Preparation method of high permeability fast water injection well scale remover
A technology for water injection wells and descaling agents, which is applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve the problems of low construction labor intensity, short construction time, and low corrosion, and achieve low construction labor intensity. Short time, good treatment effect
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example 1
[0021] Weigh 100g of ethyl silicate, 50g of butanol, 40g of deionized water and 32g of phosphotungstic acid into a three-necked flask, put them in a water bath, heat to reflux, pour them into a glass beaker after reflux for 3 hours, and put them in a water bath In the pot, heat up to 60°C, keep stirring for 3 hours, put it in an oven, dry at 100°C for 6 hours, put it into a grinder after drying, and pass through a 100-mesh sieve to obtain catalyst powder; Add 6g of glucosamine hydrochloride and 250mL of deionized water to the four-necked flask of the tube, thermometer and water separator in sequence, adjust the pH value to 7.0 with a mass fraction of 20% sodium hydroxide solution, and then add 2.5g of the above-mentioned Catalyst powder, stir evenly, put it into a water bath, heat up to 35°C, heat and stir for 5 hours, and use 20% sodium hydroxide solution to keep the pH of the reaction solution at 7.0 during the reaction; filter to obtain Filtrate, adjust the pH of the filtra...
example 2
[0024]Weigh 150g of ethyl silicate, 80g of butanol, 45g of deionized water and 33g of phosphotungstic acid into a three-necked flask, put them in a water bath, heat to reflux, pour them into a glass beaker after reflux for 4 hours, and put them in a water bath In the pot, heat up to 65°C, keep stirring for 4 hours, put it in an oven, dry at 105°C for 7 hours, put it into a grinder after drying, and pass through a 110-mesh sieve to obtain catalyst powder; Add 7g of glucosamine hydrochloride and 275mL of deionized water to the four-necked flask of the tube, thermometer and water separator in sequence, adjust the pH value to 7.0 with a 20% mass fraction of sodium hydroxide solution, and then add 2.7g of the above-mentioned Put the catalyst powder into a water bath after stirring evenly, raise the temperature to 37°C, and keep stirring for 5.5 hours. During the reaction, use 20% sodium hydroxide solution to keep the pH value of the reaction solution at 7.0; filter after the above r...
example 3
[0027] Weigh 200g of ethyl silicate, 100g of butanol, 50g of deionized water and 35g of phosphotungstic acid into a three-necked flask, put them in a water bath, heat to reflux, pour them into a glass beaker after reflux for 5 hours, and put them in a water bath In the pot, heat up to 70°C, keep warm and stir for 5 hours, put it in an oven, dry at 110°C for 8 hours, put it into a grinder after drying, and pass it through a 120-mesh sieve to obtain catalyst powder; Add 8g of glucosamine hydrochloride and 300mL of deionized water to the four-necked flask of the tube, thermometer and water separator in sequence, adjust the pH value to 7.0 with a 20% mass fraction of sodium hydroxide solution, and then add 3.0g of the above-mentioned Catalyst powder, stir evenly, put it into a water bath, heat up to 40°C, heat and stir for 6 hours, and use 20% sodium hydroxide solution to keep the pH of the reaction solution at 7.0 during the reaction; filter to obtain Filtrate, adjust the pH of t...
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