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Solvent composition, cleaning method, coating film formation method, heat transfer medium, and heat cycle system

A technology of solvent composition and film coating, which is applied in the preparation of detergent mixture composition, detergent composition, non-surface active detergent composition, etc., can solve the problems that have not been recorded, and achieve excellent stability and cleanability Excellent, excellent solubility effect

Active Publication Date: 2018-03-27
ASAHI GLASS CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, in Patent Documents 1 and 2, there is no description of adding 1-chloro-3,3-difluoro-1-propyne to 1-chloro-2,3,3-trifluoro-1-propene to make 1- Chloro-2,3,3-trifluoro-1-propene stabilization technology

Method used

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  • Solvent composition, cleaning method, coating film formation method, heat transfer medium, and heat cycle system
  • Solvent composition, cleaning method, coating film formation method, heat transfer medium, and heat cycle system
  • Solvent composition, cleaning method, coating film formation method, heat transfer medium, and heat cycle system

Examples

Experimental program
Comparison scheme
Effect test

Embodiment

[0133] Hereinafter, the present invention will be described in detail through examples. The present invention is not limited to these embodiments. Examples 1-17 are examples of the solvent composition of the present invention, and examples 18-21 are comparative examples.

manufacture example

[0134] (Manufacturing example: Manufacturing of HCFC-244ca)

[0135] A 2-liter four-necked flask equipped with a stirrer, a Dimuro cooler, and a glass distillation tower filled with Raschig rings (the number of plates measured is 5 layers) is charged with 1204g (9.12 mol) 2,2,3,3-tetra Fluoropropanol (TFPO) and 12g (0.17 mole) of N,N-dimethylformamide (DMF). 1078 g (9.12 mol) of thionyl chloride was dropped, and the mixture was stirred at normal temperature for 12 hours. The reactor was heated to 100°C, and reactive distillation was carried out using a reflux timer under the condition that the ratio of reflux time / distillation time was 5 / 1. The distilled HCFC-244ca was neutralized with a 20% by mass aqueous potassium hydroxide solution. The recovered HCFC-244ca (purity 100%) was 979 g (6.50 mol).

[0136] (Production example: Production of HCFO-1233yd and 1-chloro-3,3-difluoro-1-propyne)

[0137] Using 2000 g of HCFC-244ca as a raw material, 19.9 g of tetra-n-butylammonium chlori...

example 1～17

[0138] (Examples 1-17: Production of solvent composition (Example))

[0139] Using the above-obtained HCFO-1233yd (Z), HCFO-1233yd (E) and the mixture (X), according to the content ratio shown in Table 1, 100 g of HCFO-1233yd (Z) and / or HCFO-1233yd ( E) Solvent composition with 1-chloro-3,3-difluoro-1-propyne as a stabilizer. The values ​​of HCFO-1233yd(Z), HCFO-1233yd(E) and 1-chloro-3,3-difluoro-1-propyne shown in Table 1 are relative to the content of HCFO-1233yd and 1-chloro-3 The content ratio (mass%) of each component to the total content of 3-difluoro-1-propyne. In addition, the solvent compositions of Examples 1 to 17 are solvent compositions composed only of HCFO-1233yd and 1-chloro-3,3-difluoro-1-propyne.

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Abstract

Provided are: a solvent composition that has an excellent ability to dissolve various organic substances, has excellent cleaning performance and drying properties, does not cause detrimental effects to the global environment, and has superior stability; a cleaning method using the solvent composition; a coating film formation method; a heat transfer medium that includes the solvent composition; and a heat cycle system using the heat transfer medium. A solvent composition that includes 1-chloro-2,3,3-trifluoro-1-propene and 1-chloro-3,3-difluoro-1-propene; a cleaning method in which the solventcomposition is brought into contact with an article to be cleaned; a method in which a non-volatile organic compound is dissolved in the solvent composition to prepare a coating film-forming composition, the coating film-forming composition is applied upon an object to be coated, and thereafter the solvent composition is evaporated to form a coating film comprising the non-volatile organic compound; a heat transfer medium that includes the solvent composition; and a heat cycle system using the heat transfer medium.

Description

Technical field [0001] The present invention relates to a solvent composition that has excellent solubility for various organic substances, excellent cleaning properties, sufficient drying properties, no adverse effect on the global environment, and excellent stability. Specifically, the solvent composition of the present invention can be used for a wide range of applications such as cleaning solvents, diluting coating solvents, and thermal conductive media. Background technique [0002] In the manufacture of ICs, electronic components, precision mechanical parts, optical components, etc., in the manufacturing process, assembly process, final finishing process, etc., the parts are cleaned with a cleaning solvent to remove the solder adhering to the parts. Agent, processing oil, wax, mold release agent, dust, etc. In addition, as a method for manufacturing articles with coating films containing various organic chemical substances such as lubricants, it is known, for example, to p...

Claims

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Application Information

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IPC IPC(8): C11D3/24C09D7/20C09D201/00C09K5/04
CPCC11D7/5018C11D7/30B08B3/08C09K5/10C09D7/20C11D2111/12C09D201/00C09K5/044C09K2205/126C08K5/02C08B3/08C07C21/18C07C21/22C11D3/43C07C19/10
Inventor 中村允彦光冈宏明市野川真理藤森厚史冈本秀一
Owner ASAHI GLASS CO LTD
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