Method for extracting ginger gingerol
A technology of gingerol and gingerol, which is applied in the field of biological raw material extraction, can solve the problems of poor product quality, increased solvent loss, and more damage to active ingredients, and achieve a large amount of precipitation, fast separation speed, and reduced cost effect
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Embodiment 1
[0031] like figure 1 Shown: the method for extracting ginger gingerol 1, comprises the following steps:
[0032] 1) First wash 100g of ginger, weigh the ginger and water in a weight ratio of 1:2;
[0033] 2) Grinding the ginger with water, squeezing the ginger residue to obtain ginger juice with a concentration of 50%;
[0034] 3) regulate the pH value of ginger juice to 5.5, then add sodium chloride solution in ginger juice, mix to obtain mixed solution, wherein, the volume of sodium chloride solution is 20% of the volume weight of ginger juice; The score is 60%.
[0035] 4) Slowly heat the mixed solution, stop heating until the mixed solution boils, let it stand for precipitation, and filter to obtain the precipitate, which is the crude gingerol;
[0036] 5) Add edible alcohol to the crude gingerol, extract 3 times, combine the extracts, distill under reduced pressure, recover to obtain gingerol 1, and the weight ratio of crude gingerol to edible alcohol is 1:20.
[0037...
Embodiment 2
[0039] The method for extracting gingerol 2 comprises the following steps:
[0040] 1) First, wash the ginger, and weigh the ginger and water in a weight ratio of 1:1;
[0041] 2) Grinding the ginger with water, squeezing the ginger residue to obtain ginger juice with a concentration of 40%;
[0042] 3) regulate the pH value of ginger juice to 5.0, then add sodium chloride salt solution in ginger juice, mix to obtain mixed liquor, wherein, the weight of sodium chloride solution is 10% of ginger juice weight; The quality score is 80%.
[0043] 4) Slowly heat the mixed solution, stop heating until the mixed solution boils, let it stand for precipitation, and filter to obtain the precipitate, which is the crude gingerol;
[0044] 5) Add edible alcohol to the crude gingerol, extract 3 times, combine the extracts, distill under reduced pressure, recover to obtain gingerol 2, and the weight ratio of the crude gingerol to the organic solvent is 1:40.
[0045] 6) the benefit of thi...
Embodiment 3
[0047] The method for extracting gingerol 3 comprises the following steps:
[0048] 1) First, wash the ginger, and weigh the ginger and water in a weight ratio of 1:3;
[0049]2) Grinding the ginger with water, squeezing the ginger residue to obtain ginger juice with a concentration of 30% to 50%;
[0050] 3) adjust the pH value of the ginger juice to 6.0, then add the magnesium chloride solution to the ginger juice, and mix to obtain a mixed solution, wherein the weight of the magnesium chloride solution is 30% of the weight of the ginger juice; the mass fraction of the magnesium chloride solution is 500%.
[0051] 4) Slowly heat the mixed solution, stop heating until the mixed solution boils, let it stand for precipitation, and filter to obtain the precipitate, which is the crude gingerol;
[0052] 5) Add edible alcohol to the crude gingerol, extract twice, combine the extracts, distill under reduced pressure, recover to obtain gingerol 3, and the weight ratio of the crude ...
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