E-cigarette nicotine liquid and preparation method thereof
A technology of e-cigarette liquid and tobacco leaves, which is applied in the fields of tobacco, tobacco processing, application, etc., can solve the problems of low nicotine content, green gas, and change the style characteristics of e-cigarette liquid, and achieve a simple preparation process and easy operation Effect
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Embodiment 1
[0032] The electronic cigarette liquid in this embodiment is composed of the following components in mass percentage: 3% high nicotine tobacco extract, 5% tobacco essence, 20% glycerin, 10% deionized water, and the balance is propylene glycol.
[0033] The preparation steps of high nicotine tobacco extract are as follows:
[0034] 1) Pretreatment: Weigh 1 kg of flue-cured tobacco raw material, place the raw material in a SY-III-A experimental tobacco processor, spray commercially available ammonia water with 8% raw material mass, and place it in a sealed place for 12 hours to fully absorb the tobacco leaves, then heat Bake at 70°C for 4 hours;
[0035] 2) Grinding the baked material to 10 meshes, and rolling it through a roller-type wall breaking machine for 3 times to obtain powder;
[0036] Subcritical extraction: add butane (mass ratio 1:8) to the powder, extract at a temperature of 25°C and saturated vapor pressure for 2 hours to obtain an extract;
[0037] The extract i...
Embodiment 2
[0043] The e-cigarette liquid in this embodiment is composed of the following components in mass percentage: 0.1% high nicotine tobacco extract, 2% tobacco essence, 10% glycerin, 5% deionized water, and the balance is propylene glycol.
[0044] The preparation steps of high nicotine tobacco extract are as follows:
[0045] 1) Pretreatment: Weigh 1 kg of flue-cured tobacco raw material, place the raw material in a SY-III-A type experimental tobacco processor, spray a saturated aqueous solution of histidine with 20% raw material quality, seal and place for 6 hours, so that the tobacco leaves can be fully absorbed, Then heat to 40°C and bake for 2h;
[0046] 2) Pulverize the baked material to 100 mesh, and roll it through a rolling-type wall breaking machine for 3 times to obtain powder;
[0047] Subcritical extraction: add dimethyl ether (mass ratio 1:12) to the powder, extract at a temperature of 45°C and saturated vapor pressure for 0.5h to obtain an extract;
[0048] The ex...
Embodiment 3
[0054] The e-cigarette liquid in this embodiment is composed of the following components in mass percentage: 1.5% of high-nicotine tobacco extract, 3% of tobacco essence, 15% of glycerin, 8% of water, and the balance is propylene glycol;
[0055] The preparation steps of high nicotine tobacco extract are as follows:
[0056] 1) Pretreatment: Weigh 1 kg of flue-cured tobacco raw material, place the raw material in a SY-III-A type experimental tobacco processor, spray 25% lysine saturated aqueous solution of the raw material quality, seal and place for 10 hours, so that the tobacco leaves can be fully absorbed, Then heat to 60°C and bake for 5h;
[0057] 2) Pulverize the baked material to 50 mesh, and roll it through a rolling-type wall breaking machine for 3 times to obtain powder;
[0058] Subcritical extraction: add butane (mass ratio 1:10) to the powder, extract at a temperature of 45°C and saturated vapor pressure for 1.5 hours to obtain an extract;
[0059] The extract i...
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