Building heat-insulating foam material and preparation method thereof
A thermal insulation material and construction technology, applied in the field of materials, can solve the problems of reduced storage stability of finished products, poor compatibility between inorganic fillers and polymers, high thermal conductivity, etc., and achieve good thermal insulation, improved mechanical properties, and low thermal conductivity. Effect
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Embodiment 1
[0025] 1. The organic filler emulsion is composed of the following raw materials in parts by weight:
[0026] Carbon nanotube 17, ricinoleic acid 4, 8-hydroxyquinoline 1, monoethanolamine 3, Span-801, pentaerythritol 8,
[0027] The preparation method comprises the following steps:
[0028] (1) Take carbon nanotubes, add them to 97% sulfuric acid solution that is 40 times its weight, raise the temperature to 65°C, heat and stir for 3 hours, filter, wash the precipitate with water, dry at 105°C in vacuum for 2 hours, and cool to At room temperature, oxidized carbon nanotubes are obtained;
[0029] (2) Take pentaerythritol, keep stirring at 80°C for 20 minutes, add 8-hydroxyquinoline, keep stirring for 10 minutes, add the above-mentioned carbon dioxide nanotubes, put it into a constant temperature water bath at 60°C, add monoethanolamine, keep stirring 3 hours, discharging, to obtain alcohol aminated carbon nanotubes;
[0030] (3) Take ricinoleic acid, add it to 20 times its ...
Embodiment 2
[0040] 1. Preparation of organic filler emulsion:
[0041] It is composed of the following raw materials in parts by weight:
[0042] Carbon nanotube 10, ricinoleic acid 3, 8-hydroxyquinoline 0.6, monoethanolamine 2, Span-800.4, pentaerythritol 6;
[0043] The preparation method comprises the following steps:
[0044] (1) Take carbon nanotubes, add them to 95% sulfuric acid solution that is 30 times its weight, increase the temperature to 60°C, heat and stir for 2 hours, filter, wash the precipitate with water, dry at 100°C for 1 hour in vacuum, and cool to At room temperature, oxidized carbon nanotubes are obtained;
[0045] (2) Take pentaerythritol, keep stirring at 75°C for 15 minutes, add 8-hydroxyquinoline, keep stirring for 4 minutes, add the above-mentioned carbon dioxide nanotubes, put it into a constant temperature water bath at 50°C, add monoethanolamine, keep stirring 2 hours, discharging, to obtain alcohol aminated carbon nanotubes;
[0046] (3) Take ricinoleic...
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