Full-dull polyester and polyester composite yarn and preparation method thereof

A technology of full extinction and composite filament, which is applied in the manufacture of rayon, chemical post-treatment of synthetic polymer rayon, spinneret assembly, etc.

Active Publication Date: 2018-05-04
JIANGSU HENGLI CHEM FIBER
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the performance of single matte PET fiber or bright PET fiber still cannot meet the needs of consumers. How to overcome the difficulties in the production and processing of heterogeneous composite yarns to realize the composite

Method used

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  • Full-dull polyester and polyester composite yarn and preparation method thereof
  • Full-dull polyester and polyester composite yarn and preparation method thereof
  • Full-dull polyester and polyester composite yarn and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0070] A kind of preparation method of fully dull polyester composite yarn, the steps are as follows:

[0071] (1) Preparation of oiling agent for oiling: 2-hydroxymethyl-12-crown-4 and dodecyl phosphate potassium salt, trimethylolpropane laurate and sodium dodecyl sulfonate After mixing evenly at room temperature, add it to 9# mineral oil and stir evenly at 40°C for 1 hour to obtain an oil agent. The addition amount of each component is as follows in parts by weight: 9# mineral oil is 2 parts; trimethylolpropane Lauric acid ester is 10 parts; 2-hydroxymethyl-12-crown-4 is 90 parts; dodecyl phosphate potassium salt is 8 parts; sodium dodecylsulfonate is 3 parts; the prepared oil The content of the crown ether is 79.6wt%. The high temperature resistance of the oil is excellent. After heat treatment at 200°C for 2 hours, the thermal weight loss is 14.5wt%. The viscosity of the oil is low. At (50±0.01)°C, the kinematic viscosity 29.6mm 2 / s, the kinematic viscosity after the co...

Embodiment 2

[0077] A kind of preparation method of fully dull polyester composite yarn, the steps are as follows:

[0078] (1) Preparation of oiling agent for oiling: 15-crown ether-5 and isomeric tridecanol polyoxyethylene ether phosphate potassium salt, trimethylolpropane laurate and sodium pentadecylsulfonate in After mixing evenly at room temperature, add it to 10# mineral oil and stir evenly at 43°C for 1.5 hours to obtain the oil agent. In parts by weight, the addition amount of each component is as follows: 10# mineral oil is 2 parts; 15 parts of propane laurate; 70 parts of 15-crown-5; 10 parts of potassium isotridecyl polyoxyethylene ether phosphate; 7 parts of sodium pentadecyl sulfonate; prepared oil The content of crown ether in the agent is 67.30wt%. The high temperature resistance of the oil agent is excellent. After heat treatment at 200°C for 2 hours, the thermal weight loss is 13wt%. The viscosity of the oil agent is low. 28.1mm 2 / s, the kinematic viscosity after the c...

Embodiment 3

[0084] A kind of preparation method of fully dull polyester composite yarn, the steps are as follows:

[0085] (1) Preparation of oiling agent for oiling: mix 2-hydroxymethyl-15-crown-5 with potassium salt of tetradecyl phosphate, trimethylolpropane laurate and sodium pentadecylsulfonate After mixing evenly at room temperature, add it to 11# mineral oil and stir evenly at 48°C for 3 hours to obtain an oil agent. The addition amount of each component is as follows in parts by weight: 11# mineral oil is 8 parts; 10 parts of propane laurate; 85 parts of 2-hydroxymethyl-15-crown-5; 11 parts of potassium tetradecyl phosphate; 5 parts of sodium pentadecylsulfonate; The content of crown ether in the oil is 70.83wt%. The high temperature resistance of the oil is excellent. After heat treatment at 200°C for 2 hours, the thermal weight loss is 11wt%. The viscosity of the oil is low. Viscosity is 30.1mm 2 / s, the kinematic viscosity after the concentration is 10wt% emulsion configured ...

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Abstract

The invention relates to a full-dull polyester and polyester composite yarn and a preparation method thereof. According to the preparation method, dull PET (polyethylene terephthalate) melts and super-bright PET melts are metered, extruded by a composite spinneret plate, cooled, coated with oil and wound to prepare POYs (polyester pre-oriented yarns); the POYs are heated, drawn, falsely twisted, shaped in a heating manner and wound to prepare DTYs (draw texturing yarns) through a yarn guide pipe and a network, namely, the full-dull polyester and polyester composite yarn. An oil agent for oiling contains crown ether, the content of the crown ether is 67.30-85.58wt%, a full-dull polyester and polyester composite yarn extruded by the same composite spinneret plate simultaneously contain dullPET monofilaments dispersed matt agents and super-bright PET monofilaments dispersed matt agents, the matt agents are mixture of unformed titanium dioxide and unformed silicon dioxide or mixture of calcium carbonate and unformed silicon dioxide, and the composite yarn gloss is lower than 20%. The preparation method is simple, the smooth spinning of fibers is achieved in the preparation process, and fabrics prepared by the method are excellent in performance and has great application values.

Description

technical field [0001] The invention belongs to the field of fiber preparation, and relates to a full-dull polyester composite yarn and a preparation method thereof. Background technique [0002] With the development of modern textile technology and the continuous improvement of people's living standards, people put forward higher requirements for the output, performance and quality of chemical fibers used in clothing, decorative and industrial textiles. Therefore, in recent years, researchers have devoted themselves to chemical Research and development of new varieties of fibers to meet people's market demand for fibers with high added value. [0003] At present, there is a demand for high-sensitivity and high-functionality textiles in the consumer market. In order to meet these needs, traditional fiber manufacturing must be transformed, and high-function fibers, high-sensitivity fibers, smart fibers, and degradable fibers must be developed. Improve the technological conte...

Claims

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Application Information

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IPC IPC(8): D01D4/02D01D5/253D01F6/92D01F1/10D01F11/08D06M13/11D06M13/295D06M13/256D06M13/224D06M13/02D06M101/32
CPCD01D4/02D01D5/253D01F1/10D01F6/92D01F11/08D02G1/20D06M13/02D06M13/11D06M13/224D06M13/256D06M13/292D06M13/295D06M2101/32
Inventor 尹立新张烨陈瑞王力军张群
Owner JIANGSU HENGLI CHEM FIBER
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