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Method for extracting ginger gingerol

A technology of gingerol and gingerol, which is applied in the field of biological raw material extraction, can solve the problems of poor product quality, increased solvent loss, and more damage to active ingredients, and achieve a large amount of precipitation, fast separation speed, and reduced cost effect

Active Publication Date: 2019-05-10
济南巨鼎食品有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] 1) The water boiling method takes a long time and consumes more energy. Due to prolonged heating, the active ingredients are more damaged, so the product quality is poor;
[0005] 2) Column chromatography is difficult to be used in mass production due to the limitation of eluent and elution volume;
[0006] 3) The organic solvent extraction method extracts gingerol according to the principle of similar miscibility, because the solubility of the solvent is limited, in order to improve the extraction rate, the main method is to increase the amount of solvent. As the amount of solvent increases, the consumption also increases , the cost will inevitably rise, so the economic benefits often show negative growth, and it cannot be put into production, and can only stay in the experimental stage of the laboratory; such as absolute ethanol to extract gingerol, the extraction rate of gingerol increases with the amount of absolute ethanol increase and slowly improve, so the extraction rate of gingerol often increases, but at the same time, the loss of absolute ethanol also increases significantly. In addition, the process is longer, so the energy consumption is more, the solvent loss increases, and the production cost rises. The final economic benefits usually show negative growth, and cannot be put into production, but can only stay in the laboratory;
[0007] 4) Physical methods can be divided into three types: freezing method, microwave method and ultrasonic method according to different processing methods; these three methods can play a certain auxiliary role in extraction, but at the same time increase energy consumption and production costs

Method used

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  • Method for extracting ginger gingerol

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] like figure 1 Shown: the method for extracting ginger gingerol 1, comprises the following steps:

[0032] 1) First wash 100g of ginger, weigh the ginger and water in a weight ratio of 1:2;

[0033] 2) Grinding the ginger with water, squeezing the ginger residue to obtain ginger juice with a concentration of 50%;

[0034] 3) regulate the pH value of ginger juice to 5.5, then add sodium chloride solution in ginger juice, mix to obtain mixed solution, wherein, the volume of sodium chloride solution is 20% of the volume weight of ginger juice; The score is 60%.

[0035] 4) Slowly heat the mixed solution, stop heating until the mixed solution boils, let it stand for precipitation, and filter to obtain the precipitate, which is the crude gingerol;

[0036] 5) Add edible alcohol to the crude gingerol, extract 3 times, combine the extracts, distill under reduced pressure, recover to obtain gingerol 1, and the weight ratio of crude gingerol to edible alcohol is 1:20.

[0037...

Embodiment 2

[0039] The method for extracting gingerol 2 comprises the following steps:

[0040] 1) First, wash the ginger, and weigh the ginger and water in a weight ratio of 1:1;

[0041] 2) Grinding the ginger with water, squeezing the ginger residue to obtain ginger juice with a concentration of 40%;

[0042] 3) regulate the pH value of ginger juice to 5.0, then add sodium chloride salt solution in ginger juice, mix to obtain mixed liquor, wherein, the weight of sodium chloride solution is 10% of ginger juice weight; The quality score is 80%.

[0043] 4) Slowly heat the mixed solution, stop heating until the mixed solution boils, let it stand for precipitation, and filter to obtain the precipitate, which is the crude gingerol;

[0044] 5) Add edible alcohol to the crude gingerol, extract 3 times, combine the extracts, distill under reduced pressure, recover to obtain gingerol 2, and the weight ratio of the crude gingerol to the organic solvent is 1:40.

[0045] 6) the benefit of thi...

Embodiment 3

[0047] The method for extracting gingerol 3 comprises the following steps:

[0048] 1) First, wash the ginger, and weigh the ginger and water in a weight ratio of 1:3;

[0049]2) Grinding the ginger with water, squeezing the ginger residue to obtain ginger juice with a concentration of 30% to 50%;

[0050] 3) adjust the pH value of the ginger juice to 6.0, then add the magnesium chloride solution to the ginger juice, and mix to obtain a mixed solution, wherein the weight of the magnesium chloride solution is 30% of the weight of the ginger juice; the mass fraction of the magnesium chloride solution is 500%.

[0051] 4) Slowly heat the mixed solution, stop heating until the mixed solution boils, let it stand for precipitation, and filter to obtain the precipitate, which is the crude gingerol;

[0052] 5) Add edible alcohol to the crude gingerol, extract twice, combine the extracts, distill under reduced pressure, recover to obtain gingerol 3, and the weight ratio of the crude ...

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PUM

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Abstract

The invention discloses a method for extracting ginger gingerol. The method comprises the following steps: adding water into ginger for grinding, and squeezing to separate ginger dregs to obtain ginger juice; adjusting the pH value of the ginger juice to 4 to 6, then adding a light metal salt solution into the ginger juice, carrying out uniform mixing to obtain a mixed solution, slowly heating the mixed solution, stopping heating till the mixed solution is boiled, standing and settling, and filtering to obtain precipitates which are gingerol coarse products; and adding an organic solvent into the gingerol coarse products, carrying out extraction for 1 to 3 times, mixing extracting solutions, carrying out decompression distillation, and carrying out recycling to obtain the gingerol. According to the method disclosed by the invention, the gingerol coarse products are separated by settling; the separation speed is high, and the quantity of the precipitates is large; furthermore, the quality of the precipitates is high, and the precipitates still can keep the original active state; and when the gingerol coarse products are returned into the ginger juice, the ginger juice still has the original taste. Compared with the conventional extraction method, the method has the advantage that the use amount is reduced by 80 percent or above.

Description

technical field [0001] The invention relates to the field of extraction of biological raw materials, in particular to a method for extracting gingerol from ginger. Background technique [0002] Ginger is the fresh rhizome of the perennial herb ginger (Zingiber officinale Roscoe) of the monocot Zingiberaceae. Ginger is a perennial herb that is cultivated as an annual. The rhizome is hypertrophic and contains volatile oil. The rhizome of ginger (dried ginger) has a pungent taste and is used as a vegetable, spice and medicine. Warm in nature, its unique "gingerol" can stimulate the gastrointestinal mucosa, make the gastrointestinal congestion, and enhance digestion. It can effectively treat abdominal distension, abdominal pain, diarrhea, vomiting, etc. caused by eating too much cold and cool food. Oxidative, anti-allergic, and cholesterol-lowering effects in blood and liver. [0003] At present, there are many methods for extracting gingerol from ginger, mainly including wate...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C07C49/255C07C45/79C07C45/78
CPCC07C45/78C07C45/79C07C49/255
Inventor 仇小燕李安明李长春姜益泉王立华田春元戴余军袁玲张正林张林张福云况启生
Owner 济南巨鼎食品有限公司
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