitate mica flakes; resuspend the mica flakes in 1% hydrochloric acid (HCl) solution, ultrasonicate 10h, rinse repeatedly with distilled water until the pH value is 7.0; carry out density gradient centrifugation, first centrifuge at 2000rpm for 5min, discard the precipitate, remove the incompletely dissociated mica particles, then centrifuge at 6000rpm for 5min, discard the supernatant, remove the mica fragments, and the precipitate weighs Suspended in deionized water to obtain a monolayer mica suspension.
[0044] (2) Preparation of supporting substrate: S...
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