Method for preparing B4C fiber through in-situ combustion
An in-situ combustion and fiber technology, applied in the field of ceramic fibers, can solve the problems of low product purity, low raw material utilization rate, difficult control of reaction process and product morphology, etc., to achieve high purity, ensure leaching efficiency, and improve product added value. Effect
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Embodiment 1
[0049] A kind of in situ combustion synthesis preparation B 4 The method of C fiber, its process flow chart sees figure 1 , specifically follow the steps below:
[0050] Step 1: Mechanical Activation
[0051] Boron oxide and magnesium powder are mixed in a molar ratio, put into a high-energy ball mill for mechanical activation treatment, and a boron-containing precursor mixture is obtained; wherein, in a molar ratio, B 2 o 3 : Mg=1:3; the process parameters of the high-energy ball mill are: the mass ratio of material to ball is 1:10, the ball milling speed is 300rpm, and the ball milling time is 30min.
[0052] Step 2: Self-propagating synthesis
[0053] Mix the boron-containing precursor mixture and carbon fiber evenly in molar ratio, put it into the mold, press it into a block billet at 10MPa, place it in a self-propagating reaction furnace, and use the local ignition method to initiate the self-propagating reaction, and the temperature is controlled at 500°C , to obtai...
Embodiment 2
[0062] A kind of in situ combustion synthesis preparation B 4 The method of C fiber is carried out as follows:
[0063] Step 1: Mechanical Activation
[0064] Boron oxide and magnesium powder are mixed in a molar ratio, put into a high-energy ball mill for mechanical activation treatment, and a boron-containing precursor mixture is obtained; wherein, in a molar ratio, B 2 o 3 : Mg=1:2.5; The process parameters of the high-energy ball mill are: the mass ratio of material to ball is 1:15, the ball milling speed is 200rpm, and the ball milling time is 60min.
[0065] Step 2: Self-propagating synthesis
[0066] Mix the boron-containing precursor mixture and carbon fiber evenly in molar ratio, put it into the mold, press it into a block billet at 20MPa, place it in a self-propagating reaction furnace, and use the local ignition method to initiate the self-propagating reaction, and the temperature is controlled at 800°C , to obtain the reaction material, after the reaction mater...
Embodiment 3
[0075] A kind of in situ combustion synthesis preparation B 4 The method of C fiber is carried out as follows:
[0076] Step 1: Mechanical Activation
[0077] Boron oxide and magnesium powder are mixed in a molar ratio, put into a high-energy ball mill for mechanical activation treatment, and a boron-containing precursor mixture is obtained; wherein, in a molar ratio, B 2 o 3 : Mg=1:3; The technological parameters of the high-energy ball mill are: the mass ratio of material to ball is 1:20, the ball milling speed is 400rpm, and the ball milling time is 100min.
[0078] Step 2: Self-propagating synthesis
[0079] Mix the boron-containing precursor mixture and carbon fiber evenly in molar ratio, put it into the mold, press it into a block billet at 40MPa, place it in a self-propagating reaction furnace, and use the local ignition method to initiate the self-propagating reaction, and the temperature is controlled at 600°C , to obtain the reaction material, after the reaction ...
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