Sealing thermo-curing resin material
A thermosetting, resin material technology, used in the field of electronic components, packaging material preparation, can solve the problems of low tensile strength, dielectric constant, dielectric loss, etc., achieve good sealing effect, excellent comprehensive performance, wide range The effect of the application foreground
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[0029] The preparation method of the thermosetting resin material for sealing comprises the following steps:
[0030] S1: Combine 2,2'-[(1-methylethylene)bis(4,1-phenylenecarbaldehyde)]dioxirane and methylene-bis(1,3-benzenediol) - Tetraglycidyl ether, silicone resin modified tung oil alkyd resin, o-cresol novolac epoxy resin A, dioctyl phthalate, ethylene propylene rubber, polysiloxane mixed, at a temperature of 240-255 ° C, rotating speed Stir at 300-400r / min for 6-8min to prepare mixture A;
[0031] S2: Under nitrogen protection, add oleyl amino acid potassium, sodium metasilicate, paraffin, carbon fiber, polymaleimide, phthalic acid, silicon dioxide, N-2 to the mixture A prepared in step 1 -(aminoethyl)-3-aminopropylmethyldimethoxysilane coupling agent, modified polyacrylate compatibilizer, 2,2'-methylene-bis-(4-ethyl-6 - tert-butylphenol), anhydrite stabilizer, DCP bridging agent, acrylate regulator, azobisisobutyric acid (ethylene glycol acrylate) ester initiator, di-t...
Embodiment 1
[0036] A thermosetting resin material for sealing, made of the following raw materials in units of weight: 2,2'-[(1-methylethylene)bis(4,1-phenylenecarbaldehyde)]bicyclo Oxyethane and methylene-bis(1,3-benzenediol)-tetraglycidyl ether 220 parts, silicone resin modified tung oil alkyd resin 65 parts, o-cresol novolac epoxy resin A50 parts, phthalic acid 25 parts of dioctyl ester, 42 parts of ethylene propylene rubber, 27 parts of polysiloxane, 23 parts of oleyl amino acid potassium, 19 parts of sodium metasilicate, 30 parts of paraffin wax, 20 parts of carbon fiber, 17 parts of polymaleimide, 20 parts of phthalic acid, 20 parts of silicon dioxide, 4 parts of N-2-(aminoethyl)-3-aminopropylmethyldimethoxysilane coupling agent, 4 parts of modified polyacrylate compatibilizer 2,2'-methylene-bis-(4-ethyl-6-tert-butylphenol) 1.2 parts, anhydrite stabilizer 0.9 parts, DCP bridging agent 0.9 parts, acrylate regulator 0.8 parts 0.5 parts, 0.5 parts of 701 powder strengthening agent, 0....
Embodiment 2
[0046] A thermosetting resin material for sealing, 2,2'-[(1-methylethylene)bis(4,1-phenylenecarbaldehyde)]dioxirane and methylene Base-bis(1,3-benzenediol)-tetraglycidyl ether 168 parts, silicone resin modified tung oil alkyd resin 54 parts, o-cresol novolac epoxy resin A44 parts, dioctyl phthalate 25 parts, 35 parts of ethylene propylene rubber, 22 parts of polysiloxane, 20 parts of potassium oleyl amino acid, 16 parts of sodium metasilicate, 26 parts of paraffin, 14 parts of carbon fiber, 15 parts of polymaleimide, 14 parts of phthalic acid , 14 parts of silicon dioxide, 3 parts of N-2-(aminoethyl)-3-aminopropylmethyldimethoxysilane coupling agent, 3 parts of modified polyacrylate compatibilizer, 2,2' -Methylene-bis-(4-ethyl-6-tert-butylphenol) 0.8 parts, anhydrous gypsum stabilizer 0.6 parts, DCP bridging agent 0.6 parts, acrylate regulator 0.5 parts, 701 powder strengthening agent 0.4 parts, 0.4 parts of polyaluminum chloride coagulant, 0.5 parts of styrene-butadiene ther...
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