Efficient process for producing stevioside
A production process, stevioside technology, applied in the field of high-efficiency stevioside production technology, can solve the problems of unqualified product quality indicators, large stevioside content loss, large sewage treatment volume, etc., and achieve long resin regeneration cycle and resin treatment volume Large, low-volume effects
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Embodiment 1
[0023] (1) Take 100kg of fresh stevia leaves that have not been dried in the sun. After testing, the stevioside content is 6.36%, and the water content is 50.8%. Extracted 4 times in the extractor at 160r / min, each time extracted for 1.5h, to obtain 436L extract;
[0024] (2) Add 6.25L 30°C mass fraction of 25% ferrous sulfate aqueous solution to the extract, adjust the pH value to 9.3 with 30°C mass fraction of 25% calcium hydroxide aqueous solution, stir and flocculate at 30°C for 30 minutes, filter through 500 mesh Obtain filtrate after cloth filtration;
[0025] (3) Adsorb the filtrate with macroporous adsorption resin DA201-H, and analyze it with ethanol aqueous solution with a volume fraction of 30%, to obtain a primary analysis solution;
[0026] (4) Concentrate the primary analysis solution at 58°C until the ethanol content is 15.3%, then pass through cation exchange resin D001 and anion exchange resin D941 in sequence for desalination and decolorization, and after an...
Embodiment 2
[0029] (1) Take 100kg of fresh stevia leaves that have not been dried in the sun. After testing, the stevioside content is 5.87%, and the water content is 50.6%. Extracted 4 times in an extractor at 160r / min, each time for 1.5h, to obtain 440L extract;
[0030] (2) Add 10L 30°C mass fraction of 25% ferrous sulfate aqueous solution to the extract, adjust the pH value to 9.2 with 30°C mass fraction of 25% calcium hydroxide aqueous solution, stir and flocculate at 30°C for 30min, filter cloth with 500 mesh Obtain filtrate after filtering;
[0031] (3) Adsorb the filtrate with macroporous adsorption resin DA201-H, and analyze it with ethanol aqueous solution with a volume fraction of 40%, to obtain a primary analysis solution;
[0032] (4) Concentrate the primary analysis solution at 60°C until the ethanol content is 15.8%, then pass through cation exchange resin D001 and anion exchange resin D762 in sequence for desalination and decolorization, and obtain the secondary analysis ...
Embodiment 3
[0035] (1) Take 100kg of fresh stevia leaves that have not been dried in the sun. After testing, the stevioside content is 6.20%, and the water content is 51.4%. Grind it with a ball mill to a paste of 200 mesh or finer, add 200L of 20℃ water, and spray Extracted 5 times in an extractor with a shower pressure of 0.3MPa, and extracted for 1.5 hours each time to obtain 1042L extract;
[0036] (2) Add 20L 31°C mass fraction of 25% ferrous chloride aqueous solution to the extract, adjust the pH value to 9.3 with 31°C mass fraction of 25% calcium hydroxide aqueous solution, stir and flocculate at 31°C for 30 minutes, filter with 500 mesh Obtain filtrate after cloth filtration;
[0037] (3) Adsorb the filtrate with macroporous adsorption resin DA201-H, and analyze it with ethanol aqueous solution with a volume fraction of 50%, to obtain a primary analysis solution;
[0038] (4) Concentrate the primary analysis solution at 57°C until the ethanol content is 15.0%, then pass through c...
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