Fire-proof glass membrane based on PAM-inorganic medium phase separation and polymerization and polymerization and preparation method and application of glass membrane

A technology of inorganic matrix and fireproof glass, which is applied in the field of fireproof material manufacturing, can solve the problems of complex processing of perfusion fireproof glass, limitation of installation cost and scope of use, compound glass cannot be cut at will, and achieves small weight, variable properties, easy processing The effect of convenient installation and transportation

Inactive Publication Date: 2018-04-06
ZHEJIANG SHUREN UNIV
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  • Abstract
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  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although the composite fire-resistant glass prepared by the interlayer method has heat insulation, earthquake resistance, and impact resistance, its fire resistance is generally poor; while the perfusion fire-resistant glass prepared by the grouting method has good fire-resistant integrity and good heat insulation effect. However, due to the large amount of water contained in the grout, the thickness and weight of the fireproof glass are large, which limits its installation cost and scope of use.
At the same time, because the custom-made double-glazed box is filled with fireproof liquid to form a gel layer during processing, this makes the processing of poured fireproof glass complicated, and the composite glass processed according to size cannot be cut at will.

Method used

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  • Fire-proof glass membrane based on PAM-inorganic medium phase separation and polymerization and polymerization and preparation method and application of glass membrane

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] The first step is to dissolve sodium metaaluminate with deionized water, and adjust the pH of the solution to 9.0 with sodium hydroxide to completely dissolve the sodium metaaluminate, heat and evaporate the solution to near saturation, cool to room temperature, stand still, filter, and take The filtrate is used as the inorganic matrix saturated solution A for subsequent use;

[0018] In the second step, mix 92 parts by weight of acrylamide with 8 parts by weight of a saturated aqueous solution of N,N'-methylenebisacrylamide mixture, add pure water under stirring until it is completely dissolved, and filter to obtain a saturated solution after standing still B standby;

[0019] In the third step, the hydrogen peroxide is made into an aqueous solution with a mass fraction of 10% with purified water to obtain initiator solution C for subsequent use.

[0020] The fourth step is to fully mix 40 parts by weight of solution A and 60 parts by weight of solution B, add 0.2 par...

Embodiment 2

[0022] In the first step, 70 parts by weight of aluminum potassium sulfate are dissolved in deionized water, and the pH of the solution is adjusted to 11.0 with sodium hydroxide, so that aluminum potassium sulfate is completely dissolved, and 25 parts by weight of water glass, 5 parts by weight of Sodium chloride is heated and stirred to make it completely dissolved, the solution is heated and evaporated to saturation, cooled to room temperature, left to stand, filtered, and the filtrate is taken as the inorganic matrix saturated solution A for subsequent use;

[0023] In the second step, mix 98 parts by weight of acrylamide with 2 parts by weight of a saturated aqueous solution of N,N'-methylenebisacrylamide mixture, add pure water under stirring until it is completely dissolved, and filter after standing to obtain the polymer Monomer saturated solution B is for later use.

[0024] In the third step, potassium persulfate is prepared into an aqueous solution with a mass fracti...

Embodiment 3

[0027] In the first step, 40 parts by weight of aluminum chloride are dissolved in deionized water, and the pH of the solution is adjusted to 10.0 with sodium hydroxide to completely dissolve the aluminum chloride, and 45 parts by weight of water glass, 15 parts by weight of The sodium chloride is heated and stirred to make it completely dissolved, the solution is heated and evaporated to saturation, cooled to room temperature, left to stand, filtered, and the filtrate is used as the inorganic matrix saturated solution A for subsequent use;

[0028] In the second step, mix 97 parts by weight of acrylamide with 3 parts by weight of a saturated aqueous solution of N,N'-methylenebisacrylamide mixture, add pure water under stirring until it is completely dissolved, and filter to obtain a saturated solution after standing still B standby.

[0029] In the third step, the ammonium persulfate is formulated into an aqueous solution with a mass fraction of 10% with purified water, and t...

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Abstract

The invention discloses a fire-proof glass membrane based on PAM-inorganic medium phase separation and polymerization and a preparation method and application of the glass membrane. The preparation method comprises the steps that 30-60 weight parts of saturated aqueous solution of acrylic amide and N,N'-methylenebis acrylamid mixture and 40-70 weight parts of saturated aqueous solution, with the pH larger than 9, of an inorganic medium are sufficiently mixed, then 0.2-1.5 weight parts of initiator with the mass fraction of 10% is added into the mixed solution, after uniform mixing, tape casting or molding is conducted, and then the fire-proof glass membrane based on the PAM-inorganic medium phase separation and polymerization is obtained through polymerization, wherein the inorganic mediumis formed by one or two of water glass and aluminum salt in any proportion. Under high-temperature firing of a fire disaster, the water-proof glass membrane can form a fire-proof material covering layer, the covering layer is made to become an inorganic water-proof skeleton, the mechanical strength, the fire resistance and the thermal-insulation effect of the fire-proof layer are improved, and the mechanical integrity and the thermal-insulation fire resistance can be kept in the fire disaster.

Description

technical field [0001] The invention relates to the field of fireproof material manufacturing, in particular to a fireproof glass film based on PAM-inorganic matrix phase separation polymerization and its preparation method and application. Background technique [0002] Fireproof glass is a kind of safety glass. It is a special glass with transparency that can block flames, smoke, heat radiation, prevent flames from spreading, and maintain integrity and stability within a certain period of time. It should also have certain resistance Impact strength, it can still play a protective role for a certain period of time under the flame baking at 1000 ℃. Fire-resistant glass is now being widely used in large-scale public building partitions, fire compartments, outdoor curtain walls and other building parts. Fire-resistant glass is characterized by transparency, which satisfies the harmony and unity of building fire protection and architectural aesthetics to the greatest extent. ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08J5/18C08F220/56C08F222/38C03C27/12B32B17/10B32B27/34C08L33/26
CPCC08J5/18B32B17/10724B32B27/34B32B2307/304B32B2307/3065C08F220/56C08J2333/26C08F222/385
Inventor 王智敏沈素媚陆胤张德勇许惠英田甜赵兴勇秦世明
Owner ZHEJIANG SHUREN UNIV
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