Nitrogen and phosphorus co-doped composite material, preparation method and application and capacitor electrode
A technology of capacitor electrodes and composite materials, which is used in the manufacture of hybrid capacitor electrodes and hybrid/electric double layer capacitors, etc., can solve the problems of low energy density, limited application and industrialized production, high current charge-discharge difference, etc., and achieve excellent electrical performance. , the effect of huge application potential and industrial value
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Embodiment 1
[0061] S1: Mix egg yolk, deionized water and potassium ferricyanide, and ultrasonicate for 30 minutes; wherein, the mass ratio of egg yolk, deionized water and potassium ferricyanide is 1:10:5;
[0062] S2: after the end of ultrasound, dissolve for 30 minutes while stirring;
[0063] S3: After stirring and dissolving, fully dry at 120°C for 19 hours to obtain a crude product;
[0064] S4: The crude product was calcined at 1000° C. for 2 hours under the protection of nitrogen gas to obtain a nitrogen-phosphorus co-doped carbon nanotube-wrapped iron compound composite material, which was named M1.
Embodiment 2-3
[0065] Embodiment 2-3: the investigation of high temperature treatment temperature in step S4
[0066] Except that the high-temperature calcination treatment temperature in step S4 was replaced by 900°C and 1100°C respectively, other operations remained unchanged, so that Example 1 was repeated, and thus Examples 2-3 were carried out in sequence, and the obtained composite materials were named in sequence for M2 and M3.
Embodiment 4
[0067] Embodiment 4: the investigation when not adding iron compound in step S1
[0068] Except that the potassium ferricyanide in step S1 was omitted, other operations were kept unchanged, so that Example 1 was repeated to obtain Example 4, and the obtained material was named M4.
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Abstract
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